Development of the chromatographic fi{ligature}ngerprint of Scutellaria barbata D. Don by GC-MS combined with Chemometrics methods

Journal of Pharmaceutical and Biomedical Analysis

Volumn 55, Issue 3, 2011, Pages 391-396

  Pan, Ruijing ^a   Guo, Fangqiu ^a   Lu, Hongmei ^a   Feng, Wei wei ^a   liang, Yi zeng ^a  

^a CENTRAL SOUTH UNIVERSITY   (China)

Author keywords

Chemometrics methods; Chromatographic fingerprint; GC MS; Scutellaria barbata D. Don

Indexed keywords

ESSENTIAL OIL; PLANT EXTRACT; SCUTELLARIA BARBATA EXTRACT; UNCLASSIFIED DRUG; HERBACEOUS AGENT; VEGETABLE OIL;

ARTICLE; CHEMOMETRIC ANALYSIS; CHINESE MEDICINE; CONTROLLED STUDY; CORRELATION COEFFICIENT; LOBELIA; MASS FRAGMENTOGRAPHY; NONHUMAN; OLDENLANDIA; PRINCIPAL COMPONENT ANALYSIS; PRIORITY JOURNAL; SCUTELLARIA BARBATA; CHEMISTRY; CHINA; GROWTH, DEVELOPMENT AND AGING; INSTRUMENTATION; METHODOLOGY; QUALITY CONTROL; REPRODUCIBILITY; SCUTELLARIA; STANDARD;

CHINA; DRUGS, CHINESE HERBAL; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LOBELIA; OILS, VOLATILE; OLDENLANDIA; PLANT OILS; PRINCIPAL COMPONENT ANALYSIS; QUALITY CONTROL; REPRODUCIBILITY OF RESULTS; SCUTELLARIA;

EID: 79953190351     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2011.01.016     Document Type: Article

References (21)

1. Welsh W.J., Lin W., Tersigni S.H., Collantes E., Duta R., Carey M.S., Zielinski W.L., Brower J., Spencer J.A., Layloff T.P. Pharmaceutical fingerprinting: evaluation of neural networks and chemometric techniques for distinguishing among same-product manufacturers. Anal. Chem. 1996, 68:3473-3482.
2. Di X., Chan K.K.C., Leung H.W., Huie C.W. Fingerprint profiling of acid hydrolyzates of polysaccharides extracted from the fruiting bodies and spores of Lingzhi by high-performance thin-layer chromatography. J. Chromatogr. A 2003, 1018:85-95.
3. Xie P.-S. International symposium on quality of TCM with chromatographic fingerprint. Guangzhou 2001, 18-28.
4. van Beek T.A. Chemical analysis of Ginkgo biloba leaves and extracts. J. Chromatogr. A 2002, 967:21-55.
5. Sticher O. Quality of Ginkgo preparations. Planta Med. 1993, 59:2.
6. Smith R.M., Burford M.D. Comparison of flavanoids in feverfew varieties and related species by principal components analysis. Chemom. Intell. Lab. Syst. 1993, 18:285-291.
7. Zeeb D.J., Nelson B.C., Albert K., Dalluge J.J. Separation and identification of twelve Catechins in tea using liquid chromatography/atmospheric pressure chemical ionization-mass spectrometry. Anal. Chem. 2000, 72:5020-5026.
8. Christophe Pérès C.V., Jean-Louis Berdagué Solid-phase microextraction-mass spectrometry: an new approach to the rapid characterization of cheeses. Anal. Chem. 2001, 73:1030-1036.
9. Hasler A., Sticher O., Meier B. Identification and determination of the flavonoids from Ginkgo biloba by high-performance liquid chromatography. J. Chromatogr. A 1992, 605:41-48.
10. Wielandt W., Ellwanger A., Albert K., Lindner E. n-Alkyl fluorenyl phases in chromatography. I. Synthesis and characterization. J. Chromatogr. A 1998, 805:71-83.
11. State Drug Administration of China, Chinese Patent Medicines, vol. 22, 2000, p. 671.
12. Ong E.S. Chemical assay of glycyrrhizin in medicinal plants by pressurized liquid extraction (PLE) with capillary zone electrophoresis (CZE). J. Sep. Sci. 2002, 25:825-831.
13. Xie P.-S. The analysis of chromatographic fingerprint is an efficient method for quality control. Chin. Drug Res. Clin. Pharm. 2001, 12:141.
14. Valentao P., Andrade P.B., Areias F., Ferreres F., Seabra R.M. Analysis of vervain flavonoids by HPLC/diode array detector method. Its application to quality control. J. Agric. Food Chem. 1999, 47:4579-4582.
15. Yan F., Liang Y.-Z., Cai J.-N., Wang Z.-T., Losahan X., Zhang Z.-X. Analysis of Cnidium monnieri fruits in different regions of China. Talanta 2001, 53:1155-1162.
16. Gong F., Wang B.-T., Liang Y.-Z., Chau F.-T., Fung Y.-S. Variable selection for discriminating herbal medicines with chromatographic fingerprints. Anal. Chim. Acta 2006, 572:265-271.
17. Oprean R., Tamas M., Sandulescu R., Roman L. n-Alkyl fluorenyl phases in chromatography. I. Synthesis and characterization. J. Pharm. Biomed. Anal. 1998, 18:651-657.
18. Chinese Pharmacopoeia Committee, Chinese Pharmacopoeia, Appendix 57, Publishing House of Chemical Industry, Beijing, 2005.
19. Xie B.-G., Gong T., Tang M.-H. An approach based on HPLC-fingerprint and chemometrics to quality consistency evaluation of liuweidihuang pills produced by different manufactures. J. Pharm. Biomed. Anal. 2008, 48:1261-1266.
20. Mok D.K.W., Chau F.-T. Chemical information of Chinese medicines: a challenge to chemist. Chemom. Intell. Lab. Syst. 2006, 82:210-217.
21. Liang Y.-Z., Xie P.-S., Chan K. Quality control of herbal medicines. J. Chromatogr. B 2004, 812:53-70.