A en-templated 3D coordination polymer based on H2pzdc with macrometallocycles

Inorganic Chemistry Communications

Volumn 13, Issue 11, 2010, Pages 1227-1230

  Wang, Hai Ning ^a   Qin, Jun Sheng ^a   Du, Dong Ying ^a   Xu, Guang Juan ^a   Wang, Xin Long ^a   Shao, Kui Zhan ^a   Yuan, Gang ^a   Li, Lian Jie ^a   Su, Zhong Min ^a  

^a NORTHEAST NORMAL UNIVERSITY   (China)

Author keywords

Coordination polymer; Luminescence; Macrometallocycle; Template; Zinc(II)

Indexed keywords

EID: 77956916652     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.06.011     Document Type: Article

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28. 2O (0.11 g), pyrazine-2, 3-dicarboxylic acid (0.25 g), three drops of ethylenediamine, deionized water (10 mL) was stirred for 30 min and then sealed in a 23 mL Teflon reactor and heated at 150 °C for 72 h. Coulorless block crystals of 1 were obtained, which were washed with water and dried in air with a 22% yield based on Zn. Elemental Anal. Calcd. (%) for it: C, 34.21; H, 1.75; N, 15.35; O, 27.81. Found: C, 34.28; H, 1.80; N, 15.01; O, 27.92.
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