C-ansa-zirconocene complexes with O/S donor ligands: Novel homoleptic six coordinate 4-mercaptophenolate complex of Zr(IV)

Inorganica Chimica Acta

Volumn 363, Issue 13, 2010, Pages 3489-3497

  Antiñolo, Antonio ^a   Fernández Galán, Rafael ^a   Molina, Noelia ^a   Otero, Antonio ^a   Rivilla, Iván ^a   Rodríguez, Ana M ^a  

^a UNIVERSITY OF CASTILLA LA MANCHA   (Spain)

Author keywords

Homoleptic; Metallocene; Phenolate; Thiolate; Zirconium

Indexed keywords

CHLORINE COMPOUNDS; LIGANDS; ORGANOMETALLICS; SINGLE CRYSTALS; SYNTHESIS (CHEMICAL); ZIRCONIUM;

4-MERCAPTOPHENOL; ANSA ZIRCONOCENE; DONOR LIGANDS; HIGHER YIELD; HOMOLEPTIC; PHENOLATE; SINGLE-CRYSTAL X-RAY DIFFRACTION STUDIES; THIOLATES;

ZIRCONIUM COMPOUNDS;

EID: 77957706440     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ica.2010.07.003     Document Type: Article

References (55)

1. D.C. Bradley, R.C. Mehrotra, A. Singh, and I.P. Rothwell Alkoxo and Aryloxo Derivatives of Metals 2001 Academic Press London
2. P. Sobota Coord. Chem. Rev. 248 2004 1047
3. J.M. Basset, B.C. Gates, J.P. Candy, A. Choplin, M. Leconte, F. Quignard, and C. Santini Surface Organometallic Chemistry: Molecular Approaches to Surface Catalysis 1988 Kluwer Dordrecht, The Netherlands
4. C. Coperet, M. Chabanas, R.P. Saint-Arroman, and J.M. Basset Angew. Chem., Int. Ed. 42 2003 156
5. J.R. Dilworth, and J. Hu Adv. Inorg. Chem. 40 1993 411 and references therein
6. D. Sellmann, R. Ruf, F. Knoch, and M. Moll Inorg. Chem. 34 1995 4745
7. R.C. Fay G. Wilkinson, R.D. Gillard, J.A. McCleverty, Comprehensive Coordination Chemistry vol. 3 1987 Pergamon Press Oxford (Chapter 32)
8. M.H. Chisholm, and I.P. Rothwell G. Wilkinson, R.D. Gillard, J.A. McCleverty, Comprehensive Coordination Chemistry vol. 2 1987 Pergamon Press Oxford (Chapter 15.3)
9. T.T. Nadasdi, and D.W. Stephan Inorg. Chem. 33 1994 1532
10. T.T. Nadasdi, and D.W. Stephan Inorg. Chem. 32 1993 5933
11. T.T. Nadasdi, Y. Huang, and D.W. Stephan Inorg. Chem. 32 1993 347
12. T.T. Nadasdi, and D.W. Stephan Organometallics 11 1992 116
13. D.W. Stephan Organometallics 10 1991 2037
14. D.W. Stephan J. Chem. Soc., Chem. Commun. 1991 129
15. D.W. Stephan Organometallics 9 1990 2718
16. P. Jutzi, T. Redeker, B. Neumann, and H.G. Stammler Organometallics 15 1996 4153
17. P. Jutzi, T. Heidemann, B. Neumann, and H.G. Stammler J. Organomet. Chem. 472 1994 27
18. R. Fandos, C. Hernandez, A. Otero, A. Rodríguez, M.J. Ruiz, and P. Terreros J. Organomet. Chem. 606 2000 156
19. R. Fandos, C. Hernandez, A. Otero, A. Rodríguez, M.J. Ruiz, and P. Terreros Eur. J. Inorg. Chem. 2003 493
20. R. Fandos, M. Lanfranchi, M.A. Pellinghelli, A. Otero, M.J. Ruiz, and P. Terreros Organometallics 15 1996 4725
21. A. Antiñolo, F. Carrillo-Hermosilla, A. Corrochano, R. Fandos, J. Fernández-Baeza, A.M. Rodríguez, M.J. Ruiz, and A. Otero Organometallics 18 1999 5219
22. A. Antiñolo, R. Fernández-Galán, A. Otero, S. Prashar, I. Rivilla, A.M. Rodríguez, and M.A. Maestro Organometallics 23 2004 5108
23. A. Antiñolo, R. Fernández-Galán, A. Otero, S. Prashar, I. Rivilla, and A.M. Rodríguez J. Organomet. Chem. 691 2006 2924
24. A. Antiñolo, R. Fernández-Galán, N. Molina, A. Otero, I. Rivilla, and A.M. Rodríguez J. Organomet. Chem. 694 2009 1959
25. A. Antiñolo, M. Fajardo, S. Gómez-Ruiz, I. López-Solera, A. Otero, S. Prashar, and A.M. Rodríguez J. Organomet. Chem. 683 2003 11
