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Volumn 12, Issue 5, 2011, Pages 375-379

TiO2-SO42- as a novel solid acid catalyst for highly efficient, solvent free and easy synthesis of chalcones under microwave irradiation

(3) Krishnakumar, B a Velmurugan, R a Swaminathan, M a

a ANNAMALAI UNIVERSITY (India)

Author keywords

Chalcones; Lewis acidity; Microwave irradiation; Solid acid catalyst; Sulfated titania

Indexed keywords

CHALCONES; LEWIS ACIDITY; REACTION TIME; RECYCLABLE CATALYST; SOL-GEL METHODS; SOLID ACID CATALYST; SOLID ACID CATALYSTS; SOLVENT FREE; SULFATED TITANIA; TIO;

CATALYSTS; IRRADIATION; SOL-GEL PROCESS; SYNTHESIS (CHEMICAL); TITANIUM COMPOUNDS; TITANIUM DIOXIDE;

MICROWAVE IRRADIATION;

EID: 78649323350 PISSN: 15667367 EISSN: None Source Type: Journal
DOI: 10.1016/j.catcom.2010.10.015 Document Type: Article

Times cited : (58)

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- note
- 1H NMR (CDCl3, 500 MHz) (δ, ppm): 7.84 (d, J = 15.5, 1 H β), 7.55 (d, J = 15.5, 1 H α), 8.05 (m, 2 H), 7.65-7.40 (other aromatic protons, 8 H); 13 C NMR (CDCl3, 500 MHz) (δ, ppm): 190.43 (C?O), 132.82 (Cβ), 122.12 (Cα), 144.79-128.50 (aromatic carbons); GC-MS (m/z): 209.0 (M + 1).

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