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note
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-1): 3424 (w), 3125 (w), 1529 (m), 1307 (w), 1247 (w), 1130 (w), 1066 (s), 961 (s), 799 (s), 649 (w).
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22
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78649326534
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note
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2 = 0.1326 (all data). Data were collected on a Bruker Apex II CCD diffractometer with graphite-monochromated Mo Ka radiation (λ = 0.71069 Å). The structures were solved with direct methods and refined with full-matrix least squares (SHELX-97).
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