Combined Crystallization and Drying in a Pilot-Scale Spray Dryer

Drying Technology

Volumn 30, Issue 9, 2012, Pages 998-1007

  Das, Debolina ^a   Langrish, Timothy A G ^a  

^a UNIVERSITY OF SYDNEY   (Australia)

Author keywords

Dairy products; Food processing; One step crystallization; Particle technology; Product design; Product engineering; Reaction engineering; Sorption; Spray drying; Sprays; Stickiness

Indexed keywords

ONE-STEP CRYSTALLIZATION; PARTICLE TECHNOLOGY; PRODUCT ENGINEERING; REACTION ENGINEERING; SPRAYS; STICKINESS;

AIR; DAIRY PRODUCTS; DIFFERENTIAL SCANNING CALORIMETRY; FLOW RATE; FOOD PROCESSING; MOISTURE DETERMINATION; POWDERS; PRODUCT DESIGN; SORPTION; SPRAY DRYING; SUGARS; THERMAL LOAD;

DRYERS (EQUIPMENT);

EID: 84861954794     PISSN: 07373937     EISSN: 15322300     Source Type: Journal    
DOI: 10.1080/07373937.2012.678529     Document Type: Article

References (42)

1. Bhandari, B.R.; Howes, T. Implication of glass transition for the drying and stability of dried foods. Journal of Food Engineering 1998, 40 (1), 71-79.
2. Masters, K. Spray Drying an Introduction to Principles, Operational Practice and Applications; Leonard Hill Books: London, 1972.
3. Ozmen, L.; Langrish, T.A.G. Comparison of glass transition temperature and stick point temperature for skim milk powder. Drying Technology 2002, 20 (6), 1177-1192.
4. White, G.W.; Cakebread, S.H. The glassy state in certain sugar containing food products. International Journal of Food Science and Technology 1966, 1 (1), 73-82.
5. Bhandari, B.R.; Datta, N.; Howes, T. Problems associated with spray drying of sugar-rich foods. Drying Technology 1997, 15 (2), 671-684.
6. Buckton, G.; Darcy, P.Assessment of disorder in crystalline powders-A review of analytical techniques and their application. International Journal of Pharmaceutics1999, 179(2), 141-158.
7. Jouppila, K.; Kansikas, J.; Roos, Y.H. Glass transition, water plasticization, and lactose crystallization in skim milk powder. Journal of Dairy Sciences 1997, 80 (12), 3152-3160.
8. Jouppila, K.; Roos, Y.H. Glass transitions and crystallization in milk powders. Journal of Dairy Sciences 1994, 77 (10), 2907-2915.
9. Chiou, D.; Langrish, T.A.G.; Braham, R. Partial crystallization behaviour during spray drying: simulations and experiments. Drying Technology 2008, 26 (1), 27-38.
10. Langrish, T.A.G.; Wang, S. Crystallization rates for amorphous sucrose and lactose powders from spray drying: A comparison. Drying Technology 2009, 27 (4), 606-614.
11. Anderson, G. The Anhydro Paradry process. In The Importance of Whey and Whey Components in Food and Nutrition (Proceedings of the International Whey Conference); B. Behr's Verlag: Munich, Germany, 2001; 1-411.
12. Písecký, J. Spray drying in the cheese industry. International Dairy Journal 2005, 15 (6-9), 531-536.
13. Schuck, P.; Dolivet, A. Lactose crystallization: Determination of a-lactose monohydrate in spray-dried dairy products. Lait 2002, 82 (4), 413-421.
14. Chiou, D.; Langrish, T.A.G. Crystallization of amorphous components in spray-dried powders. Drying Technology 2007, 25 (9), 1427-1435.
15. Chiou, D.; Langrish, T.A.G.; Braham, R. The effect of temperature on the crystallinity of lactose powders produced by spray drying. Journal of Food Engineering 2008, 86 (2), 288-293.
16. Haque, M.K.; Roos, Y.H. Crystallization and X-ray diffraction of spray dried and freeze-dried amorphous lactose. Carbohydrate Research 2004, 340 (2), 293-301.
17. Islam, M.I.U.; Langrish, T.A.G. Comparing the crystallization of sucrose and lactose in spray dryers. Food and Bioproducts Processing 2009, 87 (2), 87-95.
18. Roos, Y.H.; Karel, M. Differential scanning calorimetry study of phase transitions affecting the quality of dehydrated materials. Biotechnology Progress 1990, 6 (2), 159-163.
19. Roos, Y.H.; Karel, M. Plasticizing effect of water on thermal behaviour and crystallization of amorphous food models. Journal of Food Science 1991, 56 (1), 38-43.
20. Roos, Y.H.; Karel, M. Crystallization of amorphous lactose. Journal of Food Science 1992, 57 (3), 775-777.
