Performance and matrix effect observed in QuEChERS extraction and tandem mass spectrometry analyses of pesticide residues in different target crops

Journal of Chromatographic Science

Volumn 49, Issue 9, 2011, Pages 709-714

  Lucini, Luigi ^a   Molinari, Gian Pietro ^a  

^a UNIVERSITÀ CATTOLICA DEL SACRO CUORE   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

CUCUMIS; FRAGARIA X ANANASSA; LYCOPERSICON ESCULENTUM; MALUS X DOMESTICA; PRUNUS PERSICA;

EID: 80755168848     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chrsci/49.9.709     Document Type: Article

References (31)

1. B.K. Matuszewski, M.L. Constanzer, and C.M. Chavezeng. Matrix effect in quantitative LC-MS-MS analyses of biological fluids: A method for determination of finasteride in human plasma at picogram per millilitre concentrations. Anal. Chem. 70: 882-889 (1998).
2. B.K. Matuszewski, M.L. Constanzer, and C.M. Chavezeng. Strategies for the assessment of matrix effect in quantitative bioanalytical methods based on HPLCMS/ MS. Anal. Chem. 75: 3019-3030 (2003). (Pubitemid 36830428)
3. S.D. Clarke, H.M. Hill, T.A.G. Noctor, and D. Thomas. Matrix-related modification of ionization in bioanalytical liquid chromatography-atmospheric pressure ionization tandem mass spectrometry. Pharm. Sci. 2: 203-207 (1996). (Pubitemid 28121808)
4. K. Bester, G. Bordin, A. Rodriguez, H. Schimmel, J. Pauwels, and G. Vanvyncht. How to overcome matrix effects in the determination of pesticides in fruit by HPLC-ESI-MS-MS. Fresenius' J Anal Chem 371: 550-555 (2001).
5. C. Fierens, L.M. Thienpont, D. Stoeckl, and A.P. Deleenheer. Matrix effect in the quantitative analysis of urinary C-peptide by liquid chromatography tandem MS spectrometry. Rapid Commun. Mass Sp. 14: 936-937 (2000). (Pubitemid 30367586)
6. A. Kruve, A. Kunnapas, K. Herodes, and I. Leito. Matrix effects in pesticide multiresidue analysis by liquid chromatography-mass spectrometry. J. Chromatogr. A 1187: 58-66 (2008).
7. R. King, R. Bonfiglio, C. Fernandez-Metzler, C. Miller-Stein, and T. Olah. Mechanistic investigation of ionization suppression in electrospray ionization. J. Am. Soc. Mass. Spectrom. 11: 942-950 (2000). (Pubitemid 34546664)
8. N.B. Cech and C.G. Enke. Relating electrospray ionization response to nonpolar character of small peptides. Anal. Chem. 72: 2717-2723 (2000). (Pubitemid 30452234)
9. P.J. Taylor. Matrix effects: The Achilles heel of quantitative high-performance liquid chromatography-electrospray-tandem mass spectrometry. Clin. Biochem. 38: 328-334 (2005). (Pubitemid 40342863)
10. E.M. Thurman, I. Ferrer, and D. Barcelo. Choosing between Atmospheric Pressure Chemical Ionization and Electrospray Ionization interfaces for the HPLC/MS analysis of pesticides. Anal. Chem. 73: 5441-5449 (2001). (Pubitemid 33108553)
11. A. Kloepfer, J.B. Quintana, and T.J. Reemtsma. Operational options to reduce matrix effects in liquid chromatography-electrospray ionization-mass spectrometry analysis of aqueous environmental samples. J. Chromatogr. A 1067: 153-160 (2005). (Pubitemid 40363400)
12. S.C. Cunha, S.J. Lehotay, K. Mastovska, J.O. Fernandes, and B.M. Oliveira. Evaluation of the QuEChERS sample preparation approach for the analysis of pesticide residues in olives. J. Sep. Sci. 30: 620-632 (2007). (Pubitemid 46510577)
13. C. Diez, W.A. Traag, P. Zommer, P. Marinero, and J. Atienza. Comparison of an acetonitrile extraction/partitioning and "dispersive solid-phase extraction" method with classical multi-residue methods for extraction of herbicide residues in barley samples. J. Chromatogr. A 1131: 11-23 (2006). (Pubitemid 44485659)
14. A. Garrido Frenich, M.D.M. Aguilera-luiz, J.L. Martinez Vidal, and R. Romerogonzalez. Comparison of several extraction techniques for multiclass analysis of veterinary drugs in eggs using ultra-high pressure liquid chromatography- tandem mass spectrometry. Anal. Chim. Acta 661: 150-160 (2010).
15. R. Lorenzini, V. Burato, M.D. Bella, M. Doria, I. Braschi, P. Flori, V. Cardenia, and R. Boni. Proceedings of Giornate Fitopatologiche 2008, Eds. Università di Bologna, Cervia (RA), Italy, 2008, pp. 521-528.
