Stereoselective liquid chromatographic determination of 1 -oxobufuralol and 1 -hydroxybufuralol in rat liver microsomal fraction using hollow-fiber liquid-phase microextraction for sample preparation

Journal of Separation Science

Volumn 34, Issue 24, 2011, Pages 3578-3586

  Barth, Thiago ^a   Simões, Rodrigo A ^a   Pupo, Mônica T ^a   Okano, Laura T ^a   Bonato, Pierina S ^a  

^a UNIVERSITY OF SÃO PAULO   (Brazil)

Author keywords

Bufuralol metabolites; Enantioseparation; Hollow fiber liquid phase microextraction; Microsomal fraction

Indexed keywords

ACCEPTOR PHASE; ANALYTES; CHIRALCEL OD-H; CHROMATOGRAPHIC DETERMINATION; CONCENTRATION RANGES; DIETHYLAMINES; ENANTIOSEPARATION; EXTRACTION PROCEDURE; HOLLOW FIBER; HPLC ANALYSIS; IN-VITRO; LIQUID PHASE MICROEXTRACTION; MICROSOMAL FRACTION; MICROSOMAL PREPARATIONS; MOBILE PHASE; N-OCTANOL; OPTIMIZED CONDITIONS; QUANTIFICATION LIMIT; RAT LIVERS; RECOVERY RATE; SAMPLE PREPARATION; STEREO-SELECTIVE; UV DETECTION; VALIDATED METHODS;

ACETIC ACID; LIQUID CHROMATOGRAPHY; LIQUIDS; METABOLISM; METABOLITES; ORGANIC SOLVENTS; RATS; STEREOSELECTIVITY;

SOLVENT EXTRACTION;

1' HYDROXYBUFURALOL; 1' OXOBUFURALOL; 2 PROPANOL; ACETIC ACID; BUFURALOL; DIETHYLAMINE; HEXANE; METHANOL; OCTANOL; ORGANIC SOLVENT; UNCLASSIFIED DRUG;

ARTICLE; DRUG DETERMINATION; DRUG TRANSFORMATION; ENANTIOMER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HOLLOW FIBER; IN VITRO STUDY; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; LIQUID PHASE MICROEXTRACTION; LIVER MICROSOME; NONHUMAN; PH; PRIORITY JOURNAL; RAT; STEREOCHEMISTRY; STEREOISOMERISM; ULTRAVIOLET RADIATION; VALIDATION PROCESS;

ANALYTIC SAMPLE PREPARATION METHODS; ANIMALS; CHROMATOGRAPHY, LIQUID; ETHANOLAMINES; LIQUID PHASE MICROEXTRACTION; MALE; MICROSOMES, LIVER; RATS; RATS, WISTAR; STEREOISOMERISM;

EID: 83455223423     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201100464     Document Type: Article

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