21. Oakley, D.E. Scale-up of spray dryers with the aid of computational fluid dynamics. Drying Technology 1994, 12 (1), 217-233.
22. Kieviet, F.; Kerkhof, P.J.A.M. Measurements of particle residence time distributions in a co-current spray dryer. Drying Technology 1995, 13 (5-7), 1241-1248.
23. Thybo, P.; Hovgaard, L.; Lindelov, J.S.; Brask, A.; Andersen, S.K. Scaling up the spray drying process from pilot to production scale using an atomized droplet size criterion. Pharmaceutical Research 2008, 25 (7), 1610-1620.
24. Kota, K.; Langrish, T.A.G. Prediction of deposition patterns in a pilot-scale spray dryer using computational fluid dynamics (CFD) simulations. Chemical Product and Process Modeling 2007, 3 (2), Art. 26.
25. Southwell, D.B.; Langrish, T.A.G. The effect of swirl on flow stability in spray dryers. Chemical Engineering Research and Design 2001, 79 (3), 222-234.
26. Southwell, D.B. Operability and performance assessment of spray dryers. Ph.D. Thesis, Department of Chemical Engineering, University of Sydney, Sydney, Australia, 2000.
27. Langrish, T.A.G.; Chan, W.C.; Kota, K. Comparison of maltodextrin and skim milk wall deposition rates in a pilot-scale spray dryer. Powder Technology 2007, 179 (1-2), 84-89.
28. Ozmen, L.; Langrish, T.A.G. An experimental investigation of the wall deposition of milk powder in a pilot-scale spray dryer. Drying Technology 2003, 21 (7), 1253-1272.
29. Maa, Y.F.; Costantino, H.R.; Nguyen, P.A.; Hsu, C.C. The effect of operating and formulation variables on the morphology of spray-dried protein particles. Pharmaceutical Development and Technology 1997, 2 (3), 213-223.
30. Prinn, K.B.; Costantino, H.R.; Tracy, M. Statistical modeling of protein spray drying at the lab scale. AAPS PharmSciTech 2002, 3 (1), 1-8.
31. Ibach, A.; Kind, M. Crystallization kinetics of amorphous lactose, whey permeate and whey powders. Carbohydrate Research 2007, 342 (10), 1357-1365.
32. Bronlund, J.; Paterson, T. Moisture sorption isotherms for crystalline, amorphous and predominantly crystalline lactose powders. International Dairy Journal 2004, 14 (3), 247-254.
33. Hill, V.L.; Craig, D.Q.M.; Freely, L.C. Characterisation of spray-dried lactose using modulated differential scanning calorimetry. International Journal of Pharmaceutics 1998, 161 (1), 95-107.
34. Lehto, V.P.; Tenho, M.; Vähä-Heikkilä, K.; Harjunen, P.; Päällysaho, M.; Välisaari, J.; Niemelä, P.; Järvinen, K. The comparison of seven different methods to quantify the amorphous content of spray dried lactose. Powder Technology 2006, 167 (2), 85-93.
35. Wang, S.; Langrish, T.A.G. Measurements of the crystallization rates of amorphous sucrose and lactose powders from spray drying. International Journal of Food Engineering 2007, 3 (4), 1-17.
36. Williams, M.L.; Landel, R.F.; Ferry, J.D. The temperature dependence of relaxation mechanisms in amorphous polymers and other glass-forming liquids. Journal of the American Chemical Society 1955, 77 (14), 3701-3707.
37. Islam, M.I.U.; Langrish, T.A.G. An investigation into lactose crystallization under high temperature conditions during spray drying. Food Research International 2010, 43 (1), 46-56.
38. Lefort, R.; Caron, V.; Willart, J.F.; Descamps, M. Mutarotational kinetics and glass transition of lactose. Solid State Communications 2006, 140 (7-8), 329-334.
39. Gombás, A.; Szabó-Révész, P.; Kata, M.; Regdon, G. Jr.; Erõs, I. Quantitative determination of crystallinity of α -lactose monohydrate by DSC. Journal of Thermal Analysis and Calorimetry 2002, 68 (2), 503-510.
40. Kent, J.; McLeod, J. Spray-Dryer Optimization. http://www.niroinc.com/html/chemical/cpdfs/spray_dryer_optimization.pdf (accessed August 12, 2010).
41. Islam, M.I.U.; Langrish, T.A.G.; Chiou, D. Particle crystallization during spray drying in humid air. Journal of Food Engineering 2010, 99 (1), 55-62.
42. Lamy, T.; Collins, N.; Langrish, T.A.G. The use of water deposition to study the main factors in wall collisions of droplets in a pharmaceutical-scale spray dryer. Atomisation and Sprays 2008, 18 (6), 523-551.