Development and validation of the high performance liquid chromatography-ion exclusion method for detection of lactic acid in milk

Food Chemistry

Volumn 135, Issue 3, 2012, Pages 1078-1082

  Milagres, Maria Patricia ^a   Brandão, Sebastião César Cardoso ^a   Magalhães, Mirella Araujo ^b   Minim, Valéria Paula Rodrigues ^a   Minim, Luis Antonio ^a  

^a FEDERAL UNIVERSITY OF VIÇOSA   (Brazil)

^b Ministry of Agriculture   (Brazil)

Author keywords

High performance liquid chromatography; Ion exclusion; Lactic acid; Method development; Method validation; Milk

Indexed keywords

ANALYTICAL METHOD; ANOVA ANALYSIS; CALIBRATION CURVES; DETECTION AND QUANTIFICATION LIMIT; ION EXCLUSION; METHOD DEVELOPMENT; METHOD VALIDATIONS; MILK; QUALITY CONTROL TOOL; UV DETECTION; VARIATION COEFFICIENT;

CHROMATOGRAPHY; FERMENTED MILK; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IONS;

LACTIC ACID;

LACTIC ACID; SODIUM HYDROXIDE;

ACCURACY; ARTICLE; CALIBRATION; FERMENTED PRODUCT; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ION EXCLUSION CHROMATOGRAPHY; MILK LEVEL; QUALITY CONTROL; ULTRAVIOLET RADIATION; VALIDATION PROCESS;

ANIMALS; CATTLE; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; LACTIC ACID; MILK;

EID: 84865790515     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2012.05.047     Document Type: Article

References (18)

1. S.F. Al-Zenki, H.M. Al-Mazeedi, S.N. Al-Hooti, T. Al-Atti, Q. Al-Mutawah, and H.F. Al-Omirah Quality and safety characteristics of milk sold in the state of kuwait Journal of Food Processing and Preservation 31 278 2007 702 713 (Pubitemid 350209541)
2. AOAC - Association of Official Analytical Chemists (1998), Official methods of analysis (18th ed.), Washington.
3. BIS - Bureau Indian Standards (1960). Identical Standard No. 1279. Methods of test for dairy industry: Part 1 rapid examination of milk, New Delhi.
4. G.E.P. Box, J.S. Hunter, and W.G. Hunter Statistics for experimenters: An introduction to design, data analysis, and model building 1st ed. 1978 John Wiley & Sons New York
5. F. Chinnici, U. Spinabelli, C. Riponi, and A. Amati Optimization of the determination of organic acids and sugars in fruit juices by ion-exclusion liquid chromatography Journal of Food Composition and Analysis 18 2005 121 130 (Pubitemid 39646719)
6. R. De Longhi, N. Spinardi, M.T. Nishimura, M.Y. Miyabe, L.C. Aragon-Alegro, and M.R. Costa A survey of the physicochemical and microbiological quality of ultra-heat-treated whole milk in Brazil during their shelf life International Journal of Dairy Technology 65 45 2011 50
7. FDA - Food and Drug Administration (2007). Grade A pasteurized milk ordinance - 2007 revision. US Department of Health and Human Services, Public Health Service, Food and Drug Administration.
8. K. Fischer, H.-P. Bipp, D. Bieniek, and A. Kettrup Determination of monomeric sugar and carboxylic acids by ion-exclusion chromatography Journal of Chromatography A 706 1995 361 373
9. MAPA - Ministério da Agricultura, Pecuária e Abastecimento do Brasil (2006). Instrução Normativa No. 68 de 12 de Dezembro de 2006. Métodos analíticos oficiais físico-químicos para controle de leite e produtos lácteos. Diário Oficial da União, Seção 1, p. 8.
10. M. Mori, K. Tanaka, M.I.H. Helaleh, Q. Xu, M. Ikedo, and Y. Ogura High-speed simultaneous ion-exclusion/cation-exchange chromatography of anions and cations on a weakly acidic cation-exchange resin column Journal of Chromatography A 997 2003 191 197 (Pubitemid 36627776)
11. S. Nada, D. Ilija, T. Igor, M. Jelena, and G. Ruzica Implication of food safety measures on microbiological quality of raw and pasteurized milk Food Control 25 2012 728 731
12. M. Novič, and P.R. Haddad Analyte-stationary phase interactions in ion-exclusion chromatography Journal of Chromatography A 1118 16 2006 19 28 (Pubitemid 43795880)
13. R.K. Robinson Dairy microbiology 2nd ed. 2002 Elsevier Applied Science London
14. K. Tanaka, H. Chikara, W. Hu, and K. Hasebe Separation of carboxylic acids on a weakly acidic cation-exchange resin by ion-exclusion chromatography Journal of Chromatography A 860 1999 187 196 (Pubitemid 29327217)
15. P. Walstra, T.J. Geurts, A. Noomen, A. Jellema, and M.A.J.S. Van Boekel Dairy technology. Principles of milk properties and processes 1st ed. 2002 Marcel Dekker New York
16. H.M. Wehr, and J.F. Frank Standard methods for the examination of dairy products 17th ed. 2004 American Public Health Association
17. T. Xiong, Q. Guan, S. Song, M. Hao, and M. Xie Dynamic changes of lactic acid bacteria flora during Chinese sauerkraut fermentation Food Control 26 2012 178 181
18. L. Yang, L. Liu, B.A. Olsen, and M.A. Nussbaum The determination of oxalic acid, oxamic acid and oxamide in a drug substance by ion exclusion chromatography Journal of Pharmaceutical and Biomedical Analysis 22 2000 487 493 (Pubitemid 30151238)