메뉴 건너뛰기




Volumn 74, Issue 2, 2010, Pages 219-224

Separation of azadirachtin and other limonoids from crude neem oil via solvent precipitation

Author keywords

Azadirachtin; Limonoids; Neem oil; Precipitation

Indexed keywords

AZADIRACHTIN; FINE POWDERS; NEEM OIL; OIL RATIO; OPTIMUM CONDITIONS; PRE-CONCENTRATION; PRECIPITATION METHODS; SOLVENT INDUCED; SOLVENT PRECIPITATION; STARTING MATERIALS;

EID: 77955515436     PISSN: 13835866     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.seppur.2010.06.008     Document Type: Article
Times cited : (26)

References (41)
  • 2
    • 67349137631 scopus 로고    scopus 로고
    • Azadirachtin, a scientific gold mine
    • E.D. Morgan Azadirachtin, a scientific gold mine Bioorgan. Med. Chem. 17 2009 4096 4105
    • (2009) Bioorgan. Med. Chem. , vol.17 , pp. 4096-4105
    • Morgan, E.D.1
  • 3
    • 30844438912 scopus 로고    scopus 로고
    • Botanical insecticides, deterrents, and repellents in modern agriculture and an increasingly regulated world
    • M.B. Isman Botanical insecticides, deterrents, and repellents in modern agriculture and an increasingly regulated world Annu. Rev. Entomol. 51 2006 45 66
    • (2006) Annu. Rev. Entomol. , vol.51 , pp. 45-66
    • Isman, M.B.1
  • 4
    • 0033784663 scopus 로고    scopus 로고
    • Insect antifeedant and growth-regulating activities of neem seed oil: The role of major tetranortriterpenoids
    • T.R. Govindachari, G. Suresh, G. Gopalakrishnan, and S.D. Wesley Insect antifeedant and growth-regulating activities of neem seed oil: the role of major tetranortriterpenoids J. Appl. Entomol. 124 2000 287 291
    • (2000) J. Appl. Entomol. , vol.124 , pp. 287-291
    • Govindachari, T.R.1    Suresh, G.2    Gopalakrishnan, G.3    Wesley, S.D.4
  • 5
    • 0029849413 scopus 로고    scopus 로고
    • Insect antifeedant and growth-regulating activities of salannin and other C-seco limonoids from neem oil in relation to azadirachtin
    • T.R. Govindachari, N.S. Narasimhan, G. Suresh, P.D. Partho, and G. Gopalakrishnan Insect antifeedant and growth-regulating activities of salannin and other C-seco limonoids from neem oil in relation to azadirachtin J. Chem. Ecol. 22 1996 1453 1461
    • (1996) J. Chem. Ecol. , vol.22 , pp. 1453-1461
    • Govindachari, T.R.1    Narasimhan, N.S.2    Suresh, G.3    Partho, P.D.4    Gopalakrishnan, G.5
  • 6
    • 33747077781 scopus 로고
    • Insecticidal and antifeedant bioactivities of neem oils and their relationship to azadirachtin content
    • M.B. Isman, O. Koul, A. Luczynski, and J. Kaminski Insecticidal and antifeedant bioactivities of neem oils and their relationship to azadirachtin content J. Agric. Food Chem. 38 1990 1406 1411
    • (1990) J. Agric. Food Chem. , vol.38 , pp. 1406-1411
    • Isman, M.B.1    Koul, O.2    Luczynski, A.3    Kaminski, J.4
  • 7
    • 0030624816 scopus 로고    scopus 로고
    • Effects of the neem tree compounds azadirachtin, salannin, nimbin, and 6-desacetylnimbin on ecdysone 20-monooxygenase activity
    • M.J. Mitchell, S.L. Smith, S. Johnson, and E.D. Morgan Effects of the neem tree compounds azadirachtin, salannin, nimbin, and 6-desacetylnimbin on ecdysone 20-monooxygenase activity Arch. Insect Biochem. 35 1997 199 209
    • (1997) Arch. Insect Biochem. , vol.35 , pp. 199-209
    • Mitchell, M.J.1    Smith, S.L.2    Johnson, S.3    Morgan, E.D.4
  • 8
    • 0000022901 scopus 로고    scopus 로고
    • Physicochemical and chemical variation in neem oils and some bioactivity leads against Spodoptera litura F.
    • J. Kumar, and B.S. Parmar Physicochemical and chemical variation in neem oils and some bioactivity leads against Spodoptera litura F. J. Agric. Food Chem. 44 1996 2137 2143
    • (1996) J. Agric. Food Chem. , vol.44 , pp. 2137-2143
