-
3
-
-
42149190768
-
-
A.A. Agbodjan, B.E. Cooley, R.C.B. Copley, J.A. Corfield, R.C. Flanagan, B.N. Glover, R. Guidetti, D. Haigh, P.D. Howes, M.M. Jackson, R.T. Matsuoka, K.J. Medhurst, A. Millar, M.J. Sharp, M.J. Slater, J.F. Toczko, and S. Xie J. Org. Chem. 73 2008 3094 3102
-
(2008)
J. Org. Chem.
, vol.73
, pp. 3094-3102
-
-
Agbodjan, A.A.1
Cooley, B.E.2
Copley, R.C.B.3
Corfield, J.A.4
Flanagan, R.C.5
Glover, B.N.6
Guidetti, R.7
Haigh, D.8
Howes, P.D.9
Jackson, M.M.10
Matsuoka, R.T.11
Medhurst, K.J.12
Millar, A.13
Sharp, M.J.14
Slater, M.J.15
Toczko, J.F.16
Xie, S.17
-
5
-
-
72449191235
-
-
T. Hida, S. Mitsumori, T. Homa, Y. Hiramatsu, H. Hashizume, T. Okada, M. Kakinuma, K. Kawata, K. Oda, A. Hasegawa, T. Masui, and H. Nogusa Org. Process Res. Dev. 13 2009 1413 1418
-
(2009)
Org. Process Res. Dev.
, vol.13
, pp. 1413-1418
-
-
Hida, T.1
Mitsumori, S.2
Homa, T.3
Hiramatsu, Y.4
Hashizume, H.5
Okada, T.6
Kakinuma, M.7
Kawata, K.8
Oda, K.9
Hasegawa, A.10
Masui, T.11
Nogusa, H.12
-
7
-
-
0000749329
-
-
S. Saito, T. Hasegawa, M. Inaba, R. Nishida, T. Fuji, S. Nomizu, and T. Moriwake Chem. Lett. 13 1984 1389 1392
-
(1984)
Chem. Lett.
, vol.13
, pp. 1389-1392
-
-
Saito, S.1
Hasegawa, T.2
Inaba, M.3
Nishida, R.4
Fuji, T.5
Nomizu, S.6
Moriwake, T.7
-
11
-
-
17744384724
-
-
J.Y.L. Chung, R. Cvetovich, J. Amato, J.C. McWilliams, R. Reamer, and L. DiMicheke J. Org. Chem. 70 2005 3592 3601
-
(2005)
J. Org. Chem.
, vol.70
, pp. 3592-3601
-
-
Chung, J.Y.L.1
Cvetovich, R.2
Amato, J.3
McWilliams, J.C.4
Reamer, R.5
Dimicheke, L.6
-
16
-
-
0000288404
-
-
2-Aminoethanol with 2 equiv of borane was shown to rapidly reduce ketones but not esters or amides. S. Istuno, T. Wakasugi, K. Ito, A. Hirao, and S. Nakahama Bull. Chem. Soc. Jpn. 58 1985 1669 1673
-
(1985)
Bull. Chem. Soc. Jpn.
, vol.58
, pp. 1669-1673
-
-
Istuno, S.1
Wakasugi, T.2
Ito, K.3
Hirao, A.4
Nakahama, S.5
-
17
-
-
30944462359
-
-
V. Stepanenko, M. Ortiz-Marcailes, W. Correa, M. De Jesus, S. Espinosa, and L. Ortiz Tetrahedron: Asymmetry 17 2006 112 115
-
(2006)
Tetrahedron: Asymmetry
, vol.17
, pp. 112-115
-
-
Stepanenko, V.1
Ortiz-Marcailes, M.2
Correa, W.3
De Jesus, M.4
Espinosa, S.5
Ortiz, L.6
-
18
-
-
44949109272
-
-
K. Huang, F.G. Merced, M. Ortiz-Marcailes, H.J. Melendez, W. Correa, and M. De Jesús J. Org. Chem. 73 2008 4017 4026
-
(2008)
