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Tetrahedron Letters

Volumn 52, Issue 28, 2011, Pages 3551-3554

Bifunctional Aryloxylate Esters as potential oxidatively cleavable linkers

(4) Czarnecki, P V a Kampert, A a Barbe, S a Tiller, J C a

a TU DORTMUND UNIVERSITY (Germany)

Author keywords

Aryloxalate ester; Autocatalysis; Oxidative cleavable linker; Reaction kinetics

Indexed keywords

ARYL OXALATE ESTER; ESTER; UNCLASSIFIED DRUG;

ARTICLE; CATALYSIS; DEGRADATION; OXIDATION; SYNTHESIS;

EID: 79958758587 PISSN: 00404039 EISSN: 18733581 Source Type: Journal
DOI: 10.1016/j.tetlet.2011.04.083 Document Type: Article

Times cited : (4)

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- note
- 13C NMR (400 MHz, DMSO): δ = 19.57, 120.10, 123.44, 129.65, 131.05, 137.06, 148.34, 154.44 ppm. Preparation of bis(4-bromo-3,5-dimethylphenol) oxalate (AOE3). Following the general procedure it was prepared from 4-bromo-3,5-dimethylphenol (5.17 g; 26 mmol, 1.0 equiv), oxalyl chloride (1.63 g, 13 mmol, 0.5 equiv) and NaH (1.05 g, 60% in oil, 26 mmol), in a similar manner to that described above

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