An accurate quantitative LC/ESI-MS/MS method for sirolimus in human whole blood

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 879, Issue 13-14, 2011, Pages 987-992

  Mano, Nariyasu ^a,b   Sato, Mayumi ^a   Nozawa, Marina ^b   Matsumoto, Yotaro ^a   Mori, Masaru ^a   Yamaguchi, Hiroaki ^a,b,c   Goto, Junichi ^a   Shimada, Miki ^a,b  

^a TOHOKU UNIVERSITY HOSPITAL   (Japan)

^b TOHOKU UNIVERSITY   (Japan)

^c HOKKAIDO UNIVERSITY   (Japan)

Author keywords

Immunoassay; LC ESI MS MS; Sirolimus; Therapeutic drug monitoring

Indexed keywords

ANALYTICAL METHOD; CROSS-REACTIVITY; HYDROPHILIC COMPOUNDS; IMMUNOASSAY; LC/ESI-MS/MS; LINEAR RANGE; MATRIX EFFECTS; MINIMAL MATRIX; OCTADECYL; PRETREATMENT PROCEDURE; PROTEIN PRECIPITATION; REFERENCE METHOD; SIROLIMUS; THERAPEUTIC DRUG MONITORING; WHOLE BLOOD; ZINC SULFATE;

BLOOD; IMMUNOLOGY; METHANOL; ORGANIC SOLVENTS; PATIENT MONITORING; PHOSPHOLIPIDS; PRECIPITATION (CHEMICAL); SILICA; SILICA GEL;

CHEMICALS REMOVAL (WATER TREATMENT);

PHOSPHOLIPID; RAPAMYCIN; ZINC SULFATE;

ACCURACY; ARTICLE; CROSS REACTION; DRUG BLOOD LEVEL; DRUG MONITORING; ELECTROSPRAY MASS SPECTROMETRY; HUMAN; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MICROPARTICLE ENZYME IMMUNOASSAY; PRIORITY JOURNAL; QUANTITATIVE ASSAY; VALIDATION PROCESS;

CHROMATOGRAPHY, LIQUID; DRUG STABILITY; HUMANS; HYDROPHOBIC AND HYDROPHILIC INTERACTIONS; IMMUNOASSAY; REPRODUCIBILITY OF RESULTS; SIROLIMUS; SOLID PHASE EXTRACTION; SOLUBILITY; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY; TIME FACTORS;

EID: 79953305159     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2011.03.013     Document Type: Article

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