Rearrangement of the tris(2-pyridylthio)methanido ligand in an iron(II) complex containing an Fe-C bond

Inorganic Chemistry

Volumn 50, Issue 3, 2011, Pages 708-710

  Halder, Partha ^a   Paine, Tapan Kanti ^a  

^a DEPARTMENT OF MATERIALS SCIENCE   (India)

Author keywords

[No Author keywords available]

Indexed keywords

2 THIOPYRIDINE; 2-THIOPYRIDINE; FERROUS ION; PYRIDINE DERIVATIVE;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; SYNTHESIS;

FERROUS COMPOUNDS; MODELS, MOLECULAR; PYRIDINES;

EID: 79951618873     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic101913p     Document Type: Article

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24. Crystal data of 1-OTf: Mr = 657.54, triclinic, space group P1̄, a = 8.9779(5) Å, b = 10.8480(6) A, c = 13.2027(8) Å, α = 97.436(5)°, β = 94.259(5)°, γ = 92.101(5)°, V = 1270.11(13) Å3, Z = 2, ρ = 1.719 mgm-3,μ(Mo Kα) = 1.062 mm-1, F(000) = 666, GOF = 1.093. A total of 11 995 reflections were collected in the range 1.56° ≤ θ ≤ 25.00°, 4477 of which were unique (Rint = 0.0223). R1 (wR2) = 0.0527 (0.1528) for 343 parameters and 3931 reflections [I >2σ(7)].
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26. int = 0.0612). R1 (wR2) = 0.0394 (0.1024) for 370 parameters and 4787 reflections [I > 2σ(I)].