Asymmetric flow field-flow fractionation with multiangle light scattering detection for characterization of cellulose nanocrystals

Biomacromolecules

Volumn 13, Issue 9, 2012, Pages 2671-2679

  Guan, Xia ^a   Cueto, Rafael ^b   Russo, Paul ^b   Qi, Yadong ^c   Wu, Qinglin ^a  

^a LOUISIANA STATE UNIVERSITY AGRICULTURAL CENTER   (United States)

^b LOUISIANA STATE UNIVERSITY   (United States)

^c SOUTHERN UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ASYMMETRIC FLOWS; CELLULOSE NANOCRYSTALS; CRYSTAL LENGTH; CRYSTAL LENGTH DISTRIBUTION; ELUTION BEHAVIOR; ELUTION PROFILES; HIGH DEGREE OF ACCURACY; HIGH-PRESSURE HOMOGENIZERS; HOMOGENIZATION TREATMENT; MICROCRYSTALLINE CELLULOSE; MULTI-ANGLE LIGHT SCATTERINGS; PEAK SHAPES; RIGID RODS; ROD-LIKE PARTICLES; SAMPLE LOADS; SEPARATION PROCESS; SIZE DISTRIBUTION MEASUREMENTS; TEM IMAGES; TOBACCO MOSAIC VIRUS; TRANSMISSION ELECTRON MICROSCOPY TEM;

DETECTORS; HIGH PRESSURE EFFECTS; LIGHT SCATTERING; PARTICLE SIZE ANALYSIS; TRANSMISSION ELECTRON MICROSCOPY; VIRUSES;

CELLULOSE DERIVATIVES;

CELLULOSE NANOCRYSTAL; MICROCRYSTALLINE CELLULOSE; NANOCRYSTAL; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL STRUCTURE; ELUTION; FIELD FLOW FRACTIONATION; LIGHT SCATTERING; PARTICLE SIZE; PRIORITY JOURNAL; TRANSMISSION ELECTRON MICROSCOPY;

CELLULOSE; FRACTIONATION, FIELD FLOW; LIGHT; MICROSCOPY, ELECTRON, TRANSMISSION; NANOPARTICLES; PARTICLE SIZE; SCATTERING, RADIATION;

CELLULOSE DERIVATIVES; DETECTORS; HIGH PRESSURE; OPTICAL SCATTERING; PARTICLE SIZE; TRANSMISSION ELECTRON MICROSCOPY; VIRUSES;

GOSSYPIUM HIRSUTUM; TOBACCO MOSAIC VIRUS;

EID: 84866068311     PISSN: 15257797     EISSN: 15264602     Source Type: Journal    
DOI: 10.1021/bm300595a     Document Type: Article

References (33)

