The preparation of certified calibration solutions for azaspiracid-1, -2, and -3, potent marine biotoxins found in shellfish

Analytical and Bioanalytical Chemistry

Volumn 398, Issue 5, 2010, Pages 2243-2252

  Perez, Ruth A ^a   Rehmann, Nils ^b,c   Crain, Sheila ^a   Leblanc, Patricia ^a   Craft, Cheryl ^a   MacKinnon, Shawna ^a   Reeves, Kelley ^a   Burton, Ian W ^a   Walter, John A ^a   Hess, Philipp ^b,d   Quilliam, Michael A ^a   Melanson, Jeremy E ^a  

^a NATIONAL RESEARCH COUNCIL CANADA   (Canada)

^b MARINE INSTITUTE   (Ireland)

^c 921 College Hill Road   (Canada)

^d IFREMER   (France)

Author keywords

Marine toxins; Mass spectrometry LC MS; Reference materials

Indexed keywords

AZASPIRACID; CALIBRATION SOLUTIONS; GLASS AMPOULES; HIGH PURITY; LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY; MARINE TOXINS; MASS SPECTROMETRY/LC-MS; METHOD DEVELOPMENT; METHOD VALIDATIONS; MONITORING PROGRAMS; NMR SPECTROSCOPY; PREPARATIVE LIQUID CHROMATOGRAPHY; REFERENCE MATERIAL; STOCK SOLUTIONS;

ARGON; CALIBRATION; LIQUIDS; MASS SPECTROMETRY; METABOLITES; METHANOL; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RESONANCE;

LIQUID CHROMATOGRAPHY;

AZASPIRACID; AZASPIRACID 2; AZASPIRACID 3; AZASPIRACID-2; AZASPIRACID-3; FURAN DERIVATIVE; MARINE TOXIN; PYRAN DERIVATIVE; SPIRO COMPOUND;

ANIMAL; ARTICLE; BIVALVE; CHEMICAL STRUCTURE; CHEMISTRY; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SHELLFISH; SOLUTION AND SOLUBILITY;

ANIMALS; BIVALVIA; FURANS; MAGNETIC RESONANCE SPECTROSCOPY; MARINE TOXINS; MASS SPECTROMETRY; MOLECULAR STRUCTURE; PYRANS; SHELLFISH; SOLUTIONS; SPIRO COMPOUNDS;

EID: 78049337987     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-010-4161-2     Document Type: Article

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