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Volumn 805, Issue 1-2, 1998, Pages 71-83

n-Alkyl fluorenyl phases in chromatography. I. Synthesis and characterization

Author keywords

interactions; Fluorenyl alkyl silanes; Interphases; LC; Nuclear magnetic resonance spectroscopy; Polynuclear aromatic hydrocarbons; Solid state NMR spectroscopy; Stationary phases

Indexed keywords

FLUORENE DERIVATIVE; POLYCYCLIC AROMATIC HYDROCARBON; SILANE DERIVATIVE;

EID: 0032076035     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0021-9673(98)00014-4     Document Type: Article
Times cited : (21)

References (47)
  • 1
    • 0344904506 scopus 로고
    • (Editor), (Packings and Stationary Phases in Chromatographic Techniques), Marcel Dekker, New York, Basel
    • K.K. Unger (Editor), Chromatogr. Sci., Vol. 47 (Packings and Stationary Phases in Chromatographic Techniques), Marcel Dekker, New York, Basel, 1990.
    • (1990) Chromatogr. Sci. , vol.47
    • Unger, K.K.1
  • 13
    • 0011315553 scopus 로고
    • in K. K. Unger (Editor) (Packings and Stationary Phases in Chromatographic Techniques), Marcel Dekker, New York, Basel
    • H. Hemetsberger, in K. K. Unger (Editor), Chromatogr. Sci., Vol. 47 (Packings and Stationary Phases in Chromatographic Techniques), Marcel Dekker, New York, Basel, 1990, p. 511.
    • (1990) Chromatogr. Sci. , vol.47 , pp. 511
    • Hemetsberger, H.1
  • 32
    • 0344904484 scopus 로고    scopus 로고
    • Due to the incomplete hydrosilation reaction no satisfactory elemental analyses were obtainable. Because of the still present educt, the carbon value was found to be too high, whereas the hydrogen value was too low.
    • Due to the incomplete hydrosilation reaction no satisfactory elemental analyses were obtainable. Because of the still present educt, the carbon value was found to be too high, whereas the hydrogen value was too low.
  • 37
    • 0345335613 scopus 로고    scopus 로고
    • 0), two signals in the alkyl area are attributed to the terminal methylene groups of the spacer. Due to the sensitivity of the silyl group to moisture, purification of these compounds proved to be difficult. However, further purification is not necessary because the educts 1 and 2 are washed out during the modification process.
    • 0), two signals in the alkyl area are attributed to the terminal methylene groups of the spacer. Due to the sensitivity of the silyl group to moisture, purification of these compounds proved to be difficult. However, further purification is not necessary because the educts 1 and 2 are washed out during the modification process.
  • 40
    • 0345335611 scopus 로고    scopus 로고
    • M, T, Q=one, two and three SiO and SiCl bonds, respectively; n=0-3, m=0-4.
    • M, T, Q=one, two and three SiO and SiCl bonds, respectively; n=0-3, m=0-4.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.