Optimisation for subcritical fluid extraction of 17-methyltestosterone with 1,1,1,2-tetrafluoroethane for HPLC analysis

Food Chemistry

Volumn 135, Issue 4, 2012, Pages 2988-2993

  Han, Yuqian ^a   Ma, Qinchuan ^a   Lu, Jie ^a   Xue, Yong ^a   Xue, Changhu ^a  

^a OCEAN UNIVERSITY OF CHINA   (China)

Author keywords

17 Methyltestosterone; Aquatic products; Determination; Subcritical R134a extraction

Indexed keywords

1 ,1 ,1 ,2-TETRAFLUOROETHANE; AQUATIC PRODUCTS; COSOLVENTS; DETERMINATION; EXTRACTION CONDITIONS; EXTRACTION PRESSURE; HPLC ANALYSIS; METHYL-TESTOSTERONE; MOBILE PHASE; OPTIMISATIONS; RESPONSE SURFACE METHODOLOGY; SENSITIVE METHOD; SUBCRITICAL FLUIDS;

ACETONITRILE;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

METHYLTESTOSTERONE; NORFLURANE;

ARTICLE; CONTROLLED STUDY; DRUG DETERMINATION; DRUG ISOLATION; EXTRACTION AND EXTRACTS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIMIT OF DETECTION; LINEAR SYSTEM; NONHUMAN; PRESSURE; PROCESS OPTIMIZATION; RESPONSE SURFACE METHOD; SUBCRITICAL FLUID EXTRACTION; TEMPERATURE; VALIDATION PROCESS;

ANDROGENS; ANIMALS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, SUPERCRITICAL FLUID; DRUG RESIDUES; FISHES; HYDROCARBONS, FLUORINATED; MEAT; METHYLTESTOSTERONE;

EID: 84865336671     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2012.07.081     Document Type: Article

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