Monitoring of pesticide residues in vegetables marketed in Al-Qassim region, Saudi Arabia

Ecotoxicology and Environmental Safety

Volumn 73, Issue 6, 2010, Pages 1433-1439

  Osman, K A ^a   Al Humaid, A M ^b   Al Rehiayani, S M ^b   Al Redhaiman, K N ^b  

^a ALEXANDRIA UNIVERSITY   (Egypt)

^b QASSIM UNIVERSITY   (Saudi Arabia)

Author keywords

Gas chromatography; Pesticide; Qassim; Residues; Solid phase extraction; Vegetables

Indexed keywords

BIPHENYL; CARBARIL; CARBOFURAN; CHLORPYRIFOS; ETHIOFENCARB; HEPTANOPHOS; PESTICIDE; PESTICIDE RESIDUE; TOLCLOFOS METHYL; UNCLASSIFIED DRUG;

CONCENTRATION (COMPOSITION); GAS CHROMATOGRAPHY; MASS SPECTROMETRY; PESTICIDE RESIDUE; POLLUTION EFFECT; POLLUTION MONITORING; VEGETABLE;

ARTICLE; AUBERGINE; CABBAGE; CARROT; CHEMICAL ANALYSIS; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; CUCUMBER; FOOD ANALYSIS; FOOD CONTAMINATION; FOOD CONTROL; LETTUCE; MASS FRAGMENTOGRAPHY; NONHUMAN; PEPPER; QUANTITATIVE ANALYSIS; SAUDI ARABIA; SQUASH; TOMATO;

ENVIRONMENTAL MONITORING; FOOD ANALYSIS; FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LIMIT OF DETECTION; PESTICIDE RESIDUES; SAUDI ARABIA; SOLID PHASE EXTRACTION; VEGETABLES;

QASIM; SAUDI ARABIA;

BRASSICA OLERACEA VAR. CAPITATA; CUCUMIS SATIVUS; DAUCUS CAROTA; LACTUCA; LYCOPERSICON ESCULENTUM;

EID: 77956226150     PISSN: 01476513     EISSN: 10902414     Source Type: Journal    
DOI: 10.1016/j.ecoenv.2010.05.020     Document Type: Article

References (42)