26. D. Polo-Cerón, S. Gómez-Ruiz, S. Prashar, M. Fajardo, A. Antiñolo, and A. Otero Eur. J. Inorg. Chem. 2007 4445
27. J.A. Samuels, E.B. Lobkovsky, W.E. Streib, K. Folting, J.C. Huffman, J.W. Zwanziger, and K.G. Caulton J. Am. Chem. Soc. 115 1993 5093
28. T.C. Rosen, K. Kirschbaum, and D.M. Giolando J. Chem. Soc., Dalton Trans. 2003 120
29. R.A. Kresinski, L. Isam, T.A. Hamor, C.J. Jones, and J.A. McCleverty J. Chem. Soc., Dalton Trans. 1991 1835
30. R. Fandos, J. Fernández-Gallardo, M.I. López-Solera, A. Otero, A. Rodríguez, M.J. Ruiz, and P. Terreros Organometallics 27 2008 4803
31. D.J. Cardin, M.F. Lappert, and C.L. Raston Chemistry of Organo-Zirconium and Hafnium Compounds 1986 Ellis Horwood Limited, Halsted Press New York
32. M.F. Lappert, C.J. Pickett, P.I. Riley, and P.I.W. Yarrow J. Chem. Soc., Dalton Trans. 1981 805
33. J.L. Atwood, G.K. Barker, J. Holton, W.E. Hunter, M.F. Lappert, and R. Pearce J. Am. Chem. Soc. 99 1977 6645
34. M.F. Lappert, P.I. Riley, P.I.W. Yarrow, J.L. Atwood, W.E. Hunter, and M.J. Zaworotko J. Chem. Soc., Dalton Trans. 1981 814
35. A. Antiñolo, R. Fernández-Galán, B. Gallego, A. Otero, S. Prashar, and A.M. Rodríguez Eur. J. Inorg. Chem. 2003 2626
36. T. Koch, S. Blaurock, F.B. Somoza Junior, A. Voigt, R. Kirmse, and E. Hey-Hawkins Organometallics 19 2000 2556
37. I.E. Nifant'ev, P.V. Ivchenko, V.V. Bagrov, and L.G. Kuz'mina Organometallics 17 1998 4734
38. E.S. Cho, U.G. Joung, B.Y. Lee, H. Lee, Y.-W. Park, Ch.-H. Lee, and D.M. Shin Organometallics 23 2004 4693
39. J.C. Green, M.L.H. Green, G.C. Taylor, and J. Saunders J. Chem. Soc., Dalton Trans. 2000 317
40. I.F. Urazowski, L.O. Atovmyan, S.G. Mkoyan, R. Broussier, P. Perron, B. Gautheron, and F. Robert J. Organomet. Chem. 536 1997 531
41. C.E. Zachmanoglou, A. Docrat, B.M. Bridgewater, G. Parkin, C.G. Brandow, J.E. Bercaw, C.N. Jardine, M. Lyall, J.C. Green, and J.B. Keister J. Am. Chem. Soc. 124 2002 9525
42. B.Y. Lee, Y.H. Kim, Y.C. Won, J.W. Han, W.H. Suh, I.S. Lee, Y.K. Chung, and K.H. Song Organometallics 21 2002 1500
43. A.D. Miller, J.L. McBee, and T.D. Tilley J. Am. Chem. Soc. 130 2008 4992
44. W.A. Howard, T.M. Trnka, and G. Parkin Inorg. Chem. 34 1995 5900
45. C.R. Baar, C.J. Levy, E.Y-J. Min, L.M. Henling, M.W. Day, and J.E. Bercaw J. Am. Chem. Soc. 126 2004 8216
46. N.W. Alcock, H.J. Clase, D.J. Duncalf, S.L. Hart, A. McCamley, P.J. McCormack, and P.C. Taylor J. Organomet. Chem. 605 2000 45
47. V.W.-W. Yam, G.-Z. Qi, and K.-K. Cheung J. Organomet. Chem. 548 1997 289
48. M.S. Rozenberg, T. Nishio, and T. Steiner New J. Chem. 23 1999 585
49. W. Stüer, K. Kirschbaum, and D.M. Giolando Angew. Chem., Int. Ed. Engl. 33 1994 1981
50. C.J. Carmalt, C.W. Dinnage, I.P. Parkin, and J.W. Steed Inorg. Chem. 39 2000 2693
51. C.J. Carmalt, C.W. Dinnage, I.P. Parkin, A.J.P. White, and D.J. Williams J. Chem. Soc., Dalton Trans. 2000 3500
52. E. Samuel, and M.D. Rausch J. Am. Chem. Soc. 95 1973 6263
53. saint+ v7.12a, Area-Detector Integration Program, Bruker-Nonius AXS, Madison, Wisconsin, USA, 2004.
54. G.M. Sheldrick, sadabs Version 2004/1, A Program for Empirical Absorption Correction, University of Göttingen, Göttingen, Germany, 2004.
55. shelxtl-nt Version 6.12, Structure Determination Package, Bruker-Nonius AXS, Madison, Wisconsin, USA, 2001.