Solid-phase microextraction - Gas chromatography mass spectrometry: A fast and simple screening method for the assessment of organophosphorus pesticides residues in wine and fruit juices

Food Chemistry

Volumn 86, Issue 2, 2004, Pages 269-274

  Zambonin, Carlo G ^a   Quinto, Maurizio ^b   De Vietro, Nicoletta ^a   Palmisano, Francesco ^a  

^a UNIVERSITY OF BARI   (Italy)

^b UNIVERSITY OF FOGGIA   (Italy)

Author keywords

Fruit juices; GC MS; Organophosphorus pesticides; SPME; Wine

Indexed keywords

DIMPYLATE; FENITROTHION; FENTHION; MALATHION; METHIDATHION; ORGANOPHOSPHATE PESTICIDE; PARATHION; PARATHION METHYL; PHORATE; SOLVENT;

ANALYTIC METHOD; ARTICLE; EUROPE; FOOD ANALYSIS; FRUIT JUICE; GAS CHROMATOGRAPHY; LAW; MASS SPECTROMETRY; QUANTITATIVE ANALYSIS; SCREENING TEST; SOLID PHASE MICROEXTRACTION; WINE;

EID: 1442360960     PISSN: 03088146     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodchem.2003.09.025     Document Type: Article

References (18)

1. Arthur C.L., Pawliszyn J. Solid phase microextraction with thermal desorption using fused optical fibers. Analytical Chemistry. 62:1990;2145-2148.
2. Beltran J., Lopez F.J., Cepria O., Hernandez F. Solid-phase microextraction for quantitative analysis of organophosphorus pesticides in environmental water samples. Journal of Chromatography A. 808:1998;257-263.
3. Bouaid A., Ramos L., Gonzalez M.J., Fernandez P., Camara C. Solid-phase microextraction method for the determination of atrazine and four organophosphorus pesticides in soil samples by gas chromatography. Journal of Chromatography A. 939:2001;13-21.
4. Choudhury T.K., Gerhardt K.O., Mawhinney T.P. Solid-phase microextraction of nitrogen- and phosphorus-containing pesticides from water and gas chromatographic analysis. Environmental Science and Technology. 30:1996;3259-3265.
5. Correia M., Delerue-Matos C., Alves A. Multi-residue methodology for pesticide screening in wines. Journal of Chromatography A. 889:2000;59-67.
6. Council Directive 90/642/EEC of 27 November 1990 on the fixing of maximum levels for pesticides residues in and on fruit and vegetables. In Official Journal of the European Communities L350, European Community, Brussels, 1990, p. 71
7. Eisert R., Levsen K. Determination of organophosphorus, triazine and 2,6-nitroaniline pesticides in aqueous samples via solid-phase microextraction (SPME) and gas chromatography with nitrogen-phosphorus detection. Fresenius Journal of Analytical Chemistry. 351:1995;555-562.
8. Eisert R., Levsen K. Determination of pesticides in aqueous samples by solid-phase microextraction in line coupled to gas chromatography-mass spectrometry. Journal of American Society Mass Spectrometry. 6:1995;1119-1130.
9. Eisert R., Levsen K., Wunsch G. Element selective detection of pesticides by gas chromatography-atomic emission detection and solid-phase microextraction. Journal of Chromatography A. 683:1994;175-183.
10. Fromberg A., Nilsson T., Richter Larsen B., Montanarella L., Facchetti S., Madsen J.O. Analysis of chloro- and nitroanilines and -benzenes in soils by headspace solid-phase microextraction. Journal of Chromatography A. 746:1996;71-81.
11. Lambropolou D.A., Albanis T.A. Headspace solid-phase microextraction in combination with gas chromatography-mass spectrometry for the rapid screening of organophosphorus pesticides in strawberries and cherries. Journal of Chromatography A. 993:2003;197-203.
12. Long G.L., Winefordner J.D. Limit of detection. Analytical Chemistry. 55:1983;712A-724A.
13. Magdic S., Boyd-Boland A., Jinno K., Pawliszyn J. Analysis of organophosphorus insecticides from environmental samples using solid-phase microextraction. Journal of Chromatography A. 736:1996;219-228.
14. Ng W.F., Mui J.K.T., Hans-Ake L. Determination of organophosphorus pesticides in soil by headspace solid-phase microextraction. Fresenius Journal of Analytical Chemistry. 363:1999;673-679.
15. Simplicio A.L., Vilas Boas L. Validation of a solid-phase microextraction method for the determination of organophosphorus pesticides in fruits and fruit juice. Journal of Chromatography A. 833:1999;35-42.
16. Valor I., Moltò J.C., Apraiz D., Font G. Matrix effects on solid-phase microextraction of organophosphorus pesticides from water. Journal of Chromatography A. 767:1997;195-203.
17. Yang, K. W., Eisert, R., Lord, H., & Pawliszyn, J. (1999). Determination of pesticides in foods by automated SPME-GC-MS. In J. Pawliszyn (Ed.), Applications of Solid Phase Microextraction (pp. 3-21). RSC Chromatography Monographs
18. Zambonin C.G., Losito I., Cilenti A., Palmisano F. Solid-phase microextraction coupled to gas chromatography-mass spectrometry for the study of soil adsorption coefficients of organophosphorus pesticides. Journal of Environmental Monitoring. 4:2002;477-481.