Screening for pesticide residues in oil seeds using solid-phase dispersion extraction and comprehensive two-dimensional gas chromatography time-of-flight mass spectrometry

Journal of Separation Science

Volumn 35, Issue 13, 2012, Pages 1634-1643

  Wang, Xiupin ^a,b   Li, Peiwu ^a,b   Zhang, Wen ^a,b   Zhang, Qi ^b   Ma, Fei ^b   Yu, Li ^b   Wang, Lin ^b  

^a INSTITUTE OF PLANT PROTECTION   (China)

^b AGRO ENVIRONMENTAL PROTECTION INSTITUTE   (China)

Author keywords

Comprehensive two dimensional gas chromatography time of flight mass spectrometry; Oil absorbing matrix solid phase dispersion extraction; Oilseed Pesticide residues; Screening

Indexed keywords

AMINOPROPYL SILICA; COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY; CONFIRMATORY ANALYSIS; CONTROL DESIGN; FALSE NEGATIVE RATE; FALSE POSITIVE RATES; HEPTACHLOR EPOXIDE; HYDROPHOBIC COMPONENTS; INTERNAL STANDARDS; OIL SAMPLES; ORGANIC CHLORINE; PESTICIDE RESIDUE; RAPE SEED; SCREENING METHODS; SCREENING PERFORMANCE; SOLID PHASE DISPERSION; SPECTRAL DECONVOLUTION; SUNFLOWER SEEDS; SYNTHETIC PYRETHROIDS; TIME OF FLIGHT MASS SPECTROMETRY;

ABSORPTION; CHLORINE; CHROMATOGRAPHY; DISPERSIONS; MASS SPECTROMETRY; MATRIX SOLID PHASE DISPERSION; OILSEEDS; PESTICIDES; QUALITY CONTROL; SCREENING; SILICA; SMOKE DETECTORS;

MASS SPECTROMETERS;

ARACHIS OIL; PESTICIDE; RAPESEED OIL; SESAME SEED OIL; SOYBEAN OIL; SUNFLOWER OIL;

ARTICLE; COMPUTER PROGRAM; FOOD CONTAMINATION; GAS CHROMATOGRAPHY; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; TIME OF FLIGHT MASS SPECTROMETRY; TWO DIMENSIONAL GAS CHROMATOGRAPHY;

ANGIOSPERMS; FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; PESTICIDE RESIDUES; SEEDS; SOLID PHASE EXTRACTION;

ARACHIS HYPOGAEA; GLYCINE MAX; HELIANTHUS; SESAMUM INDICUM;

EID: 84863696801     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201100863     Document Type: Article

References (29)

1. Matthäus, B., Brühl, L., Food/Nahrung 2003, 47, 413-419.
2. Filek, G., Lindner, W., Z. Lebensm. Unters. Forsch. 1996, 202, 19-23.
3. FDA Compliance Policy Guides (CPG Sec.575.100.), Pesticide residues in food and feed-enforcement criteria, US Food & Drug Administration, Silver Spring, MD 2002.
4. Regulation of the European Parliament and of the Council (EC NO 396/2005), on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC, Off. J. Eur. Union 2005, L70, 1-16.
5. China National Standard (GB 2763-2005), Maximum residue limits for pesticides in food, Chemical Inspection & Regulation Service (CRS) China, Hangzhou, China 2005.
6. China National Standard (GB 26130-2010), Maximum residue limits for 54 pesticides in food, Chemical Inspection & Regulation Service (CRS) China, Hangzhou, China 2011.
7. China Agricultural Industry Standard (NY 1500.38.2-2008), Maximum residue limits for twenty pesticides in vegetables and fruits, 30 April 2008 (in Chinese).
8. China Agricultural Industry Standard (NY 1500.36.2-2008), Maximum residue limits for twenty pesticides in vegetables and fruits, 30 April 2008 (in Chinese).
9. China National Standard (GB 16333-1996), Maximum residue limits of amitraz and other pesticides in food, Chemical Inspection & Regulation Service (CRS) China, Hangzhou, China 2011.
10. Hoh, E., Lehotay, S. J., Mastovska, K., Huwe, J. K., J. Chromatogr. A 2008, 1201, 69-77.
11. Hoh, E., Lehotay, S. J., Mastovska, K., Ngo, H. L., Vetter, W., Pangallo, K. C., Reddy, C. M., Environ. Sci. Technol. 2009, 43, 3240-3247.
12. Glaser, T., Lienau, A., Zeeb, D., Krucker, M., Dachtler, M., Albert, K., Chromatographia 2003, 57, S19-S25.
13. Sobhanzadeh, E., Abu Bakar, N. K., Bin Abas, M. R., Nemati, K., J. Hazard. Mater. 2011, 186, 1308-1313.
14. Gilbert-López, B., García-Reyes, J. F., Molina-Díaz, A., Talanta 2009, 79, 109-128.
15. Ferrer, C., Jose Gómez, M., García-Reyes, J. F., Ferrer, I., Michael Thurman, E., Fernández-Alba, A. R., J. Chromatogr. A 2005, 1069, 183-194.
16. Čajka, T., Maštovská, K., Lehotay, S. J., Hajšlová, J., J. Sep. Sci. 2005, 28, 1048-1060.
17. Phillips, J. B., Beens, J., J. Chromatogr. A 1999, 856, 331-347.
18. Cochran, J., J. Chromatogr. A 2008, 1186, 202-210.
19. Patel, K., Fussell, R. J., Hetmanski, M., Goodall, D. M., Keely, B. J., J. Chromatogr. A 2005, 1068, 289-296.
20. van der Lee, M. K., van der Weg, G., Traag, W. A., Mol, H. G. J., J. Chromatogr. A 2008, 1186, 325-339.
21. Schurek, J., Portolés, T., Hajslova, J., Riddellova, K., Hernández, F., Anal. Chim. Acta 2008, 611, 163-172.
22. Zrostlíková, J., Hajšlová, J., Čajka, T., J. Chromatogr. A 2003, 1019, 173-186.
23. Dallüge, J., van Rijn, M., Beens, J., Vreuls, R. J. J., Brinkman, U. A. T., J. Chromatogr. A 2002, 965, 207-217.
24. Commission Decision (2002/657/EC) of 12 August 2002, implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results, Vol. OJL221, European Commission, Brussels, Belgium 2002, pp. 8-36.
25. Gilbert-López, B., García-Reyes, J. F., Fernández-Alba, A. R., Molina-Díaz, A., J. Chromatogr. A 2010, 1217, 3736-3747.
26. Khummueng, W., Trenerry, C., Rose, G., Marriott, P. J., J. Chromatogr. A 2006, 1131, 203-214.
27. Hoggard, J. C., Wahl, J. H., Synovec, R. E., Mong, G. M., Fraga, C. G., Anal. Chem. 2010, 82, 689-698.
28. Document No. SANCO/10684/2009, Method validation and quality control procedures for pesticide residues analysis in food and feed, EU Reference Laboratories for Residues of Pesticides, DG Sanco, Brussels, Belgium 2009.
29. Soboleva, E., Ahad, K., Ambrus, Á,., Analyst 2004, 129, 1123-1129