Densification behavior and microstructure of carbon/carbon composites prepared by chemical vapor infiltration from xylene at temperatures between 900 and 1250 °c

Carbon

Volumn 49, Issue 7, 2011, Pages 2561-2570

  Deng, Hailiang ^a   Li, Kezhi ^a   Li, Hejun ^a   Li, Xin ^a   Zhang, Leilei ^a   Cao, Weifeng ^a  

^a NORTHWESTERN POLYTECHNICAL UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

DENSIFICATION BEHAVIOR; DENSITY PROFILE; DEPOSITION TEMPERATURES; EXPERIMENTAL EQUIPMENTS; FILM BOILING; HETEROGENEOUS NUCLEATION AND GROWTH; HOMOGENEOUS NUCLEATION; INITIAL DEPOSITIONS; MASS GAIN; MATRIX; POLARIZED LIGHT MICROSCOPY; PYROCARBONS; RADIAL DIRECTION; ROUGH LAMINAR; SMOOTH LAMINAR; STRUCTURAL TRANSITIONS;

AROMATIC HYDROCARBONS; CRACKING (CHEMICAL); DEPOSITION RATES; MICROSTRUCTURE; NUCLEATION; SEEPAGE; SOIL MECHANICS; VAPORS; XYLENE;

CARBON CARBON COMPOSITES;

EID: 79952991559     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carbon.2011.02.046     Document Type: Article

References (28)

1. I. Golecki Rapid vapor-phase densification of refractory composites Mater Sci Eng R20 2 1997 37 124 (Pubitemid 127404043)
2. Houdayer M, Spitz J, Tran-Van D. Process for the densification of a porous structure. US patent 4472454; 1984.
3. E. Bruneton, B. Narcy, and A. Oberlin Carbon-carbon composites prepared by a rapid densification process: I. Synthesis and physico-chemical data Carbon 35 10-11 1997 1593 1598 (Pubitemid 127396437)
4. W.C. Sun, H.J. Li, H.M. Han, S.Y. Zhang, and K.Z. Li Microstructure of the pyrocarbon matrix prepared by the CLVI process Mater Sci Eng A 369 1-2 2004 245 249
5. D. Rovillain, M. Trinquecoste, E. Bruneton, A. Derré, P. David, and P. Delha Film boiling chemical vapor infiltration: an experimental study on carbon/carbon composite materials Carbon 39 9 2001 1355 1365 (Pubitemid 32535952)
6. G.L. Vignoles, J.M. Goyhénche, P. Sébastian, J.P. Puiggali, J.F. Lines, and J. Lachaud The film-boiling densification process for C/C composite fabrication: from local scale to overall optimization Chem Eng Sci 61 17 2006 5636 5653 (Pubitemid 44043127)
7. P. Delhas, M. Trinquecoste, J.F. Lines, A. Cosculluela, J.M. Goyhénche, and M. Couzi Chemical vapor infiltration of C/C composites: fast densification processes and matrix characterizations Carbon 43 4 2005 681 691 (Pubitemid 40211985)
8. X.T. Li, K.Z. Li, H.J. Li, J. Wei, and C. Wang Microstructures and mechanical properties of C/C composites reinforced with carbon nanofibers/nanotubes produced in situ Carbon 45 8 2007 1662 1668 (Pubitemid 46990360)
9. G.L. Dong, and K.J. Hüttinger Consideration of reaction mechanisms leading to pyrolytic carbon of different textures Carbon 40 14 2002 2515 2528
10. A. Oberlin Pyrocarbons Carbon 40 1 2002 7 24 (Pubitemid 33050829)
11. K.J. Hüttinger CVD in hot wall reactors - the interaction between homogeneous gas-phase and heterogeneous surface reactions Chem Vap Deposition 4 4 1998 151 158 (Pubitemid 128463723)
12. W. Benzinger, A. Becker, and K.J. Hüttinger Chemistry and kinetics of chemical vapour deposition of pyrocarbon: I. Fundamentals of kinetics and chemical reaction engineering Carbon 34 8 1996 957 966 (Pubitemid 126341061)
13. E.J. Davies Conduction and induction heating 1990 Peter Peregrinus Ltd. London, United Kingdom
14. M.L. Lieberman, and H.O. Pierson Effect of gas phase conditions on resultant matrix pyrocarbon in carbon/carbon composites Carbon 12 3 1974 233 241
15. X. Bourrat, B. Trouvat, G. Limousin, G. Vignoles, and F. Doux Pyrocarbon anisotropy as measured by electron diffraction and polarized light J Mater Res 15 1 2000 92 101 (Pubitemid 34566537)
16. J.M. Rosas, J. Bedia-Matamoros, J. Rodríguez-Mrasol, and T. Cordero Kinetics of pyrolytic carbon infiltration for the preparation of ceramic/carbon and carbon/carbon composites Carbon 42 7 2004 1285 1290
17. Z.J. Hu, W.G. Zhang, K.J. Hüttinger, B. Reznik, and D. Gerthsen Influence of pressure, temperature and surface area/volume ratio on the texture of pyrolytic carbon deposited from methane Carbon 41 4 2003 749 758
18. O. Feron, F. Langlais, R. Naslain, and J. Thebault On kinetic and microstructural transitions in the CVD pyrocarbon from propane Carbon 37 9 1999 1343 1353
19. G.L. Vignoles, F. Langlais, C. Descamps, A. Mouchon, H.L. Poche, and N. Reuge CVD and CVI of pyrocarbon from various precursors Surf Coat Technol 188-189 2004 241 249 (Pubitemid 40318294)
20. I.D. Costa, R.A. Eng, A. Gebert, and H. Hippler Direct observation of the rate of H-atom formation in the thermal decomposition of ortho-, meta- and para-xylene behind shock waves between 1300 and 1800 K Proc Combust Inst 28 2 2000 1537 1543
21. M. Frenklach Reaction mechanism of soot formation in flames Phys Chem Chem Phys 4 2002 2028 2037
22. C.S. McEnally, L.D. Pfefferle, B. Atakan, and K. Kohse-Höinghaus Studies of aromatic hydrocarbon formation mechanisms in flames: progress towards closing the fuel gap Prog Energ Combust Sci 32 3 2006 247 294
23. H. Wang, and M. Frenklach A detailed kinetic modeling study of aromatics formation in laminar premixed acetylene and ethylene flames Combust Flame 110 1-2 1997 173 221 (Pubitemid 27273036)
24. K. Norinaga, O. Deutschmann, N. Saegusa, and J.I. Hayashi Analysis of pyrolysis products from light hydrocarbons and kinetic modeling for growth of polycyclic aromatic hydrocarbons with detailed chemistry J Anal Appl Pyrolysis 86 1 2009 148 160
25. M.G. Brioukov, J. Park, and M.C. Lin Kinetic modeling of benzene decomposition near 1000 K: the effects of toluene impurity Int J Chem Kinet 31 8 1999 577 582
26. H. Richter, W.J. Grieco, and J.B. Howard Formation mechanism of polycyclic hydrocarbons and fullerenes in premixed benzene flames Combust Flame 119 1-2 1999 1 22 (Pubitemid 29398490)
27. K. Siegmann, H. Hepp, and K. Sattler Reactive dimerization: a new PAH growth mechanism in flames Combust Sci Technol 109 1-6 1995 165 181
28. V.D. Pauw, S. Kalhöfer, and D. Gerthsen Influence of the deposition parameters on the texture of pyrolytic carbon layers deposited on planar substrates Carbon 42 2 2004 279 286