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3, which was purchased from Merck (purity: 98%) and Aldrich (purity: 99.99%).
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note
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3 (0.16 mmol), TsOH (0.16 mmol), chlorobenzene (2 mL), alcohol (16 mmol) and olefin (4 mmol) were added to a sealed tube. The reaction mixture was stirred at 80 °C for 24 h and then cooled to room temperature and extracted with ethyl acetate. After removal of organic solvent, the product was finally obtained by column chromatography on silica gel.
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