Introducing enantioselective ultrahigh-pressure liquid chromatography (eUHPLC): Theoretical inspections and ultrafast separations on a new sub-2-μm Whelk-O1 stationary phase

Analytical Chemistry

Volumn 84, Issue 15, 2012, Pages 6805-6813

  Kotoni, Dorina ^a   Ciogli, Alessia ^a   Molinaro, Carmela ^a   D'Acquarica, Ilaria ^a   Kocergin, Jelena ^b   Szczerba, Ted ^b   Ritchie, Harald ^c   Villani, Claudio ^a   Gasparrini, Francesco ^a  

^a SAPIENZA UNIVERSITY OF ROME   (Italy)

^b REGIS TECHNOLOGIES INC   (United States)

^c Thermo Fisher Scientific   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CHIRAL STATIONARY PHASE; COVALENT ATTACHMENT; EFFICIENCY LOSS; ELUTION CONDITIONS; ENANTIOSELECTIVE; HIGH-SPEED; INTERNAL DIAMETERS; INTRINSIC KINETICS; KINETIC PLOTS; LOW MOLECULAR WEIGHT; MOBILE PHASIS; NORMAL PHASE; POROUS SILICA; REVERSED PHASE; SILICA PARTICLES; STATIONARY PHASE; TIME-SCALES; ULTRA-FAST; ULTRA-HIGH-PRESSURE LIQUID CHROMATOGRAPHY; ULTRAHIGH-PRESSURE LIQUID CHROMATOGRAPHIES;

EFFICIENCY; ENANTIOSELECTIVITY; LIQUID CHROMATOGRAPHY; SEPARATION; SILICA;

SHELLFISH;

POLYSACCHARIDE; SILICON DIOXIDE;

ARTICLE; CHEMISTRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; KINETICS; POROSITY; STEREOISOMERISM; THEORETICAL MODEL;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; KINETICS; MODELS, THEORETICAL; POLYSACCHARIDES; POROSITY; SILICON DIOXIDE; STEREOISOMERISM;

EID: 84864614152     PISSN: 00032700     EISSN: 15206882     Source Type: Journal    
DOI: 10.1021/ac301335b     Document Type: Article

References (55)

