Synthesis of a coordinatively labile gold(III) methyl complex

Organometallics

Volumn 30, Issue 12, 2011, Pages 3250-3253

  Venugopal, Ajay ^a   Shaw, Anthony P ^b   Törnroos, Karl W ^c   Heyn, Richard H ^a   Tilset, Mats ^b  

^a SINTEF MATERIALS AND CHEMISTRY   (Norway)

^b UNIVERSITY OF OSLO   (Norway)

^c UNIVERSITY OF BERGEN   (Norway)

Author keywords

[No Author keywords available]

Indexed keywords

AU-COMPLEXES; LIGAND EXCHANGE REACTIONS; METHYL COMPLEXES; SILVER SALTS;

CHLORINE COMPOUNDS; SALTS; SYNTHESIS (CHEMICAL);

GOLD COMPOUNDS;

EID: 79959459233     PISSN: 02767333     EISSN: 15206041     Source Type: Journal    
DOI: 10.1021/om200327a     Document Type: Article

References (49)

1. Fürstner, A.; Davies, P. W. Angew. Chem., Int. Ed. 2007, 46, 3410
2. 2: Hashmi, A. S. K.; Weyrauch, J. P.; Rudolph, M.; Kurpejović, E. Angew. Chem., Int. Ed. 2004, 43, 6545
3. Wang, S.; Zhang, L. J. Am. Chem. Soc. 2006, 128, 14274
4. Shapiro, N. D.; Toste, F. D. J. Am. Chem. Soc. 2008, 130, 9244
5. Davies, P. W.; Albrecht, S. J.-C. Angew. Chem., Int. Ed. 2009, 48, 8372
6. Shapiro, N. D.; Shi, Y.; Toste, F. D. J. Am. Chem. Soc. 2009, 131, 11654
7. 2: Aguilar, D.; Contel, M.; Navarro, R.; Urriolabeitia, E. P. Organometallics 2007, 26, 4604
8. +: González-Arellano, C.; Corma, A.; Iglesias, M.; Sánchez, F. Chem. Commun. 2005, 1990
9. Lo, V. K.-L.; Liu, Y.; Wong, M.-K.; Che, C.-M. Org. Lett. 2006, 8, 1529
10. Debono, N.; Iglesias, M.; Sánchez, F. Adv. Synth. Catal. 2007, 349, 2470
11. -: Casado, R.; Contel, M.; Laguna, M.; Romero, P.; Sanz., S. J. Am. Chem. Soc. 2003, 125, 11925
12. Adé, A.; Cerrada, E.; Contel, M.; Laguna, M.; Merino, P.; Tejero, T. J. Organomet. Chem. 2004, 689, 1788 Others: Zhou, C.-Y.; Chan, P. W. H.; Che, C.-M. Org. Lett. 2006, 8, 325
13. Lo, V. K.-Y.; Kung, K. K.-Y.; Wong, M.-K.; Che, C.-M. J. Organomet. Chem. 2009, 694, 583
14. Corma, A.; Domínguez, I.; Doménech, A.; Fornés, V.; Gómez-García, C. J.; Ródenas, T.; Sabater, M. J. J. Catal. 2009, 265, 238
15. Oña-Burgos, P.; Fernández, I.; Roces, L.; Torre Fernández, L.; García-Granda, S.; López Ortiz, F. Organometallics 2009, 28, 1739
16. Pažický, M.; Loos, A.; Ferreira, M. J.; Serra, D.; Vinokurov, N.; Rominger, F.; Jäkel, C.; Hashmi, A. S. K.; Limbach, M. Organometallics 2010, 29, 4448
17. Hashmi, A. S. K. Angew. Chem., Int. Ed. 2010, 49, 5232
18. Peng, Y.; Cui, L.; Zhang, G.; Zhang, L. J. Am. Chem. Soc. 2009, 131, 5062
19. Zhang, G.; Peng, Y.; Cui, L; Zhang, L. Angew. Chem., Int. Ed. 2009, 48, 3112
20. Iglesias, A.; Muñiz, K. Chem.-Eur. J. 2009, 15, 10563
21. Zhang, G.; Cui, L.; Wang, Y.; Zhang, L. J. Am. Chem. Soc. 2010, 132, 1474
