Analysis of steroids in human urine by on line liquid chromatography-gas chromatography-mass spectrometry using the Through Oven Transfer Adsorption Desorption interface and a fraction collector

Analytica Chimica Acta

Volumn 741, Issue , 2012, Pages 78-85

  Toledano, Rosa M ^a   Díaz Plaza, Eva M ^b   Cortés, José M ^a   Blázquez, Inmaculada ^b   Vázquez, Ana ^a   Villén, Jesús ^a   Muñoz Guerra, Jesús ^b  

^a UNIVERSITY OF CASTILLA LA MANCHA   (Spain)

^b Laboratorio de Control de Dopaje   (Spain)

Author keywords

Doping; Human urine; Natural steroids; On line coupled liquid chromatography gas chromatography mass spectrometry; Steroid analysis; Through Oven Transfer Adsorption Desorption interface with fraction collector

Indexed keywords

ADSORPTION DESORPTION; CHROMATOGRAPHY-MASS SPECTROMETRY; HUMAN URINE; NATURAL STEROIDS; STEROID ANALYSIS;

BODY FLUIDS; DOPING (ADDITIVES); GAS CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; OVENS;

LIPIDS;

11 OXOETIOCHOLANOLONE; 5 ALFADIOL; 5 BETADIOL; ANDROSTERONE; EPITESTOSTERONE; ETIOCHOLANOLONE; HYDROXYANDROSTERONE; PREGNANEDIOL; STEROID; TESTOSTERONE; UNCLASSIFIED DRUG;

ANALYTIC METHOD; ARTICLE; AUTOMATION; CONCENTRATION (PARAMETERS); CONTAMINATION; CONTROLLED STUDY; DERIVATIZATION; DOPING; FRACTION COLLECTOR; GAS CHROMATOGRAPHY; HUMAN; LABORATORY DEVICE; LIMIT OF DETECTION; LIQUID CHROMATOGRAPHY; MASS FRAGMENTOGRAPHY; MASS SPECTROMETER; MASS SPECTROMETRY; ONLINE ANALYSIS; PRIORITY JOURNAL; REPRODUCIBILITY; SENSITIVITY ANALYSIS; STEROID ANALYSIS; THROUGH OVEN TRANSFER ADSORPTION DESORPTION; URINALYSIS; VALIDATION PROCESS;

ADSORPTION; ANALYTIC SAMPLE PREPARATION METHODS; CHEMICAL FRACTIONATION; CHROMATOGRAPHY, LIQUID; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; LIMIT OF DETECTION; ONLINE SYSTEMS; REPRODUCIBILITY OF RESULTS; STEROIDS; URINALYSIS;

EID: 84864316286     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2012.06.050     Document Type: Article

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