Development of GC-MS/MS method with programmable temperature vaporization large volume injection for monitoring of 17β-estradiol and 2-methoxyestradiol in plasma

Analytica Chimica Acta

Volumn 709, Issue , 2012, Pages 73-80

  Tsakalof, A K ^a   Gkagtzis, D C ^a   Koukoulis, G N ^b   Hadjichristodoulou, C S ^a  

^a UNIVERSITY OF THESSALY   (Greece)

^b UNIVERSITY HOSPITAL OF LARISSA   (Greece)

Author keywords

17 Estradiol; 2 Methoxyestradiol; GC MS MS; Pre eclampsia; Steroids

Indexed keywords

2-METHOXYESTRADIOL; BIOLOGICAL SAMPLES; CONCENTRATION LEVELS; CONCENTRATION RANGES; DERIVATIZATIONS; DIAGNOSTIC MARKERS; ENDOCRINE DISEASE; GC-MS/MS; ION FRAGMENTATION; ION SCAN; ION TRAPS; LARGE VOLUME INJECTION; LIMIT OF DETECTION; MASS SPECTRA; MOLECULAR IONS; PLASMA CONCENTRATION; PLASMA SAMPLES; PRE-ECLAMPSIA; PRECURSOR IONS; PROGRAMMED TEMPERATURE; PROTEIN PRECIPITATION; SOLID-PHASE EXTRACTION; STEROIDS; TRIFLUOROACETIC ANHYDRIDES;

DIAGNOSIS; ION SOURCES; LIPIDS; MASS SPECTROMETRY; METABOLISM; METABOLITES; OPTIMIZATION; PLASMAS; QUALITY CONTROL; VAPORIZATION;

IONS;

2 METHOXYESTRADIOL; ESTRADIOL; TRIFLUOROACETIC ANHYDRIDE;

ACCURACY; ARTICLE; CONTROLLED STUDY; DERIVATIZATION; GAS FLOW; ION TRAP MASS SPECTROMETRY; LIMIT OF DETECTION; MASS FRAGMENTOGRAPHY; PRECIPITATION; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; PRODUCT RECOVERY; QUANTITATIVE ANALYSIS; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; STEROID ANALYSIS; VAPORIZATION;

ESTRADIOL; FEMALE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; PRE-ECLAMPSIA; PREGNANCY; SOLID PHASE EXTRACTION; TEMPERATURE; VOLATILIZATION;

EID: 84155163834     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2011.09.043     Document Type: Article

References (37)

