The detection of nicotine in a Late Mayan period flask by gas chromatography and liquid chromatography mass spectrometry methods

Rapid Communications in Mass Spectrometry

Volumn 26, Issue 4, 2012, Pages 403-411

  Zagorevski, Dmitri V ^a   Loughmiller Newman, Jennifer A ^b  

^a RENSSELAER POLYTECHNIC INSTITUTE   (United States)

^b STATE UNIVERSITY OF NEW YORK   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

BOTTLES; GAS CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; TOBACCO;

GASCHROMATOGRAPHY-MASS SPECTROMETRY; HIGH MASS ACCURACIES; HIGH RESOLUTION; LIBRARY OF CONGRESS; LIQUID CHROMATOGRAPHY - MASS SPECTROMETRIES; LITERATURE DATA; MASS SPECTRAL; MASS SPECTROMETRY ANALYSIS; SPECTRAL CHARACTERISTICS; TANDEM-MASS SPECTROMETRY;

NICOTINE;

EID: 84856273819     PISSN: 09514198     EISSN: 10970231     Source Type: Journal    
DOI: 10.1002/rcm.5339     Document Type: Article

References (33)

1. W.J. Hurst, S.M. Tarka Jr, T.G. Powis, F. Valdez Jr, T.R. Hester,. Cacao usage by the earliest Maya civilization. Nature 2002, 418, 289.
2. W.J. Hurst, R.A. Martin, S.M. Tarka Jr, G.D. Hall,. Authentication of cocoa in Maya vessels using high-performance liquid chromatography techniques. J. Chromatogr. 1989, 466, 279.
3. Organic Mass Spectrometry in Art and Archaeology, (Eds:, M.P. Colombini, F. Modugno,), John Wiley, Chichester, 2009.
4. Theory and Practice of Archaeological Residue Analysis, British Archaeological Reports International Series 1650, (Eds:, H. Barnard, J.W. Eerkens,). Archaeopress, Oxford, 2007.
5. P. Jacob III, G.D. Byrd,. Use of chromatographic and mass spectrometric techniques for the determination of nicotine and its metabolites, in Analytical Determination of Nicotine and Related Compounds and Their Metabolites, (Eds:, J.W. Gorrod, P. Jacob III,). Elsevier, Amsterdam, 1999, pp. 191-224.
6. P.A. Crooks, G.D. Byrd,. Use of high-performance liquid chromatographic-mass spectrometric (LC-MS) techniques for the determination of nicotine and its metabolites, in Analytical Determination of Nicotine and Related Compounds and Their Metabolites, (Eds:, J.W. Gorrod, P. Jacob III,). Elsevier, Amsterdam, 1999, pp. 225-264.
7. D.A. Leyden, E. Leitner, B. Siegmund,. Determination of nicotine in pharmaceutical products and dietary sources, in Analytical Determination of Nicotine and Related Compounds and Their Metabolites, (Eds:, J.W. Gorrod, P. Jacob III,). Elsevier, Amsterdam, 1999, pp. 393-420.
8. H. Wischmann, S. Hummel, M.A. Rothschild, B. Herrmann,. Analysis of nicotine in archaeological skeletons from the Early Modern Age and from the Bronze Age. Anc. Biomol. 2002, 4, 47.
9. S.M. Rafferty,. Identification of nicotine by gas chromatography/mass spectroscopy analysis of smoking pipe residue. J. Archaeol. Sci. 2002, 29, 897.
10. NIST/EPA/NIH Mass Spectral Library (2008 Edition).
11. T.P. Moyer, J.R. Charlson, R.J. Enger, L.C. Dale, J.O. Ebbert, D.R. Schroeder, R.D. Hurt,. Simultaneous analysis of nicotine, nicotine metabolites, and tobacco alkaloids in serum or urine by tandem mass spectrometry, with clinically relevant metabolic profiles. Clin. Chem. 2002, 48, 1460.
12. D.W. Armstrong, X. Wang, N. Ercal,. Enantiomeric composition of nicotine in smokeless tobacco, medicinal products, and commercial reagents. Chirality 1998, 10, 587.
13. M. Pelegrini, E. Marchei, S. Rossi, F. Vagnarelli, A. Durgbanshi, O. Garcia-Algar, O. Vall, S. Pichini,. Liquid chromatography/electrospray ionization tandem mass spectrometry assay for determination of nicotine and metabolites, caffeine and arecoline in breast milk. Rapid Commun. Mass Spectrom. 2007, 21, 2693.
