Determination of the nateglinide polymorphic purity through DSC

Journal of Pharmaceutical and Biomedical Analysis

Volumn 54, Issue 5, 2011, Pages 1196-1199

  Bruni, G ^a   Berbenni, V ^a   Milanese, C ^a   Girella, A ^a   Cardini, A ^b   Lanfranconi, S ^b   Marini, A ^a  

^a UNIVERSITY OF PAVIA   (Italy)

^b AMSA SpA   (Italy)

Author keywords

DSC; Nateglinide; Polymorphism; Purity; Quantification

Indexed keywords

NATEGLINIDE;

ARTICLE; DIFFERENTIAL SCANNING CALORIMETRY; DRUG DETERMINATION; DRUG PURITY; DRUG SCREENING; GRINDING; HEATING; MELTING POINT; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS;

CALORIMETRY, DIFFERENTIAL SCANNING; CRYSTALLIZATION; CYCLOHEXANES; DRUG COMPOUNDING; DRUG CONTAMINATION; HYDROGEN-ION CONCENTRATION; HYPOGLYCEMIC AGENTS; PHENYLALANINE; TRANSITION TEMPERATURE;

EID: 78751701555     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2010.12.003     Document Type: Article

References (7)

1. Bruni G., Berbenni V., Milanese C., Girella A., Cardini A., Viganò E., Lanfranconi S., Marini A. Thermodynamic relationships between nateglinide polymorphs. J. Pharm. Biomed. Anal. 2009, 50:764-770.
2. Bruni G., Berbenni V., Milanese C., Girella A., Cardini A., Lanfranconi S., Marini A. New solid modifications of nateglinide. J. Pharm. Biomed. Anal. 2010, 51:1054-1059.
3. Bruni G., Milanese C., Bellazzi G., Berbenni V., Cofrancesco P., Marini A., Villa M. Quantification of drug amorphous fraction by DSC. J. Therm. Anal. Cal. 2007, 89:761-766.
4. Marini A., Berbenni V., Bruni G., Margheritis C., Orlandi A. Physico-chemical study of the solid forms of a new drug. J. Pharm. Sci. 2001, 90:2131-2140.
5. Marini A., Berbenni V., Bruni G., Sinistri C., Maggioni A., Orlandi A., Villa M. Physico-chemical characterization of a novel tryciclic β-lactam antibiotic. J. Pharm. Sci. 2000, 89:232-240.
6. Hilfiker R. Polymorphism in the Pharmaceutical Industry 2006, Wiley-VCH, (Chapters 1-2).
7. Lieder R. FDA approves nateglinide for treatment of type 2 diabetes. Am. J. Health Syst. Pharm. 2001, 58:285-288.