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Crystallographic data of 1: C48H54Cu 13N24O36, Mr, 2369.18, trigonal, P3̄ a, 13.8310(12) Å. c= 11.996(2) Å. V= 1987.4(4) Å3, Z=1, ρcalcd, 1.969 g cm -3.,2θ, 52.22, 15≤h≤16, 15≤k≤16, 14≤ l≤11, T=294(2) K. 9944 measured reflections. R1, 0.0372, wR2= 0.1116 for 1702 reflections [I≥2σ(I, and R1= 0.0648. WR2, 0.-1277 for 2345 independent reflections (all data) and 183 parameters, GOF= 1.168. CCDC 651942 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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2 = 0.-1277 for 2345 independent reflections (all data) and 183 parameters, GOF= 1.168. CCDC 651942 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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