Optimization of solvent bar microextraction combined with gas chromatography mass spectrometry for preconcentration and determination of tramadol in biological samples

Journal of Chromatography A

Volumn 1251, Issue , 2012, Pages 48-53

  Ghasemi, Ensieh ^a  

^a ISLAMIC AZAD UNIVERSITY   (Iran)

Author keywords

Chemometric design; GC MS; Solvent bar; Tramadol; Two phase liquid microextraction

Indexed keywords

ANALYTICAL METHOD; AQUEOUS SAMPLES; BIOLOGICAL SAMPLES; BOX-BEHNKEN DESIGN; CHEMOMETRICES; DETECTION LIMITS; EXPERIMENTAL PARAMETERS; EXTRACTION EFFICIENCIES; EXTRACTION TIME; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GC-MS; MICROEXTRACTION; ORGANIC PHASE; PLACKETT-BURMAN; POLYPROPYLENE HOLLOW FIBER; PRE-CONCENTRATION; SCREENING DESIGN; SENSITIVE METHOD; SOLVENT BAR MICROEXTRACTION; STIRRING RATES; TRAMADOL;

GAS CHROMATOGRAPHY; IONIC STRENGTH; OPTIMIZATION; POLYPROPYLENES; SOLVENTS;

SOLVENT EXTRACTION;

NONANOL; POLYPROPYLENE; TRAMADOL;

ANALYTIC METHOD; AQUEOUS SOLUTION; ARTICLE; CONCENTRATION (PARAMETERS); DRUG BLOOD LEVEL; DRUG DETERMINATION; DRUG ISOLATION; DRUG URINE LEVEL; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HOLLOW FIBER; HUMAN; INTERMETHOD COMPARISON; LIMIT OF DETECTION; LIQUID LIQUID EXTRACTION; LIQUID PHASE MICROEXTRACTION; MASS SPECTROMETRY; NONHUMAN; PH; PRIORITY JOURNAL; RABBIT; SENSITIVITY ANALYSIS; SOLID PHASE EXTRACTION; SOLID PHASE MICROEXTRACTION; SOLVENT BAR EXTRACTION; SOLVENT EXTRACTION; TEMPERATURE; TIME;

ANIMALS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HAIR; HUMANS; HYDROGEN-ION CONCENTRATION; LIMIT OF DETECTION; LIQUID PHASE MICROEXTRACTION; OSMOLAR CONCENTRATION; RABBITS; REPRODUCIBILITY OF RESULTS; TRAMADOL;

EID: 84864059017     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.06.060     Document Type: Article

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