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2O was sealed in a Teflon-lined stainless steel vessel, heated at 140 °C for 2 days under autogenous pressure, and then cooled to room temperature. Green block crystals of 1 were harvested in ca. 40% yield. Anal. Calcd. for 1: C, 28.99; H, 2.50; N, 22.54. Found: C, 28.68; H, 2.70; N, 22.39. CAUTION: Although not encountered in our experiments, azido compounds of metal ions are potentially explosive. Only a small amount of the materials should be prepared, and it should be handled with care
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2O was sealed in a Teflon-lined stainless steel vessel, heated at 140 °C for 2 days under autogenous pressure, and then cooled to room temperature. Green block crystals of 1 were harvested in ca. 40% yield. Anal. Calcd. for 1: C, 28.99; H, 2.50; N, 22.54. Found: C, 28.68; H, 2.70; N, 22.39. CAUTION: Although not encountered in our experiments, azido compounds of metal ions are potentially explosive. Only a small amount of the materials should be prepared, and it should be handled with care
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