16. S. Walorczyk. Development of a multi-residue method for the determination of pesticides in cereals and dry animal feed using gas chromatography-tandem quadrupole mass spectrometry: II improvement and extension to new analytes. J. Chromatogr. A 1208: 202-214 (2008).
17. J. Dong, X.Y. Pan, L.P. Zhu, J. Sun, and S.Q. Pan. Improvements and applications of the QuEChERS method in multi-residue analysis of 54 pesticides in vegetables and fruits. Fenxi Ceshi Xuebao 27: 66-69 (2008).
18. Y. Jiang, X. Li, J. Xu, C. Pan, J. Zhang, and W. Niu. Multiresidue method for the determination of 77 pesticides in wine using QuEChERS sample preparation and gas chromatography with mass spectrometry. Food Addit. Contam. A 26: 859-866 (2009).
19. C. Lesueur, M. Gartner, A. Mentler, and M. Fuerhacker. Comparison of four extraction methods for the analysis of 24 pesticides in soil samples with gas chromatography- mass spectrometry and liquid chromatography-ion trap-mass spectrometry. Talanta 75: 284-293 (2008).
20. T.D. Nguyen, J.E. Yu, D.M. Lee, and G.H. Lee. A multiresidue method for the determination of 107 pesticides in cabbage and radish using QuEChERS sample preparation method and gas chromatography mass spectrometry. Food Chem. 110: 207-213 (2008).
21. C.Pan, H. Zhang, S. Chen, Y. Xu, and S. Jiang. Determination of chloramphenicol residues in honey by monolithic column liquid chromatography-mass spectrometry after use of quechers clean-up. Acta Chromatogr. 17: 320-327 (2006).
22. P. Paya, M. Anastassiades, D. Mack, I. Sigalova, B. Tasdelen, J. Oliva, and A. Barba. Analysis of pesticide residues using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometric detection. Anal. Bioanal. Chem. 389: 1697-1714 (2007). (Pubitemid 350231577)
23. O.D. Prestes, C.A. Friggi, M.B. Adaime, and R. Zanella. QuEChERS: A modern sample preparation method for pesticide multiresidue determination in food by chromatographic methods coupled to mass spectrometry. Quim. Nova 32: 1620-1634 (2009).
24. F. Ploessl, M. Giera, and F. Bracher. Multiresidue analytical method using dispersive solid-phase extraction and gas chromatography/ion trap mass spectrometry to determine pharmaceuticals in whole blood. J. Chromatogr. A 1135: 19-26 (2006). (Pubitemid 44635547)
25. A. Garridofrenich, J.L. Martinez-vidal, E. Pastormontoro, and R. Romero-gonzalez. High-throughput determination of pesticide residues in food commodities by use of ultra-performance liquid chromatography-tandem mass spectrometry. Anal. Bioanal. Chem. 390: 947-959 (2008).
26. B. Kmellar, P. Fodor, L. Pareja, C. Ferrer, A. Martinez-Uroz Valverde, and A.R. Fernandez-Alba. Validation and uncertainty study of a comprehensive list of 160 pesticide residues in multi-class vegetables by liquid chromatographytandem mass spectrometry. J. Chromatogr. A 1215: 37-50 (2008).
27. S.B. Stubbing and T. Bigwood. The development and validation of a multiclass liquid chromatography tandem mass spectrometry (LC-MS/MS) procedure for the determination of veterinary drug residues in animal tissue using a QuEChERS (QUick, Easy, CHeap, Effective, Rugged and Safe) approach. Anal. Chim. Acta 637: 68-78 (2009).
28. S.L. Wang, Y.J. Xu, C.P. Pan, S.R. Jiang, and F.M. Liu. Application of matrix solidphase dispersion and liquid chromatography-mass spectrometry to fungicide residue analysis in fruits and vegetables. Anal. Bioanal. Chem. 387: 673-685 (2007).
29. D. Buhrman, P. Price, and P. Rudewicz. Quantitation of SR 27417 in Human Plasma Using Electrospray Liquid Chromatography-Tandem Mass Spectrometry: A Study of Ion Suppression. J. Am. Soc. Mass Spectrom. 7: 1099-1105 (1996). (Pubitemid 26359222)
30. L. Lucini and G.P. Molinari. Fate of the plant growth regulator BNOA (2-naphthyloxyacetic acid) following spray application to tomato. Agrochimica LIV, 34-40 (2010).
31. T. Pihlström. Method validation and quality control procedures for pesticide residues analysis in food and feed, SANCO/10684/2009; Eds. EU SANCO Directorate: Brussels, Belgium, 2010; pp. 10.