1. Zhou, C.; Wu, Q.; Yue, Y.; Zhang, Q. Application of rod-shaped cellulose nanocrystals in polyacrylamide hydrogels J. Colloid Interface Sci. 2011, 353 (1) 116-123
2. Favier, V.; Chanzy, H.; Cavaille, J. Y. Polymer nanocomposites reinforced by cellulose whiskers Macromolecules 1995, 28 (18) 6365-6367
3. Yoshiharu, N.; Shigenori, K.; Masahisa, W.; Takeshi, O. Cellulose microcrystal film of high uniaxial orientation Macromolecules 1997, 30 (20) 6395-6397
4. Liu, H.; Liu, D.; Yao, F.; Wu, Q. Fabrication and properties of transparent polymethylmethacrylate/cellulose nanocrystals composites Bioresour. Technol. 2010, 101 (14) 5685-5692
5. Elazzouzi-Hafraoui, S.; Nishiyama, Y.; Putaux, J.-L.; Heux, L.; Dubreuil, F.; Rochas, C. The shape and size distribution of crystalline nanoparticles prepared by acid hydrolysis of native cellulose Biomacromolecules 2008, 9 (1) 57-65 (Pubitemid 351201582)
6. Lahiji, R. R.; Xu, X.; Reifenberger, R.; Raman, A.; Rudie, A.; Moon, R. J. Atomic force microscopy characterization of cellulose nanocrystals Langmuir 2010, 26 (6) 4480-4488
7. Kontturi, E.; Vuorinen, T. Indirect evidence of supramolecular changes within cellulose microfibrils of chemical pulp fibers upon drying Cellulose 2009, 16 (1) 65-74
8. de Souza Lima, M. M.; Borsali, R. Static and dynamic light scattering from polyelectrolyte microcrystal cellulose Langmuir 2002, 18 (4) 992-996 (Pubitemid 35390182)
9. de Souza Lima, M. M.; Borsali, R. Rodlike cellulose microcrystals: Structure, properties, and applications Macromol. Rapid Commun. 2004, 25 (7) 771-787
10. Messaud, F. A.; Sanderson, R. D.; Runyon, J. R.; Otte, T.; Pasch, H.; Williams, S. K. R. An overview on field-flow fractionation techniques and their applications in the separation and characterization of polymers Prog. Polym. Sci. 2009, 34 (4) 351-368
11. von der Kammer, F.; Legros, S.; Larsen, E. H.; Loeschner, K.; Hofmann, T. Separation and characterization of nanoparticles in complex food and environmental samples by field-flow fractionation Trac-Trends Anal. Chem. 2011, 30 (3) 425-436
12. Schimpf, M. E.; Caldwell, K.;; Giddings, J. C. Field-flow fractionation handbook; John Wiley and Sons, Inc.: New York, 2000.
13. Giddings, J. C. Field-flow fractionation-analysis of macromolecular, colloidal,and particulate materials Science 1993, 260 (5113) 1456-1465
14. Giddings, J. C.; Myers, M. N. Steric field-flow fractionation-new method for separating 1-100 μm particles Sep. Sci. Technol. 1978, 13 (8) 637-645 (Pubitemid 9394024)
15. Wahlund, K. G.; Giddings, J. C. Properties of an asymmetrical flow field-flow fractionation channel having one permeable wall Anal. Chem. 1987, 59 (9) 1332-1339 (Pubitemid 17568673)
16. Alasonati, E.; Benincasa, M.-A.; Slaveykova, V. I. Asymmetrical flow field-flow fractionation coupled to multiangle laser light scattering detector: Optimization of crossflow rate, carrier characteristics, and injected mass in alginate separation J. Sep. Sci. 2007, 30 (14) 2332-2340 (Pubitemid 47497036)
17. Mao, S.; Augsten, C.; Maeder, K.; Kissel, T. Characterization of chitosan and its derivatives using asymmetrical flow field-flow-fractionation: A comparison with traditional methods J. Pharm. Biomed. Anal. 2007, 45 (5) 736-741 (Pubitemid 350087562)
18. Hupfeld, S.; Ausbacher, D.; Brandl, M. Asymmetric flow field-flow fractionation of liposomes: optimization of fractionation variables J. Sep. Sci. 2009, 32 (9) 1465-1470
19. Zattoni, A.; Rambaldi, D. C.; Reschiglian, P.; Melucci, M.; Krol, S.; Coto Garcia, A. M.; Sanz-Medel, A.; Roessner, D.; Johann, C. Asymmetrical flow field-flow fractionation with multi-angle light scattering detection for the analysis of structured nanoparticles J. Chromatogr., A 2009, 1216 (52) 9106-9112
20. Chun, J.; Fagan, J. A.; Hobbie, E. K.; Bauer, B. J. Size separation of single-wall carbon nanotubes by flow-field flow fractionation Anal. Chem. 2008, 80 (7) 2514-2523 (Pubitemid 351499835)
21. Moon, M. H.; Kang, D. J.; Jung, J. H.; Kim, J. M. Separation of carbon nanotubes by frit inlet asymmetrical flow field-flow fractionation J. Sep. Sci. 2004, 27 (9) 710-717 (Pubitemid 38961245)
22. Phelan, F. R., Jr.; Bauer, B. J. Simulation of nanotube separation in field-flow fractionation (FFF) Chem. Eng. Sci. 2007, 62 (17) 4620-4635 (Pubitemid 47176525)
23. Braun, B.; Dorgan, J. R.; Chandler, J. P. Cellulosic nanowhiskers. Theory and application of light scattering from polydisperse spheroids in the Rayleigh-Gans-Debye regime Biomacromolecules 2008, 9 (4) 1255-1263 (Pubitemid 351639580)
24. Gimbert, L. J.; Andrew, K. N.; Haygarth, P. M.; Worsfold, P. J. Environmental applications of flow field-flow fractionation (FIFFF) Trac-Trends Anal. Chem. 2003, 22 (10) 615-633 (Pubitemid 41685809)
25. Zimm, B. H. The scattering of light and the radial distribution function of high polymer solutions J. Chem. Phys. 1948, 16 (12) 1093-1099
26. van de Hulst, H. C. Light scattering by small particles; Wiley: New York, 1957.
27. Yue, Y., A comparative study of cellulose I and II fibers and nanocrystals. M.S. Thesis, Louisiana State University, Baton Rouge, LA, 2011.
28. Cush, R.; Russo, P. S.; Kucukyavuz, Z.; Bu, Z. M.; Neau, D.; Shih, D.; Kucukyavuz, S.; Ricks, H. Rotational and translational diffusion of a rodlike virus in random coil polymer solutions Macromolecules 1997, 30 (17) 4920-4926 (Pubitemid 127574307)
29. Barber, P. W.; Wang, D. S. Rayleigh-Gans-Debye applicability to scattering by nonspherical particles Appl. Opt. 1978, 17 (5) 797-803
30. Buitenhuis, J.; Dhont, J. K. G.; Lekkerkerker, H. N. W. Scattering of light from cylindrical particles-coupled dipole method calculations and the range of validity of the Rayleigh-Gans-Debye approximation J. Colloid Interface Sci. 1994, 162 (1) 19-24
31. Wyatt, P. J.; Villapando, D. N. High-precision measurement of submicrometer particle size distributions Langmuir 1997, 13 (15) 3913-3914 (Pubitemid 127591798)
32. Fraden, S.; Maret, G.; Caspar, D. L. D. Angular-correlations and the isotropic-nematic phase-transition in suspensions of tobacco mosaic virus Phys. Rev. E 1993, 48 (4) 2816-2837
33. Berne, B. J.;; Pecora, R. Dynamic light scattering; Wiley: New York, 1976, Ch. 5.