1. Giddings, J. C. Anal. Chem. 1965, 37, 60
2. Knox, J. H. J. Chromatogr. Sci. 1977, 15, 362
3. Poppe, J. H. J. Chromatogr. A. 1997, 778, 3
4. Wu, N.; Lippert, J. A.; Lee, J. J. Chromatogr. A. 2001, 911, 1
5. Jerkovich, A. D.; Mellors, J. S.; Jorgenson, J. W. LC-GC Eur. 2003, 16, 20
6. Majors, R. E. LC-GC N. Am. 2005, 23, 1248
7. Majors, R. E. LC-GC N. Am. 2006, 24, 248
8. Desmet, G.; Gzil, P.; Nguyen, D.T.-T.; Guillarme, D.; Rudaz, S.; Veuthey, J.-L.; Vervoort, N.; Torok, G.; Cabooter, D.; Clicq, D. Anal. Chem. 2006, 78, 2150
9. Guillarme, D.; Nguyen, D.T.-T.; Rudaz, S.; Veuthey, J.-L. J. Chromatogr. A 2007, 1149, 20
10. Carr, P. W.; Wang, X; Stoll, D. R. Anal. Chem. 2009, 81, 5342
11. Ward, T. J.; Ward, K. D. Anal. Chem. 2012, 84, 626
12. House, D. W.; Oroskar, A. A.; Oroskar, A. R. LC-GC N. Am. 2009, 9, 22
13. House, D. W.; Oroskar, A. A. LC-GC N. Am. 2010, 9, 32
14. Chankvetadze, B.; Yamamoto, C.; Okamoto, Y. Chem. Lett. 2003, 32 (9) 850
15. Chankvetadze, B.; Yamamoto, C.; Kamigaito, M.; Tanaka, N.; Nakanishi, K.; Okamoto, Y. J. Chromatogr. A 2006, 1110, 46
16. Cancelliere, G.; Ciogli, A.; D'Acquarica, I.; Gasparrini, F.; Kocergin, J.; Misiti, D.; Pierini, M.; Ritchie, H.; Simone, P.; Villani, C. J. Chromatogr. A 2010, 1217, 990
17. Ai, F.; Li, L.; Ng, S.-C.; Tan, T. T. Y. J. Chromatogr. A 2010, 1217, 7502
18. Lomsadze, K.; Jibuti, G.; Farkas, T.; Chankvetadze, B. J. Chromatogr. A 2012, 1234, 50
19. Pirkle, W. H.; Welch, C. J.; Lamm, B. J. Org. Chem. 1992, 57, 3854
20. Pirkle, W. H.; Welch, C. J. J. Liq. Chromatogr. 1992, 15, 1947
21. Decamp, W. H. Chirality 1989, 1, 2
22. Pirkle, W. H.; Welch, C. J. Tetrahedron: Asymmetry 1994, 5, 777
23. Villani, C.; Pirkle, W. H. J. Chromatogr. 1995, 693, 63
24. Villani, C.; Pirkle, W. H. Tetrahedron: Asymmetry 1995, 6, 27
25. Casarini, D.; Lunazzi, L.; Alcaro, S.; Gasparrini, F.; Villani, C. J. Org. Chem. 1995, 60, 5515
26. Pirkle, W. H.; Brice, L. J.; Caccamese, S.; Principato, G.; Failla, S. J. Chromatogr. A 1996, 721, 241
27. Pirkle, W. H.; Brice, L. J.; Widlanksi, J.; Roestamadji, J. Tetrahedron: Asymmetry 1996, 7, 2173
28. Pirkle, W. H.; Koscho, M. E.; Wu, Z. P. J. Chromatogr. A 1996, 726, 91
29. Pirkle, W. H.; Spence, P. L. J. Chromatogr. A 1997, 775, 81
30. Pirkle, W. H.; Gan, K. Z. J. Chromatogr. A 1997, 790, 65
31. Pirkle, W. H.; Lee, C. J. Enantiomer 1997, 2, 423
32. Welch, C. J.; Szczerba, T.; Perrin, S. R. J. Chromatogr. A 1997, 758, 93
33. Magora, A.; Abu-Lafi, S.; Levin, S. J. Chromatogr. A 2000, 866, 183
34. Kennedy, J. H. J. Chromatogr. A 1996, 725, 219
35. Dungelova, J.; Lehotay, J.; Krupcik, J.; Cizmarik, J.; Armstrong, D. W. J. Sep. Sci. 2004, 27, 983
36. Pirkle, W. H.; Brice, L. J.; Terfloth, G. J. J. Chromatogr. A 1996, 753, 109
37. Oswald, P.; Desmet, K.; Sandra, J.; Krupcik, J.; Majek, P.; Armstrong, D. W. J. Chromatogr. B 2002, 776, 283
38. Kraml, C. M.; Zhou, D. H.; Byrne, N.; McConnel, O. J. Chromatogr. A 2005, 1100, 108
39. Blum, A. M.; Lynam, K. G.; Nicolas, E. C. Chirality 1994, 6, 302
40. Hamper, B. C.; Dukesherer, D. R.; Moedritzer, K. E. C. J. Chromatogr. A 1994, 666, 479
41. Badaloni, E.; Cabri, W.; Ciogli, A.; D'Acquarica, I.; Deias, R.; Gasparrini, F.; Giorgi, F.; Kotoni, D.; Villani, C. J. Chromatogr. A 2010, 1217, 1024
42. Neue, U. D.; El Fallah, M. HPLC Columns: Theory, Technology, and Practice; Wiley-VCH: New York, 1997.
43. Neue, U. D. LC-GC Eur. 2009, 22, 570
44. Desmet, G.; Clicq, D.; Gzil, P. Anal. Chem. 2005, 77, 4058
45. Gritti, F.; Kazakevich, Y.; Guiochon, G. J. Chromatogr. A 2007, 1161, 157
46. Gritti, F.; Kazakevich, Y.; Guiochon, G. J. Chromatogr. A 2007, 1169, 111
47. Al-Bokari, M.; Cherrak, D.; Guiochon, G. J. Chromatogr. A 2002, 975, 275
48. Gritti, F.; Guiochon, G. J. Chromatogr. A 2011, 1218, 907
49. Caccamese, S.; Principato, G.; Chimirr, A.; Grasso, S. Tetrahedron: Asymmetry 1996, 7, 2577
50. Wei, I. C.; Rowley, R. L. J. Chem. Eng. Data 1984, 29, 332
51. Thompson, J. W.; Kaiser, T. J.; Jorgenson, J. W. J. Chromatogr. A 2006, 1134, 201
52. Desmet, G.; Gzil, P.; Clicq, D. LC-GC Eur. 2005, 7, 403
53. Cramers, C. A.; Rijks, J. A.; Schutjes, C. P. M. Chromatographia 1981, 14, 439
54. Martin, M.; Guiochon, G. J. Chromatogr. 1974, 99, 357
55. Dossou, K. S. S.; Farcas, E.; Servais, A. C.; Chiap, P.; Chankvetadze, B.; Crommen, J.; Fillet, M. J. Chromatogr. 2012, 1234, 56