Electron backscatter diffraction (ebsd): A new technique for the identification of pigments and raw materials in historic glasses and ceramics

Archaeometry

Volumn 53, Issue 1, 2011, Pages 178-193

  Peruzzo, L ^a   Fenzi, F ^a   Vigato, P A ^a  

^a CNR   (Italy)

Author keywords

Ceramic; Electron Backscatter Diffraction (ebsd); Glass; Pigment; Production Technology; Raw Material

Indexed keywords

CERAMICS; COLOR; CRYSTALLOGRAPHY; DIFFRACTION; GLASS; PIGMENT;

EID: 78650240872     PISSN: 0003813X     EISSN: 14754754     Source Type: Journal    
DOI: 10.1111/j.1475-4754.2010.00540.x     Document Type: Article

References (50)

1. Adams, B. L., Wright, S. I., and Kunze, K., 1993, Orientation imaging: the emergence of a new microscopy, Metallurgical Transactions, A, 24, 819-31.
2. Alam, M. N., Blackman, M., and Pashley, D. W., 1954, High-angle Kikuchi patterns, Proceedings of the Royal Society of London Series A-Mathematical and Physical Sciences, 221 (1145), 224-42.
3. Alderighi, L., and Mendera, M., 1994, L'insediamento etrusco di Poggio Carlotta (Castelfiorentino). Scavi 1986-1989, Miscellanea Storica della Valdelsa, C, nos. 1-2 (267-8), 1-2, 7-98.
4. Allan, J. W., 1973, Abū'l-Qāsim's treatise on ceramics, Journal of Persian Studies, XI, 111-20.
5. Arnberg, L., Jonsson, A., and Westman, S., 1976, The structure of the δ-phase in the Cu-Sn system: a phase of γ-brass type with an 18 Å superstructure, Acta Chemica Scandinavica, 30, 187.
6. 6, a new mineral from the Cetine mine, Siena, Italy, European Journal of Mineralogy, 8, 487-92.
7. Benvenuti, M., and Guideri, S., 1991, Inventario del patrimonio minerario e mineralogico, in Toscana: aspetti naturalistici e storico-archeologici, Edizione Regione Toscana, Firenze.
8. Bianchin, S., Brianese, N., Casellato, U., Fenzi, F., Guerriero, P., Vigato, P. A., Battagliarin, M., Nodari, L., Russo, U., Galgani, M., and Mendera, M., 2005, Medieval and Renaissance glass technology in Valdelsa (Florence). Part 3: vitreous finds and crucibles, Journal of Cultural Heritage, 6, 165-82.
9. Blake, R. L., Hessevick, R. E., Zoltai, T., and Finger, L. W., 1966, Refinement of the hematite structure, American Mineralogist, 51, 123-9.
10. Boersch, H., 1937, About bands in electron diffraction, Physikalische Zeitschrift, 38, 1000-4 (in German).
11. Booth, M., Brandon, J., Brezard, R., Chieh, C., and Pearson, W. B., 1977, Gamma-brasses with F cells, Acta Crystallographica, 33, 30-6.
12. Brianese, N., Casellato U., Fenzi, F., Mendera, M., Messiga, B., Nodari, L., Riccardi, M. P., and Vigato, P. A., 2008, Incised slipware production at Castelfiorentino (Florence): the 'Via Bertini' site (15th-17th century), Archaeometry, 50, 775-96.
13. Capelli, C., and Marescotti, P., 2000, Caratterizzazione mineralogico-petrografica degli ingobbi delle ceramiche basso medievali savonesi, in Atti del I Congresso Nazionale di Archeometria, Verona 1999, 389-400, Patron, Bologna.
14. Casellato, U., Fenzi, F., Vigato, P. A., and Riccardi, M. P., 2004, Physico-chemical and mineralogical study of ceramic findings from Mary City-Turkmenistan, in Central Asia cultural values (ed. G. Rossi-Osmida), 3, 49-57, Il Punto Edizioni, Padova.
15. Casellato, U., Fenzi, F., Riccardi, M. P., Rossi Ossida, G., and Vigato, P. A., 2007, Physico-chemical and mineralogical study of ceramic findings from Mary City-Turkmenistan, Journal of Cultural Heritage, 8, 412-22.
16. Casellato, U., Fenzi, F., Mendera, M., Peruzzo, L., Riccardi, M. P., and Vigato, P. A., 2010, La produzione di ceramica graffita a Castelfiorentino (Firenze): il sito di via Bertini tra XV e XVII secolo, in Atti dell'11a giornata di archeometria della ceramica. Pesaro, 16-17 Aprile 2007 (in press).
17. Dey, B. N., and Quader, M. A., 1964, On the β→β' tranformation in Cu-Sn alloy, Indian Journal of Physics, 38, 398.
18. Dingley, D. J., 1984, Diffraction from sub-micron areas using electron backscattering in a scanning electron microscope, Scanning Electron Microscopy, 2, 569-75.
19. El-Dasher, B., and Deal, A., 2009, Application of electron backscatter diffraction to phase identification, in Electron backscatter diffraction in materials science, 2nd edn (eds. A. J. Schwartz, M. Kumar, D. P. Field and B. L. Adams), 81-96, Springer, New York.
20. Fenzi, F., Mendera, M., Peruzzo, L., and Vigato P. A., 2006, Microscopic investigations of ancient red copper-bearing glasses, paper presented at Syntheses and Methodologies in Inorganic Chemistry, SIMAC 2006, Bressanone (BZ), Italy, 3-7 December.
