Electrochemical synthesis, characterization and thermal properties of niobium ethoxide

Journal of Central South University of Technology (English Edition)

Volumn 18, Issue 1, 2011, Pages 73-77

  Cai, Ya Nan ^a   Yang, Sheng Hai ^a   Jin, Sheng Ming ^a   Yang, Hai Ping ^a   Hou, Guo Feng ^a   Xia, Jiao Yun ^a  

^a CENTRAL SOUTH UNIVERSITY   (China)

Author keywords

characterization; electrochemical synthesis; niobium ethoxide; thermal analysis

Indexed keywords

CLAUSIUS-CLAPEYRON EQUATIONS; CONDUCTIVE ADDITIVES; ELECTROCHEMICAL REACTIONS; ELECTROCHEMICAL SYNTHESIS; ENTHALPY OF VAPORIZATION; ETHOXIDES; FOURIER TRANSFORM INFRARED; LANGMUIR EQUATION; METALLIC ELEMENTS; NIOBIUM PLATES; RAMAN SPECTRA; SACRIFICIAL ANODES; TEMPERATURE DATA; TETRAETHYLAMMONIUM; THERMAL ANALYSIS; THERMAL PROPERTIES; VACUUM DISTILLATION; VAPOUR PRESSURES;

AMMONIUM COMPOUNDS; ATOMIC LAYER DEPOSITION; CHEMICAL VAPOR DEPOSITION; CHLORINE COMPOUNDS; DISTILLATION; ELECTROCHEMICAL PROPERTIES; ELECTROCHEMISTRY; ETHANOL; FOURIER TRANSFORMS; METALLIC COMPOUNDS; NIOBIUM OXIDE; NUCLEAR MAGNETIC RESONANCE; RAMAN SPECTROSCOPY; RESONANCE; STAINLESS STEEL; SYNTHESIS (CHEMICAL); THERMOANALYSIS; THERMODYNAMIC PROPERTIES;

NIOBIUM;

EID: 79951490620     PISSN: 10059784     EISSN: None     Source Type: Journal    
DOI: 10.1007/s11771-011-0661-2     Document Type: Article

References (22)

1. 5 films [J] Thin Solid Films 515 4 1674 1682 10.1016/j.tsf.2006.05.047 (Pubitemid 44716104)
2. A. Tanaka K. Miyashita T. Tashiro M. Kimura T. Sukegawa 1995 Preparation of lithium niobate films by metalorganic chemical vapor deposition with a lithium alkoxide source [J] Journal of Crystal Growth 148 3 324 326 10.1016/0022-0248(94)01003-X
3. T. Maruyama T. Kanagawa 1994 Electrochromic properties of niobium oxide thin films prepared by chemical vapor deposition [J] Journal of the Electrochemical Society 141 10 2868 2871 10.1149/1.2059247
4. WERNBERG A A, GYSLING H J. Chemical vapor deposition of niobium and tantalum oxide films: US, 5271957 [P]. 1993-12-21.
5. D. C. Bradley 2002 Metal alkoxides as precursors for electronic and ceramic materials [J] Chemical Reviews 89 6 1317 1322 10.1021/cr00096a004
6. B. D. Wood V. Mocanu B. D. Gates 2008 Solution-phase synthesis of crystalline lithium niobate nanostructures [J] Advanced Materials 20 23 4552 4556 10.1002/adma.200800333
7. M. Macek B. Orel 1998 Electrochromism of sol-gel derived niobium oxide films [J] Solar Energy Materials and Solar Cells 54 1 121 130 10.1016/S0927-0248(98)00062-2 (Pubitemid 128408962)
8. A. Pignolet G. M. Rao S. B. Krupanidhi 1995 Rapid thermal processed thin films of niobium pentoxide (Nb2O5) deposited by reactive magnetron sputtering [J] Thin Solid Films 261 1/2 18 24
9. Y. Akiyama K. Shitanaka H. Murakami Y. S. Shin M. Yoshida N. Imaishi 2007 Epitaxial growth of lithium niobate film using metalorganic chemical vapor deposition [J] Thin Solid Films 515 12 4975 4979 10.1016/j.tsf.2006.10.034 (Pubitemid 46399840)
10. 5 catalysts [J] Journal of Central South University of Technology 14 6 788 792 10.1007/s11771-007-0150-9
11. J.-c. Zhang H.-l. Zhou Y.-l. Chen Y. Shen Y.-hua. Zhang 1998 Analysis of synthetical conditions, hydrolytic process and their characteristics for niobium alkoxides [J] Journal of Shanghai University 4 1 38 44
12. S.-h. Yang Y.-m. Chen H.-p. Yang Y.-y. Liu M.-t. Tang G.-zhou. Qiu 2008 Preparation of high-purity tantalum ethoxide by vacuum distillation [J] Transactions of Nonferrous Metals Society of China 18 1 196 201 10.1016/S1003-6326(08)60035-7 (Pubitemid 351312662)
13. S.-h. Yang Y.-n. Cai H.-p. Yang S.-ming. Jin 2009 Electrochemical synthesis and characterization of tantalum alkoxides [J] Transactions of Nonferrous Metals Society of China 19 6 1504 1508 10.1016/S1003-6326(09)60060-1
14. V. A. Shreider E. P. Turevskaya N. I. Koslova N. Y. Turova 1981 Direct electrochemical synthesis of metal alkoxides [J] Inorganica Chimica Acta 53 L73 L76 10.1016/S0020-1693(00)84746-5
15. M. Y. Berezkin I. N. Chernykh E. G. Polyakov A. P. Tomilov 2006 Electrochemical synthesis of niobium(V) ethylate [J] Applied Electrochemistry and Corrosion Protection of Metals 79 5 752 756
16. SILVERSTEIN R M, WEBSTER F X, KIEMLE D. Spectrometric identification of organic compounds [M] New York: John Wiley & Sons, 2005: 82-101.
17. DOLLISH F R, FATELEY W G, BENTLEY F F. Characteristic Raman frequencies of organic compounds [M]. New York: Wiley, 1974: 218.
18. S. Rushworth H. Davies A. Kingsley T. Leese R. Odedra 2007 Volatility and vapourisation characterisation of new precursors [J] Microelectronics Reliability 47 718 721 10.1016/j.microrel.2007.01.070 (Pubitemid 46602434)
19. I. Langmuir 1913 The vapor pressure of metallic tungsten [J] Physical Review 2 329 342 10.1103/PhysRev.2.329
20. G. V. Kunte S. A. Shivashankar A. M. Umarji 2008 Thermogravimetric evaluation of the suitability of precursors for MOCVD [J] Measurement Science and Technology 19 2 1 7 10.1088/0957-0233/19/2/025704 (Pubitemid 351584355)
21. S. F. Wright D. Dollimorel J. G. Dunn K. Alexander 2004 Determination of the vapor pressure curves of adipic acid and triethanolamine using thermogravimetric analysis [J] Thermochimica Acta 421 25 30 10.1016/j.tca.2004. 02.021 (Pubitemid 40125322)
22. HOCHIDO Y, KADOKURA H, TANABE S, KOBAYASHI R. Process for purifying niobium alkoxides and tantalum alkoxides: US, 5919963 [P]. 1999-07-06.