14. T.J. Smyth, V.N. Ramachandran, A. McGuigan, J. Hopps, W.F. Smyth,. Characterisation of nicotine and related compounds using electrospray ionization with ion trap mass spectrometry and with quadrupole time-of-flight mass spectrometry and their detection by liquid chromatography/electrospray ionization mass spectrometry. Rapid Commun. Mass Spectrom. 2007, 21, 557.
15. E.I. Miller, H.-R.K. Norris, D.E. Rollins, S.T. Tiffany, D.G. Wilkins,. A novel validated procedure for the determination of nicotine, eight nicotine metabolites and two minor tobacco alkaloids in human plasma or urine by solid-phase extraction coupled with liquid chromatography-electrospray ionization-tandem mass spectrometry. J. Chromatogr. B 2010, 878, 725.
16. Z. Fan, F. Xie, Q. Xia, S. Wang, L. Ding, H. Liu,. Simultaneous determination of nicotine and its metabolites in human urine by LC-MS-MS. Chromatographia 2008, 68, 623.
17. A.C. Sanchez, M.M. Kansal, A. Dixon, P.J. Koerner, T. Matthews,. Increased sample throughput with Luna® HILIC, Application Note TN-1038. Phenomenex, Torrance, CA.
18. L. Wang, X. Liu, D. Chatfield, W. Schnute,. Simultaneous determination of nicotine and metabolites by LC-MS using an Acclaim mixed-mode HILIC-1 column, LC GC North America 2008, Feb, 56.
19. 2]-cotinine by capillary liquid chromatography-electrospray mass spectrometry. J. Chromatogr. B 2007, 857, 1.
20. Y. Iwasaki, M. Goto, K. Mochizuki, E. Terayama, R. Ito, K. Saito, N. Sugino, T. Makino, H. Nakasawa,. Development and validation of a hydrophilic interaction chromatography-tandem mass spectrometry for quantification of nicotine and its metabolites in human maternal and cord sera. Biomed. Chromatogr. 2011, 25, 503.
21. F. Marclay, M. Saugy,. Determination of nicotine and nicotine metabolites in urine by hydrophilic interaction chromatography-mass spectrometry: potential use of smokeless tobacco products by ice hockey players. J. Chrom. A 2010, 1217, 7528.
22. T. Tuomi, T. Johnsson, K. Reijula,. Analysis of nicotine, 3-hydroxycotinine, cotinine, and caffeine in urine of passive smokers by HPLC-tandem mass spectrometry. Clin. Chem. 1999, 45, 2164.
23. B. Yue, M.M. Kushnir, F.M. Urry, A.L. Rockwood,. Quantitation of nicotine, its metabolites, and other related alkaloids in urine, serum, and plasma using LC-MS-MS. Meth. Mol. Biol. 2010, 603, 389.
24. J. Beyer, F.T. Peters, T. Kraemer, H.H. Maurer,. Detection and validated quantification of toxic alkaloids in human blood plasma - comparison of LC-APCI-MS with LC-ESI-MS/MS. J. Mass Spectrom. 2007, 42, 621.
25. S. Balabanova, F. Parsche, W. Pirsig,. First identification of drugs in Egyptian mummies. Naturwissenschaften 1992, 79, 358.
26. S.A. Wells,. American drugs in Egyptian mummies: a review of the evidence. Available
27. B. Liu, W. Yao, Q. Su,. Racemization of S-(-)-nicotine during smoking and its relationship with pyrolysis process. J. Anal. Appl. Pyrolysis 2008, 81, 157.
28. P. Clayton, A. Lu, L. Bishop,. The pyrolysis of (-)-(S)-nicotine: racemization and decomposition. Chirality 2010, 22, 442.
29. K. Groark,. Angel in the Gourd: social, therapeutic, and ritual uses of tobacco (Nicotiana tabacum) among the Tzeltal and Tzotzil Maya of Chiapas, Mexico. J. Ethnobiol. 2010, 30, 5.
30. D. Stuart,. The Inscriptions from Temple XIX at Palenque. The Pre-Columbian Art Research Institute, San Francisco, 2005.
31. E. Boot,. Otot as a Vessel Classification for a Footed Bowl: Short Epigraphic Note on a Bowl in the Collection of the Museum of Fine Arts, Boston, 2009. Available:.
32. (a), J. Carlson,. Tobacco in enema? In Maya flasks and Miniature vessels. Aztlan listserve posting on FAMSI website, July 8, 2007. Available:;
33. (b) J. Carlson. Entries 16-19, 118 in The Jay I Kislak Collection at the Library of Congress: A Catalog of the Gift of the Jay I Kislak Foundation at the Library of Congress. 9p. 11-13. 42. Edited by Arthur Dunkelman. Library of Congress.