21. Fenzi, F., Mendera, M., Riccardi M. P., and Vigato P. A., 2007, Tessere musive, 'lingue' e 'pizze' rinvenute nel Duomo di Siena, in Atti del XII Colloquio dell'Associazione Italiana per lo Studio e la Conservazione del Mosaico, 147-56, Scripta Manent, Tivoli (Roma).
22. Freestone, I. C., Stapleton, C. P., and Rigby, V., 2003, The production of red glass and enamel in the Late Iron age, Roman and Byzantine periods, in Through a glass brightly: studies in Byzantine and medieval art and archaeology presented to David Buckton (ed. C. Entwistle), 142-54, Oxbow Books, Oxford.
23. Gasperin, M., 1955, Synthèse et identification de deux oxydes doubles de tantale et d'étain, Comptes Rendus Hebdomadaires des Séances de l'Académie des Sciences, 240, 2340-2.
24. 2Cl, Periodico di Mineralogia, 42, 335-45.
25. 2O and electronic charge density analysis by means of K-factors, Physics and Chemistry of Minerals, 9, 19-22.
26. Isajcev, I., 1947, Pis'ma v Zhurnal Tekhnicheskoi Fiziki, 17, 829 (in Cyrillic).
27. 3Sb, Philosophical Magazine, 4, 1302.
28. 5, Acta Crystallographica, 50, 636.
29. Lazzarini, L., Calogero, S., Burriesci, N., and Petrera, M., 1980, Chemical mineralogical and Mössbauer studies of Venetian and Paduan Renaissance sgraffito ceramics, Archaeometry, 22, 57-68.
30. Moore Valeri, A., 2004, Ceramiche rinascimentali di Castelfiorentino: l'ingobbiata e graffita in Toscana, Polistampa, Firenze.
31. Moore Valeri, A., 2006, Renaissance pottery from Tuscany, Current World Archaeology, 15, 39-42.
32. 3(m), Monatshefte für Chemie, 102, 1689-98.
33. Lloyd, G. E., 1987, Atomic number and crystallographic contrast images with the SEM: a review of backscattered electron techniques, Mineralogical Magazine, 51, 3-19.
34. Natta, G., and Baccaredda, M., 1933, Tetrossido di antimonio e antimoniati, Zeitschrift für Kristallographie, 85, 271-96.
35. Nishikawa, S., and Kikuchi, S., 1928, The diffraction of cathode rays by calcite, Proceedings of the Imperial Academy (of Japan), 4, 475-7.
36. Nowell, M. M., and Wright, S. I., 2004, Phase differentiation via combined EBSD and XEDS, Journal of Microscopy, 213, 296-305.
37. Pearson, W. B., 1958, A handbook of lattice spacings and structures of metals and alloys, Table IV.1, Pergamon Press, Oxford.
38. Peplinski, B., Schulz, G., Schultze, D., Schierhorn, E., and Zakel, E., 1994, X-ray powder diffraction investigation of ternary Au-Cu-Sn Alloys, Materials Science Forum, 166, 443.
39. Peruzzo, L., Zaghis, F., Salviulo, G., and Molin, G., 2005, Use of electron backscatter diffraction (EBSD) for the characterization of ancient metallic artifacts: a preliminary investigation on bronze finds from Frattesina, 5° FIST Geoitalia, Spoleto, 21-23 September 2005, Epitome, 1, 32.
40. Piccolpasso, C., 1879, Li tre libri del vasaio, Libro II, Pesaro.
41. Prior, D. J., Boyle, A. P., Brenker, F., Cheadle, M. C., Day, A., Lopez, G., Peruzzo, L., Reddy, S., Spiess, R., Timms, N. E., Trimby, P., Wheeler, J., and Zetterström, L., 1999, The application of electron backscatter diffraction and orientation contrast imaging in the SEM to textural problems in rocks, American Mineralogist, 84, 1741-59.
42. Schwartz, A. J., Kumar, M., Adams, B. L., and Field, D. P. (eds.), 2009, Electron backscatter diffraction in materials science, 2nd edn, Springer, New York.
43. Venables, J. A., and Harland, C. J., 1973, Electron back scattering patterns-new technique for obtaining crystallographic information in the scanning electron microscope, Philosophical Magazine, 27, 1193-200.
44. Villars, P., and Calvert, L. D. (eds.), 1991, Pearson's handbook of crystallographic data for intermetallic phases, 2nd edn, ASM International, Materials Park, Ohio.
45. Walenta, K., 1960, Natürliches Eisen(II)-Oxyd (Wüstit) aus der vulkanischen Tuffbreccie von Scharnhausen bei Stuttgart, Neues Jahrbuch für Mineralogie-Monatshefte, 150-9.
46. 4) MT100-1350, American Mineralogist, 69, 754-70.
47. Wilkinson, A. J., and Hirsch, P. B., 1997, Electron diffraction based techniques in scanning electron microscopy of bulk materials, Micron, 28, 279-308.
48. Wulff, H. E., 1966, The traditional crafts of Persia, 165, The MIT Press, Cambridge, MA.
49. Wyckoff, R. W. G., 1963, Crystal structures 1, 2nd edn, Interscience, New York.
50. Zaghis, F., Peruzzo, L., Salviulo, G., and Molin, G., 2005, A new approach in studying ancient Cu-Sn artifacts: measure of crystal orientation and phase distribution by EBSD analysis, XX IUCr, Florence, Italy, 23-31 August 2005, Acta Crystallographica, A61, C493.