1. Albero B., Sanchez-Brunete C., Tadeo J.L. Determination of organophosphorous pesticides in fruit juices by matrix solid-phase dispersion and gas chromatography. J. Agric. Food Chem. 2003, 51:6915-6921.
2. Amoah P., Drechsel P., Abaidoo R.C., Ntow W.J. Pesticide and pathogen contamination of vegetables in Ghana's urban markets. Arch. Environ. Contam. Toxicol. 2006, 50:1-6.
3. Andersson A., Pälsheden H. Comparison of the efficiency of different GLC multi-residue methods on crops containing pesticide residues. Fr. Anal. Chem. 1991, 339:365-367.
4. Araoud M., Douki W., Rhim A., Najjar M.F., Gazzah N. Multiresidue analysis of pesticides in fruits and vegetables by gas chromatography-mass spectrometry. J. Environ. Sci. Health B 2007, 42:179-187.
5. Balinova A., Mladenova R., Shtereva D. Solid-phase extraction on sorbents of different retention mechanisms followed by determination by gas chromatography-mass spectrometric and gas chromatography-electron capture detection of pesticide residues in crops. J. Chromatogr. A 2007, 1150:136-144.
6. Berrada H., Fernández M., Ruiz M.J., Moltó J.C., Mañes J., Font G. Surveillance of pesticide residues in fruits from Valencia during twenty months (2004/05). Food Control 2010, 21:36-44.
7. Businelli A., Vischetti C., Coletti A. Validation of Koc approach for modeling the fate of some herbicides in Italian soil. Fr. Anal. Chem. 1992, 1:583-588.
8. Cabras P., Conte E. Pesticide residues in grapes and wine in Italy. Food Addit. Contam. 2001, 18(10):880-885.
9. Chen L., Li X.-S., Wang Z.-Q., Pan C.-P., Jin R.-C. Residue dynamic of procymidone in leeks and soil in greenhouses by smoke generator application. Ecotoxicol. Envion. Saf. 2010, 73:73-77.
10. Clarke E.E., Levy L.S., Spurgeon A., Calvert I.A. The problems associated with pesticide use by irrigation workers in Ghana. Occup. Med. 1997, 47:301-308.
11. Council Directive, 1990. Council Directive 90/642/EEC of 27 November 1990 on the fixing of maximum levels for pesticide residues in and on certain products of plant origin, including fruit and vegetables (OJ L 350, 14/12/1990).
12. Council Directive, 2003. Commission Directive 2003/60/EC. Official Journal of the European Union, 18 June 2003.
13. Dogheim S.M., Ashraf E.M.M., Gad Alla S.A.G., Khorshid M.A., Fahmy S.M. Pesticides and heavy metals levels in Egyptian leafy vegetables and some aromatic medicinal plants. Food Addit. Contam. 2004, 21(4):323-330.
14. Du F.L., Zhu Q., Liu J. Evolution and control measures of vegetable pests and diseases. Yangtze Vegetable 2002, 3:28-29.
15. FAO/WHO, 2004. Food and Agriculture Organization/World Health Organization, Food standards programme. Codex Alimentarius Commission. Twenty-seventh Session, Geneva, Switzerland, 28 June-03 July 2004.
16. Freidberg S. Cleaning up down South: supermarkets, ethical trade and African horticulture. Soc. Cult. Geog. 2003, 4:27-43.
17. Gallivan G.J., Surgeoner G.A., Kovach J. Pesticide risk reduction on crops in the Province of Ontario. J. Environ. Qual. 2001, 30(3):798-813.
18. Gebara A.B., Ciscato C.H.P., Ferreira M.D.S., Monteiro M.D.S. Pesticide residues in vegetables and fruits monitored in Sao Paulo city, Brazil, 1994-2001. Bull. Environ. Contam. Toxicol. 2005, 75(1):163-169.
19. Gilbert-López B., Gracía-Reyes J.F., Mezcua M., Ramos-Martos N., Fernández-Alba A.R., Molina-Díaz A. Multi-residue determination of pesticides in fruit-based soft drinks by fast liquid chromatography time-of-flight mass spectrometry. Talanta 2010, 81:1310-1321.
20. González-Rodríguez R.M., Rial-Otero R., Cancho-Grande B., Simal-Gándara J. Occurrence of fungicide and insecticide residues in trade samples of leafy vegetables. Food Chem. 2008, 107:1342-1347.
21. González-Rodríguez R.M., Rial-Otero R., Cancho-Grande B., Simal-Gándara J. Determination of 23 pesticide residues in leafy vegetables using gas chromatography-ion trap mass spectrometry and analyte protectants. J. Chromatogr. A 2008, 1196-1197:100-109.
22. Gu J.T., Ding J.C., Gao T.C., Ma Y.M. The characteristics and no-pollution control of vegetable pests in Jiang-Huai Area. Anhui Agric. Sci. 2004, 32(500-501):508.
23. Herdman R.C., Pahrham W.E., Shen S. Pesticide Residues in Food: Technologies for Detection 1988, Government Printing Office, Washington.
24. Katz J.M., Winter C.K. Comparison of pesticide exposure from consumption of domestic and imported fruits and vegetables. Food Chem. Toxicol. 2009, 47:335-338.
25. Kovach J., Petzoldt C., Degnil J., Tette J. A method to measure the environmental impact of pesticides. New York's food. Life Sci. Bull. 1992, 139:1-8.
26. Levitan L. 'How to' and 'why': assessing the enviro-social impacts of pesticides. Crop Prot. 2000, 19(8-10):629-636.
27. Mansour S.A., Belal M.H., Abou-Arab A.A.K., Gad M.F. Monitoring of pesticide and heavy metals in cucumber fruits produced from different farming system. Chemosphere 2009, 75:601-609.
28. Menezes Filhoa A., Neves dos Santosa F., P.Afonso de Paula Pereira Development, validation and application of a methodology based on solid-phase micro extraction followed by gas chromatography coupled to mass spectrometry (SPME/GC-MS) for the determination of pesticide residues in mangoes. Talanta 2010, 81(346-354).
29. Nasreddine L., Parent-Massin D. Food contamination by metals and pesticides in the European Union. Should we worry?. Toxicol. Lett. 2002, 127:29-41.
30. Paulino de Pinho G., Augusto Neves A., Lopes Ribeiro de Queiroz M.E., Oliveira Silvério F. Pesticide determination in tomatoes by solid-liquid extraction with purification at low temperature and gas chromatography. Food Chem. 2010, 121:251-256.
31. Pose-Juan E., Cancho-Grande B., Rial-Otero R., Simal-Gándara J. The dissipation rates of cyprodinil, fludioxoni, procymidone and vinclozoline during storage of grape juice. Food Control 2006, 17(12):1012-1017.
32. Pose-Juan E., Rial-Otero R., Martinez-Carballo E., López-Periago E., Simal-Gándara J. Determination of metalaxyl and identification of adjuvants in wettable powder pesticide technical formulas. Anal. Bioanal. Chem. 2009, 394(6):1535-1544.
33. Poulsen M.E., Andersen J.H. Results from the monitoring of pesticide residues in fruit and vegetables on the Danish market, 2000-01. Food Addit. Contam. 2003, 20(8):742-757.
34. Pretty J., Hine R. Pesticide use and the environment. The Pesticide Detox: Towards a More Sustainable Agriculture 2005, Earthscan, London. J. Pretty (Ed.).
35. Pugliese P., Moltó J.C., Damiani P., Maíne R., Cossignani L., Mañes J. Gas chromatographic evaluation of pesticide residue contents in nectarines after non-toxic washing treatment. J. Chromatogr. A 2004, 1050:185-191.
36. Rial-Otero R., Arias-Estévez M., López-Periago E., Cancho-Grande B., Simal-Gándara J. variation in concentrations of the fungicides tebuconazole and dichlofuanid following successive applications to greenhouse-grown lettuces. J. Agric. Food Chem. 2005, 53(11):4471-4475.
37. SANCO 2003. Quality control procedures for pesticide residues analysis, guidelines for residues monitoring in the European Union, Document no. SANCO/10476/2003, Central Science Laboratory, York, UK.
38. Specht W., Pelz S., Gilsbach W. Gas-chromatographic determination of pesticide residues after clean-up by gel-permeation chromatography and mini-silica gel-column chromatography. J. Anal. Chem. 1995, 35:183-190.
39. Stan H.-J. Pesticide residue analysis in foodstuffs applying capillary gas chromatography with mass spectrometric detection state-of-the-art use of modified DFG-multimethod S19 and automated data evaluation. J. Chromatogr. A 2000, 892:347-377.
40. Štajnbaher D., Zupančič-Kralj L. Multiresidue method for determination of 90 pesticides in fresh fruits and vegetables using solid-phase extraction and gas chromatography-mass spectrometry. J. Chromatogr. A 2003, 1015:185-198.
41. Tomlin C.D.S. The e-Pesticide Manual, Version 2.2. 2002, The British Crop Protection Council, Surray, UK.
42. Winter C.K. Pesticide tolerances and their relevance as safety standard. Regul. Toxicol. Pharm. 1992, 14:137-150.