1. Nozaki O. J. Chromatogr. A 2001, 935:267.
2. Cahill D.J., Wardle P.G., Harlow C.R., Hunt L.P., Hull M.G. Hum. Reprod. 2000, 15:1909.
3. Katayama M., Takamatsu K., Kaneko S., Miyaji K., Ishikawa H., Matsuda Y. J. Sep. Sci. 2007, 30:2279.
4. Kanasaki K., Palmsten K., Sugimoto H., Ahmad S., Hamano Y., Xie L., Parry S., Augustin H.G., Gattone V.H., Folkman J., Strauss J.F., Kalluri R. Nature 2008, 453:1117.
5. Hertig A., Liere P., Chabbert-Buffet N., Fort J., Pianos A., Eychenne B., Cambourg A., Schumacher M., Berkane N., Lefevre G., Uzan S., Rondeau E., Rozenberg P., Rafestin-Oblin M.-E. Am. J. Obstetrics Gynecol. 2010, 203:477e1.
6. Hertig A., Liere P. Clin. Chim. Acta 2010, 411:1591.
7. Sibai B., Dekker G., Kupferminc M. Lancet 2005, 365:785.
8. Blair I.A. Steroids 2010, 75:297.
9. Santen R.J., Demers L., Ohorodnik S., Settlage J., Langecker P., Blanchett D., Goss P.E., Wang S. Steroids 2007, 72:666.
10. Giese R.W. J. Chromatogr. A 2003, 1000:401.
11. Shimada K., Mitamura K., Higashi T. J. Chromatogr. A 2001, 935:141.
12. Mueck A.O., Seeger H. Steroids 2010, 75:625.
13. Lakhani N.J., Lepper E.R., Sparreboom A., Dahut W.L., Venitz J., Figg W.D. Rapid Commun. Mass Spectrom. 2005, 19:1176.
14. Adlercreutz H., Kiuru P., Rasku S., Wähälä K., Fotsis T. J. Steroid Biochem. Mol. Biol. 2004, 92:399.
15. Zacharia L.C., Dubey R.K., Jackson E.K. Steroids 2004, 69:255.
16. Ha Y.W., Moon J.Y., Jung H.J., Chung B.C., Choi M.H. J. Chromatogr. B: Anal. Technol. Biomed. Life Sci. 2009, 877:4125.
17. Hübschmann H.-J. Handbook of GC/MS Fundamentals and Applications 2008, Wiley-VCH, Weinheim.
18. AbuRuz S., Millership J., Heaney L., McElnay J. J. Chromatogr. B: Anal. Technol. Biomed. Life Sci. 2003, 798:193.
19. Bianchi F., Careri M., Mangia A., Musci M., Santini S.E., Basini G. J. Pharm. Biomed. Anal. 2007, 44:711.
20. Viswanathan C., Bansal S., Booth B., DeStefano A., Rose M., Sailstad J., Shah V., Skelly J., Swann P., Weiner R. Pharm. Res. 2007, 24:1962.
21. Bansal S., DeStefano A. AAPS J. 2007, 9.
22. Analytical Methods Validation for Human Studies, US Department of Health and Human Services Food and Drug Administration, 1998.
23. Boyd C.B.R., Bethem R. Trace Quantitative Analysis by Mass Spectrometry 2008, John Wiley & Sons Ltd., Chichester, West Sussex PO19 8SQ, England.
24. Black D.M., Payne A.H., Glish G.L. J. Am. Soc. Mass Spectrom. 2006, 17:932.
25. March R.E. Int. J. Mass Spectrom. 2000, 200:285.
26. March R.E. J. Mass Spectrom. 1997, 32:351.
27. Blanchard J. J. Chromatogr. 1981, 226:455.
28. Chambers E., Wagrowski-Diehl D.M., Lu Z., Mazzeo J.R. J. Chromatogr. B: Anal. Technol. Biomed. Life Sci. 2007, 852:22.
29. Practical Aspects of Ion Trap Mass Spectrometry, Volume III: Chemical, Environmental, and Biomedical Applications 1995, CRS Press. J.F.J.T. Raymond, E. March (Eds.).
30. Gordon R.F.A. The Chemist's Companion 1972, John Wiley and sons.
31. Knapp D.R. Handbook of Analytical Derivatization Reactions 1979, John Wiley & Sons, New York.
32. Matuszewski B.K., Constanzer M.L., Chavez-Eng C.M. Anal. Chem. 2003, 75:3019.
33. Swartz M., Ian D.W. Encyclopedia of Separation Science 2007, Academic Press, Oxford, p1.
34. Lof M., Hilakivi-Clarke L., Sandin S.S., de Assis S., Yu W., Weiderpass E. BMC Womens Health 2009, 9:10.
35. Barnes C.M., McElrath T.F., Folkman J., Hansen A.R. Pediatr. Res. 2010, 67:545.
36. Butler J.C., Quarmby S.T., Ragsdale J.D., Conoley M. Proceedings 50th ASMS Conference on Mass Spectrometry and Allied Topics 2002, p625.
37. Liere P., Akwa Y., Weill-Engerer S., Eychenne B., Pianos A., Robel P., Sjovall J., Schumacher M., Baulieu E.E. J. Chromatogr. B: Biomed. Sci. Appl. 2000, 739:301.