Rapid and sensitive liquid chromatography/mass spectrometry assay for caspofungin in human aqueous humor

Antimicrobial Agents and Chemotherapy

Volumn 54, Issue 10, 2010, Pages 4467-4470

  Neoh, Chin Fen ^a   He, Hui ^a,f   Li, Jian ^a   Fullinfaw, Robert O ^b   Leung, Lok ^c   Misra, Anant ^c,g   Vajpayee, Rasik B ^c,d   Davies, Geoffrey E ^e   Stewart, Kay ^a   Kong, David C M ^a  

^a MONASH UNIVERSITY   (Australia)

^b ROYAL MELBOURNE HOSPITAL   (Australia)

^c ROYAL VICTORIAN EYE AND EAR HOSPITAL   (Australia)

^d UNIVERSITY OF MELBOURNE   (Australia)

^e Health Systems Program Office   (Australia)

^f UNIVERSITY OF TENNESSEE HEALTH SCIENCE CENTER   (United States)

^g NONE   (Australia)

Author keywords

[No Author keywords available]

Indexed keywords

ACETONITRILE; AZITHROMYCIN; CASPOFUNGIN;

ACCURACY; AQUEOUS HUMOR; ARTICLE; CONCENTRATION (PARAMETERS); DILUTION; HUMAN; LIQUID; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MULTIPLE SCLEROSIS; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SAMPLE; STANDARD; VALIDATION STUDY;

AQUEOUS HUMOR; AZITHROMYCIN; CHROMATOGRAPHY, LIQUID; ECHINOCANDINS; HUMANS; MASS SPECTROMETRY; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS;

EID: 77957357339     PISSN: 00664804     EISSN: 10986596     Source Type: Journal    
DOI: 10.1128/AAC.00509-10     Document Type: Article

References (16)

1. Chavez-Eng, C. M., M. S. Schwartz, M. L. Constanzer, and B. K. Matuszewski. 1999. Determination of a cyclic hexapeptide, a novel antifungal agent, in human plasma by high-performance liquid chromatography with ion spray and turbo ion spray tandem mass spectrometric detection. J. Chromatogr. B Biomed. Sci. Appl. 721:229-238.
2. Egle, H., R. Trittler, and K. Kummerer. 2004. An advanced double column-switching technique (LC-LC) for liquid chromatography/electrospray ionisation tandem mass spectrometry for fully automated analysis of caspofungin. Rapid Commun. Mass Spectrom. 18:2871-2877.
3. Farowski, F., O. A. Cornely, J. J. Vehreschild, P. Hartmann, T. Bauer, A. Steinbach, M. J. G. T. Ruping, and C. Muller. 2010. Quantitation of azoles and echinocandins in the compartments of peripheral blood by liquid chromatography tandem mass spectrometry. Antimicrob. Agents Chemother. 54:1815-1819.
4. Goldblum, D., K. Fausch, B. E. Frueh, R. Theurillat, W. Thormann, and S. Zimmerli. 2007. Ocular penetration of caspofungin in a rabbit uveitis model. Graefes Arch. Clin. Exp. Ophthalmol. 245:825-833.
5. Goldblum, D., B. E. Frueh, G. M. Sarra, K. Katsoulis, and S. Zimmerli. 2005. Topical caspofungin for treatment of keratitis caused by Candida albicans in a rabbit model. Antimicrob. Agents Chemother. 49:1359-1363.
6. Keski-Rahkonen, P., O. Parssinen, E. Leppanen, T. Mauriala, M. Lehtonen, and S. Auriola. 2007. Determination of tamsulosin in human aqueous humor and serum by liquid chromatography-electrospray ionization tandem mass spectrometry. J. Pharm. Biomed. Anal. 43:606-612.
7. O'Day, D. M., G. Foulds, T. E. Williams, R. D. Robinson, R. H. Allen, and W. S. Head. 1990. Ocular uptake of fluconazole following oral administration. Arch. Ophthalmol. 108:1006-1008.
8. Ozturk, F., G. F. Yavas, T. Kusbeci, Z. Cetinkaya, U. U. Inan, S. S. Ermis, and N. Kiraz. 2007. Efficacy of topical caspofungin in experimental Fusarium keratitis. Cornea 26:726-728.
9. Rochat, B., S. Bolay, A. Pascual, T. Calandra, and O. Marchetti. 2007. Liquid chromatography-mass spectrometry method for quantification of caspofungin in clinical plasma samples. J. Mass Spectrom. 42:440-449.
10. Schenkel, F., S. Rudaz, Y. Daali, M. K. Oestreicher, J. L. Veuthey, and P. Dayer. 2005. Development and validation of a new reversed-phase ion pairing liquid chromatographic method with fluorescence detection for penciclovir analysis in plasma and aqueous humour. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 826:1-7.
11. Schwartz, M. S., W. Kline, and B. K. Matuszewski. 1997. Determination of a cyclic hexapeptide (L-743 872), a novel pneumocandin antifungal agent in human plasma and urine by high-performance liquid chromatography with fluorescence detection. Anal. Chim. Acta 352:299-307.
12. Sheng, B., M. S. Schwartz, R. B. Desai, A. R. Miller, and B. K. Matuszewski. 2005. A semi-automated procedure for the determination of caspofungin in human plasma using solid-phase extraction and HPLC with fluorescence detection using secondary ionic interactions to obtain a highly purified extract. J. Liq. Chromatogr. Relat. Technol. 28:2895-2908.
13. Srinivasan, M. 2004. Fungal keratitis. Curr. Opin. Ophthalmol. 15:321-327.
14. Thomas, P. A. 2003. Current perspectives on ophthalmic mycoses. Clin. Microbiol. Rev. 16:730-797.
15. Traunmüller, F., I. Steiner, M. Zeitlinger, and C. Joukhadar. 2006. Development of a high-performance liquid chromatography method for the determination of caspofungin with amperometric detection and its application to in vitro microdialysis experiments. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 843:142-146.
16. Vorwerk, C. K., S. Tuchen, F. Streit, L. Binder, W. Hofmüller, and W. Behrens-Baumann. 2009. Aqueous humor concentrations of topically administered caspofungin in rabbits. Ophthalmic Res. 41:102-105.