J. Org. Chem.
, vol.73
, pp. 4017-4026
-
-
Huang, K.1
Merced, F.G.2
Ortiz-Marcailes, M.3
Melendez, H.J.4
Correa, W.5
De Jesús, M.6
-
19
-
-
76449096962
-
-
V. Stepanenko, M. De Jesús, W. Correa, L. Bermúdez, C. Vázquez, I. Guzmán, and M. Ortiz-Marciales Tetrahedron: Asymmetry 23 2009 2659 2665
-
(2009)
Tetrahedron: Asymmetry
, vol.23
, pp. 2659-2665
-
-
Stepanenko, V.1
De Jesús, M.2
Correa, W.3
Bermúdez, L.4
Vázquez, C.5
Guzmán, I.6
Ortiz-Marciales, M.7
-
20
-
-
66249111475
-
-
K. Huang, M. Ortiz-Marcailes, W. Correa, E. Pomales, and X.Y. Lopez J. Org. Chem. 74 2009 4195 4202
-
(2009)
J. Org. Chem.
, vol.74
, pp. 4195-4202
-
-
Huang, K.1
Ortiz-Marcailes, M.2
Correa, W.3
Pomales, E.4
Lopez, X.Y.5
-
22
-
-
0034345895
-
-
R.M. Bannister, M.H. Brooks, G.R. Evans, R.B. Katz, and N.D. Tyrrell Org. Process Res. Dev. 4 2000 467
-
(2000)
Org. Process Res. Dev.
, vol.4
, pp. 467
-
-
Bannister, R.M.1
Brooks, M.H.2
Evans, G.R.3
Katz, R.B.4
Tyrrell, N.D.5
-
28
-
-
64249093753
-
-
D. Haddenham, L. Pasumansky, J. DeSoto, S. Eagon, and B. Singaram J. Org. Chem. 74 2009 1964 1970
-
(2009)
J. Org. Chem.
, vol.74
, pp. 1964-1970
-
-
Haddenham, D.1
Pasumansky, L.2
Desoto, J.3
Eagon, S.4
Singaram, B.5
-
30
-
-
77957990659
-
-
11B NMR resonances expected based on the corresponding resonances of morpholinoborane at 0.7 ppm (t, J = 113 Hz) and bis(morpholino)diborane at 3 ppm (t, J = 115 Hz). Bis(dimethylamino)borane is at 32 ppm (d, J = 130 Hz) and dimer is at 1.6 (t, J = 67 Hz).
-
11B NMR resonances expected based on the corresponding resonances of morpholinoborane at 0.7 ppm (t, J = 113 Hz) and bis(morpholino)diborane at 3 ppm (t, J = 115 Hz). Bis(dimethylamino)borane is at 32 ppm (d, J = 130 Hz) and dimer is at 1.6 (t, J = 67 Hz).
-
-
-
-
33
-
-
2542612665
-
-
BASF data: Morpholinodiborane -18.3 (br t, J = 142 Hz), L.D. Schwartz, and P.C. Keller J. Am. Chem. Soc. 94 1972 3015 3019 dialkylaminodiborane at -18 to -21 (J = 130, 30 Hz)
-
(1972)
J. Am. Chem. Soc.
, vol.94
, pp. 3015-3019
-
-
Schwartz, L.D.1
Keller, P.C.2
-
34
-
-
77958003326
-
-
11B NMR resonance is 28 ppm (d, J = 190 Hz), BASF internal data
-
11B NMR resonance is 28 ppm (d, J = 190 Hz), BASF internal data.
-
-
-
-
37
-
-
0004152853
-
-
Springer Berlin
-
Corey assigned oxazaborolidine monomer at 28.3 ppm as broad singlet and dimer at 7.6 ppm as doublet (J = 130 Hz) but this coupling constant is inconsistant for a boron bridged hydrogen (J = 30-50 Hz), see: H. Noeth, and B. Wrackmeyer Nuclear Magnetic Resonance Spectroscopy of Boron Compounds 1978 Springer Berlin
-
(1978)
Nuclear Magnetic Resonance Spectroscopy of Boron Compounds
-
-
Noeth, H.1
Wrackmeyer, B.2
-
38
-
-
77957989359
-
-
-1
-
-1.
-
-
-
-
41
-
-
77957981942
-
-
Use of SpiroCAT with DMSB or BTHF also dramatically accelerates ester reduction at rt
-
Use of SpiroCAT with DMSB or BTHF also dramatically accelerates ester reduction at rt.
-
-
-
|