    • Kumar, J.1    Parmar, B.S.2
  • 9
  • 11
    • 0036688782 scopus 로고    scopus 로고
    • Three new tetranortriterpenoids from neem seed oil
    • G. Hallur, A. Sivramakrishnan, and S.V. Bhat Three new tetranortriterpenoids from neem seed oil J. Nat. Prod. 65 2002 1177 1179
    • (2002) J. Nat. Prod. , vol.65 , pp. 1177-1179
    • Hallur, G.1    Sivramakrishnan, A.2    Bhat, S.V.3
  • 12
    • 0025878041 scopus 로고
    • Isolation of novel azadirachtins H and I by high-performance liquid chromatography
    • T.R. Govindachari, G. Sandhya, and S.R. Ganeshraj Isolation of novel azadirachtins H and I by high-performance liquid chromatography Chromatographia 31 1991 303 305
    • (1991) Chromatographia , vol.31 , pp. 303-305
    • Govindachari, T.R.1    Sandhya, G.2    Ganeshraj, S.R.3
  • 13
    • 37049081987 scopus 로고
    • Two new Insect growth regulator meliacins from Azadirachta indica A. Juss (Meliaceae)
    • S. Siddiqui, S. Faizi, T. Mahmood, and B.S. Siddiqui Two new Insect growth regulator meliacins from Azadirachta indica A. Juss (Meliaceae) J. Chem. Soc. Perkin Trans. 1 1986 1021
    • (1986) J. Chem. Soc. Perkin Trans. , vol.1 , pp. 1021
    • Siddiqui, S.1    Faizi, S.2    Mahmood, T.3    Siddiqui, B.S.4
  • 14
    • 0039557373 scopus 로고
    • Isolation and purification of azadirachtin from neem (Azadirachta indica) seeds using flash chromatography and high-performance liquid chromatography
    • R.B. Yamasaki, J.A. Klocke, S.M. Lee, G.A. Stone, and M.V. Darlington Isolation and purification of azadirachtin from neem (Azadirachta indica) seeds using flash chromatography and high-performance liquid chromatography J. Chromatogr. 356 1986 220 226
    • (1986) J. Chromatogr. , vol.356 , pp. 220-226
    • Yamasaki, R.B.1    Klocke, J.A.2    Lee, S.M.3    Stone, G.A.4    Darlington, M.V.5
  • 15
    • 0345402399 scopus 로고
    • Isolation and purification of salannin from neem seeds and its quantification in neem and chinaberry seeds and leaves
    • R.B. Yamasaki, T.G. Ritland, M.A. Barnby, and J.A. Klocke Isolation and purification of salannin from neem seeds and its quantification in neem and chinaberry seeds and leaves J. Chromatogr. 447 1988 277 283
    • (1988) J. Chromatogr. , vol.447 , pp. 277-283
    • Yamasaki, R.B.1    Ritland, T.G.2    Barnby, M.A.3    Klocke, J.A.4
  • 16
    • 0025351541 scopus 로고
    • Simple method for the isolation of azadirachtin by preparative high-performance liquid chromatography
    • T.R. Govindachari, G. Sandhya, and S.P.G. Raj Simple method for the isolation of azadirachtin by preparative high-performance liquid chromatography J. Chromatogr. 513 1990 389 391
    • (1990) J. Chromatogr. , vol.513 , pp. 389-391
    • Govindachari, T.R.1    Sandhya, G.2    Raj, S.P.G.3
  • 17
    • 34247634996 scopus 로고    scopus 로고
    • Purification of the seven tetranortriterpenoids in neem (Azadirachta Indica) seed by counter-current chromatography sequentially followed by isocratic preparative reversed-phase high-performance liquid chromatography
    • J.C.T. Silva, G.N. Jhama, R. D'arc, L. Oliveira, and L. Brown Purification of the seven tetranortriterpenoids in neem (Azadirachta Indica) seed by counter-current chromatography sequentially followed by isocratic preparative reversed-phase high-performance liquid chromatography J. Chromatogr. A 1151 2007 203 210
    • (2007) J. Chromatogr. A , vol.1151 , pp. 203-210
    • Silva, J.C.T.1    Jhama, G.N.2    D'arc, R.3    Oliveira, L.4    Brown, L.5
  • 18
    • 0038015355 scopus 로고    scopus 로고
    • An efficient method for the purification and characterization of nematicidal azadirachtins A, B, and H, using MPLC and ESIMS
