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An almost 1:1 mixture of RAlCl2 and R2AlCl is obtained as shown by NMR spectroscopy (see Supporting Information)
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An almost 1:1 mixture of RAlCl2 and R2AlCl is obtained as shown by NMR spectroscopy (see Supporting Information).
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84055209339
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The yield was determined by iodolysis of reaction aliquots and subsequentGC analysis. The use of LiCl leads to dimerization in almost quantitative yield
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The yield was determined by iodolysis of reaction aliquots and subsequentGC analysis. The use of LiCl leads to dimerization in almost quantitative yield.
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84055214398
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In the absence of stoichiometric amounts of Zn(OAc)2 almost no cross-coupling was observed. Both the acetate anion and the zinc cation seem to be important.Wespeculate that the acetate anion is reducing the Lewis acidity of the aluminum species whereas the zinc cation favors the transfer of the aryl group to palladium
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In the absence of stoichiometric amounts of Zn(OAc)2 almost no cross-coupling was observed. Both the acetate anion and the zinc cation seem to be important.Wespeculate that the acetate anion is reducing the Lewis acidity of the aluminum species whereas the zinc cation favors the transfer of the aryl group to palladium.
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Wetried a number of metals in this reaction (Mg, Zn, In, and Al) under the same reaction conditions, and the best results were observed with Al, InCl3, and ZnCl2.
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