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In a representative reaction, 1.0 mmol of aniline derivatives, 1.1 mmol of dihalides, and 1.1 mmol of potassium carbonate in 2 mL of distilled water were placed in a 10 mL crimp-sealed, thick-walled reaction tube equipped with a pressure sensor and a magnetic stirrer. The reaction tube was placed in the microwave cavity (CEM Discover Focused Microwave Synthesis System with a built-in infrared temperature sensor), operated at 120 ± 5°C, 80-100 W, and a pressure of 65-70 psi for 20 min. After completion of the reaction, the organic portion was extracted into ethyl acetate. Removal of the solvent under reduced pressure and flash column chromatography furnished the desired product.
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