Quantification of dialkylphosphate metabolites of organophosphorus insecticides in human urine using 96-well plate sample preparation and high-performance liquid chromatography-electrospray ionization-tandem mass spectrometry

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 878, Issue 27, 2010, Pages 2567-2574

  Odetokun, Martins S ^a   Montesano, M Angela ^a   Weerasekera, Gayanga ^a   Whitehead, Ralph D ^a   Needham, Larry L ^a   Barr, Dana Boyd ^a  

^a NATIONAL CENTER FOR ENVIRONMENTAL HEALTH   (United States)

Author keywords

DAPs; Dialkylphosphate; Electrospray ionization; HPLC; Organophosphorus metabolites; Tandem mass spectrometry

Indexed keywords

DAPS; DIALKYLPHOSPHATE; ELECTROSPRAYS; HPLC; ORGANOPHOSPHORUS METABOLITES; TANDEM MASS SPECTROMETRY;

ANIMALS; BIOMOLECULES; BODY FLUIDS; COLUMN CHROMATOGRAPHY; ELECTROSPRAY IONIZATION; HIGH PRESSURE LIQUID CHROMATOGRAPHY; INSECTICIDES; IONIZATION; LIQUIDS; MASS SPECTROMETRY; METABOLISM; METABOLITES; MONITORING; NEGATIVE IONS; PARTICLE DETECTORS;

EXTRACTION;

DIETHYLTHIOPHOSPHATE; DITHIOPHOSPHORIC ACID DIMETHYL ESTER; O,O DIMETHYLTHIOPHOSPHORIC ACID; ORGANOPHOSPHATE INSECTICIDE; PHOSPHORIC ACID DIETHYL ESTER; PHOSPHORIC ACID DIMETHYL ESTER; PHOSPHORODITHIOIC ACID O,O DIETHYL ESTER; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; HYDROPHILIC INTERACTION CHROMATOGRAPHY; METABOLITE; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; TANDEM MASS SPECTROMETRY; URINALYSIS; URINE LEVEL;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; ENVIRONMENTAL EXPOSURE; HUMANS; INSECTICIDES; LIMIT OF DETECTION; OCCUPATIONAL EXPOSURE; ORGANOPHOSPHORUS COMPOUNDS; QUALITY CONTROL; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY;

ANIMALIA;

EID: 77956876371     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2010.04.027     Document Type: Article

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