22. Ball, L. T.; Green, M.; Lloyd-Jones, G. C.; Russell, C. A. Org. Lett. 2010, 12, 4724
23. Brenzovich, W. E., Jr.; Brazeau, J.-F.; Toste, F. D. Org. Lett. 2010, 12, 4728
24. Melhado, A. D.; Brenzovich, W. E., Jr.; Lackner, A. D.; Toste, F. D. J. Am. Chem. Soc. 2010, 132, 8885
25. Hopkinson, M. N.; Tessier, A.; Salisbury, A.; Giuffredi, G. T.; Combettes, L. E.; Gee, A. D.; Gouverneur, V. Chem.-Eur. J. 2010, 16, 4739
26. Brenzovich, W. E., Jr.; Benitez, D.; Lackner, A. D.; Shunatona, H. P.; Tkatchouk, E.; Goddard, W. A., III; Toste, F. D. Angew. Chem., Int. Ed. 2010, 49, 5519
27. de Haro, T.; Nevado, C. Angew. Chem., Int. Ed. 2011, 50, 906
28. Zhang, G.; Luo, Y.; Wang, Y.; Zhang, L. Angew. Chem., Int. Ed. 2011, 50, 4450
29. Mankad, N. P.; Toste, F. D. J. Am. Chem. Soc. 2010, 132, 12859
30. Komiya, S.; Huffman, J. C.; Kochi, J. K. Inorg. Chem. 1977, 16, 2138
31. Shaw, A. P.; Tilset, M.; Heyn, R. H.; Jakobsen, S. J. Coord. Chem. 2011, 64, 38
32. Paul, M.; Schmidbaur, H. Z. Naturforsch. 1994, 49b, 647
33. Schuster, O.; Schmidbaur, H. Z. Naturforsch. 2006, 61b, 1
34. Venupogal, A.; Heyn, R. H., unpublished results.
35. Vicente, J.; Chicote, M. T.; Bermúdez, M. D.; Sanchez-Santano, M. J.; Jones, P. G. J. Organomet. Chem. 1988, 354, 381
36. See Supporting Information.
37. -3, T = 123(2) K, space group P 1̄, Z = 2, R1 = 0.0167, wR2 = 0.0437, CCDC number 790402.
38. Cocco, F.; Cinellu, M. A.; Minghetti, G.; Zucca, A.; Stoccoro, S.; Maiore, L.; Manassero, M. Organometallics 2010, 29, 1064
39. Fan, D.; Meléndez, E.; Ranford, J. D.; Loo, P. F.; Vittal, J. J. J. Organomet. Chem. 2004, 689, 2969
40. Venugopal, A.; Kumer Ghosh, M.; Jürgens, H.; Törnroos, K. W.; Swang, O.; Tilset, M.; Heyn, R. H. Organometallics 2010, 29, 2248, and references therein
41. Scott, V. J.; Labinger, J. A.; Bercaw, J. E. Organometallics 2010, 29, 4090
42. Fan, D.; Yang, C.-T.; Ranford, J. D.; Lee, P. F.; Vittal, J. J. Dalton Trans 2003, 2680
43. Parish, R. V.; Wright, J. P.; Pritchard, R. G. J. Organomet. Chem. 2000, 596, 165
44. 1/ c, Z = 4, R1 = 0.0174, wR2 = 0.0441, CCDC number 790403.
45. See ref 6. Au-O, 2.201(6) Å, S-O, 1.456(6), 1.439(4), and 1.439(4) Å, Au-O-S, 128.7(4)°.
46. Preisenberger, M.; Schier, A.; Schmidbaur, H. J. Chem. Soc., Dalton Trans. 1999, 1645 Au-O, 2.110(3) Å, S-O, 1.470(3), 1.432(4), and 1.426(3) Å, Au-O-S, 120.4(2)°.
47. -3, T = 123(2) K, space group P 1̄, Z = 2, R1 = 0.0170, wR2 = 0.0430, CCDC number 790404.
48. Contel, M.; Edwards, A. J.; Garrido, J.; Hursthouse, M. B.; Laguna, M.; Terroba, R. J. Organomet. Chem. 2000, 607, 129
49. Schmidbaur, H.; Schier, A. Organometallics 2010, 29, 2