    • V. Sharma, S. Walia, J. Kumar, M.G. Nair, and B.S. Parmar An efficient method for the purification and characterization of nematicidal azadirachtins A, B, and H, using MPLC and ESIMS J. Agric. Food Chem. 51 2003 3966 4397
    • (2003) J. Agric. Food Chem. , vol.51 , pp. 3966-4397
    • Sharma, V.1    Walia, S.2    Kumar, J.3    Nair, M.G.4    Parmar, B.S.5
  • 19
    • 0032958007 scopus 로고    scopus 로고
    • Rapid separation of triterpenoids from neem seed extracts
    • A.P. Jarvis, E.D. Morgan, and C. Edwards Rapid separation of triterpenoids from neem seed extracts Phytochem. Anal. 10 1999 39 43
    • (1999) Phytochem. Anal. , vol.10 , pp. 39-43
    • Jarvis, A.P.1    Morgan, E.D.2    Edwards, C.3
  • 20
    • 0023216627 scopus 로고
    • A simplified isolation procedure for azadirachtin
    • D.R. Schroeder, and K. Nakanishi A simplified isolation procedure for azadirachtin J. Nat. Prod. 50 1987 241 244
    • (1987) J. Nat. Prod. , vol.50 , pp. 241-244
    • Schroeder, D.R.1    Nakanishi, K.2
  • 21
    • 0031842108 scopus 로고    scopus 로고
    • Stability of the natural insecticide azadirachtin in aqueous and organic solvents
    • A.P. Jarvis, S. Johnson, and E.D. Morgan Stability of the natural insecticide azadirachtin in aqueous and organic solvents Pestic. Sci. 53 1998 217 222
    • (1998) Pestic. Sci. , vol.53 , pp. 217-222
    • Jarvis, A.P.1    Johnson, S.2    Morgan, E.D.3
  • 23
    • 67650163467 scopus 로고    scopus 로고
    • Preparation of a pH-sensitive affinity precipitation polymer and its application in purification of trypsin
    • H. Wang, J. Wan, and X. Cao Preparation of a pH-sensitive affinity precipitation polymer and its application in purification of trypsin Sep. Purif. Technol. 68 2009 172 177
    • (2009) Sep. Purif. Technol. , vol.68 , pp. 172-177
    • Wang, H.1    Wan, J.2    Cao, X.3
  • 24
    • 38849134903 scopus 로고    scopus 로고
    • Recovery of surfactin from fermentation broths by a hybrid salting-out and membrane filtration process
    • H.L. Chen, Y.S. Chen, and R.S. Juang Recovery of surfactin from fermentation broths by a hybrid salting-out and membrane filtration process Sep. Purif. Technol. 59 2008 244 252
    • (2008) Sep. Purif. Technol. , vol.59 , pp. 244-252
    • Chen, H.L.1    Chen, Y.S.2    Juang, R.S.3
  • 25
    • 67650104326 scopus 로고    scopus 로고
    • Optimization of salting-out crystallization for an efficient in situ separation of synthetic anthraquinone- And azo-type reactive dyes
    • J. Cho, J.K. Cho, J. Lee, D. Lee, C. Park, and S. Kim Optimization of salting-out crystallization for an efficient in situ separation of synthetic anthraquinone- And azo-type reactive dyes Sep. Purif. Technol. 68 2009 138 144
    • (2009) Sep. Purif. Technol. , vol.68 , pp. 138-144
    • Cho, J.1    Cho, J.K.2    Lee, J.3    Lee, D.4    Park, C.5    Kim, S.6
  • 26
    • 67349179129 scopus 로고    scopus 로고
    • Extraction and purification of flavanone glycosides and kaemferol glycosides from defatted Camellia oleifera seeds by salting-out using hydrophilic isopropanol
    • J.H. Chen, B.C. Liau, T.T. Jong, and C.M.J. Chang Extraction and purification of flavanone glycosides and kaemferol glycosides from defatted Camellia oleifera seeds by salting-out using hydrophilic isopropanol Sep. Purif. Technol. 67 2009 31 37
    • (2009) Sep. Purif. Technol. , vol.67 , pp. 31-37
    • Chen, J.H.1    Liau, B.C.2    Jong, T.T.3    Chang, C.M.J.4
  • 27
    • 77950942199 scopus 로고    scopus 로고
    • One step recovery of succinic acid from fermentation broths by crystallization
    • Q. Li, D. Wang, Y. Wu, W. Li, Y. Zhang, J. Xing, and Z. Su One step recovery of succinic acid from fermentation broths by crystallization Sep. Purif. Technol. 72 2010 294 300
    • (2010) Sep. Purif. Technol. , vol.72 , pp. 294-300
    • Li, Q.1    Wang, D.2    Wu, Y.3    Li, W.4    Zhang, Y.5    Xing, J.6    Su, Z.7
  • 29
    • 33746312414 scopus 로고    scopus 로고
    • Separation and purification of two isomorphic steroids by a novel extractive drowning out crystallization
    • Q. Nie, J. Wang, and Q. Yin Separation and purification of two isomorphic steroids by a novel extractive drowning out crystallization Sep. Purif. Technol. 50 2006 342 346
    • (2006) Sep. Purif. Technol. , vol.50 , pp. 342-346
    • Nie, Q.1    Wang, J.2    Yin, Q.3
  • 30
    • 10644240984 scopus 로고    scopus 로고
    • Separation and purification of stigmasterol and β-sitosterol from phytosterol mixtures by solvent crystallization method
    • W.L. Xu, Y.B. Huang, J.H. Qian, O. Sha, and Y.Q. Wang Separation and purification of stigmasterol and β-sitosterol from phytosterol mixtures by solvent crystallization method Sep. Purif. Technol. 41 2005 173 178
    • (2005) Sep. Purif. Technol. , vol.41 , pp. 173-178
    • Xu, W.L.1    Huang, Y.B.2    Qian, J.H.3    Sha, O.4    Wang, Y.Q.5
  • 31
    • 0038382990 scopus 로고    scopus 로고
    • Recovery of fumaric acid by membrane crystallization in the production of l-malic acid
    • E. Curcio, G. Di Profio, and E. Drioli Recovery of fumaric acid by membrane crystallization in the production of l-malic acid Sep. Purif. Technol. 33 2003 63 73
    • (2003) Sep. Purif. Technol. , vol.33 , pp. 63-73
    • Curcio, E.1    Di Profio, G.2    Drioli, E.3
  • 32
    • 0036868694 scopus 로고    scopus 로고
    • Colloidal aspects of precipitation processes
    • M. Kind Colloidal aspects of precipitation processes Chem. Eng. Sci. 57 2002 4287 4293
    • (2002) Chem. Eng. Sci. , vol.57 , pp. 4287-4293
    • Kind, M.1
  • 33
    • 64449087854 scopus 로고    scopus 로고
    • The effect of crystallization conditions, crystal morphology and size on pressure filtration of L-glutamic acid and an aromatic amine
    • R. Beck, A. Häkkinen, D. Malthe-Sørenssena, and J. Andreassen The effect of crystallization conditions, crystal morphology and size on pressure filtration of L-glutamic acid and an aromatic amine Sep. Purif. Technol. 66 2009 549 558
    • (2009) Sep. Purif. Technol. , vol.66 , pp. 549-558
    • Beck, R.1    Häkkinen, A.2    Malthe-Sørenssena, D.3    Andreassen, J.4
  • 35
    • 40749132449 scopus 로고    scopus 로고
    • Separation and purification of squalene from soybean oil deodorizer distillate
    • S. Gunawan, N.S. Kasim, and Y.H. Ju Separation and purification of squalene from soybean oil deodorizer distillate Sep. Purif. Technol. 60 2008 128 135
    • (2008) Sep. Purif. Technol. , vol.60 , pp. 128-135
    • Gunawan, S.1    Kasim, N.S.2    Ju, Y.H.3
  • 39
    • 0024657426 scopus 로고
    • An invited review: Van Der Waals and other cohesive forces affecting powder fluidization
    • J. Visser An invited review: Van Der Waals and other cohesive forces affecting powder fluidization Powder Technol. 58 1989 1 10
    • (1989) Powder Technol. , vol.58 , pp. 1-10
    • Visser, J.1
  • 40
    • 0004294969 scopus 로고    scopus 로고
    • fourth ed. Butterworth-Heinemann Oxford
    • J.W. Mullin Crystallization fourth ed. 2001 Butterworth-Heinemann Oxford
    • (2001) Crystallization
    • Mullin, J.W.1
  • 41
    • 0036460022 scopus 로고    scopus 로고
    • Determination of azadirachtin and fatty acid methyl esters of Azadirachta indica seeds by HPLC and GLC
    • N. Kaushik Determination of azadirachtin and fatty acid methyl esters of Azadirachta indica seeds by HPLC and GLC Anal. Bioanal. Chem. 374 2002 1199 1204
    • (2002) Anal. Bioanal. Chem. , vol.374 , pp. 1199-1204
    • Kaushik, N.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.