The effect of crystallization conditions, crystal morphology and size on pressure filtration of l-glutamic acid and an aromatic amine

Separation and Purification Technology

Volumn 66, Issue 3, 2009, Pages 549-558

  Beck, Ralf ^a   Häkkinen, Antti ^b   Malthe Sørenssen, Didrik ^a   Andreassen, Jens Petter ^a  

^a NORWEGIAN UNIVERSITY OF SCIENCE AND TECHNOLOGY   (Norway)

^b LAPPEENRANTA UNIVERSITY OF TECHNOLOGY   (Finland)

Author keywords

Compressibility; Constant pressure cake filtration; Crystallization; FBRM chord length distribution; Morphology

Indexed keywords

AROMATIC AMINES; CAKE COMPRESSIONS; CAKE RESISTANCES; CHORD LENGTHS; CONSTANT PRESSURE CAKE FILTRATION; CRYSTAL GROWTH RATES; CRYSTAL MORPHOLOGIES; CRYSTALLIZATION CONDITIONS; CRYSTALLIZATION PROCESS; FBRM CHORD LENGTH DISTRIBUTION; FILTER CAKES; FILTER CLOTHS; INDUSTRIAL CRYSTALLIZATIONS; L-GLUTAMIC ACIDS; MONOCRYSTALLINE; NEEDLE LIKES; NEEDLE-LIKE CRYSTALS; POLY-CRYSTALLINE; POLYHEDRAL PARTICLES; PRESSURE DIFFERENCES; PRESSURE FILTRATIONS; SUPERSATURATION RATIOS; SURFACE NUCLEATIONS;

AMINES; AROMATIC COMPOUNDS; COMPRESSIBILITY; CRYSTALLIZATION; GRAIN BOUNDARIES; METALLIC GLASS; MORPHOLOGY; NEEDLES; PARTICLE SIZE ANALYSIS; POROUS MATERIALS; PRESSURE EFFECTS; SUPERSATURATION;

ACID RESISTANCE;

EID: 64449087854     PISSN: 13835866     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.seppur.2009.01.018     Document Type: Article

References (29)

1. Wieckhusen D. The development of API manufacturing processes-targets and strategies. Chimia 60 (2006) 598-604
2. Mullin J.W. Crystallization. 4th edition (2001), Elsevier, Butterworth-Heinemann, Oxford, UK
3. Prymak O., Sokolova V., Peitsch T., and Epple M. The crystallization of fluoroapatite dumbbells from supersaturated aqueous solution. Crystal Growth & Design (2006) 498-506
4. Häkkinen A., Pöllänen K., Karjalainen M., Rantanen J., Louhi-Kultanen M., and Nyström L. Batch cooling crystallization and pressure filtration of sulphathiazole: the influence of solvent composition. Biotechnology and Applied Biochemistry 41 (2005) 17-28
5. R. Beck, D. Malthe-Sørenssen, J.-P. Andreassen, Polycrystalline growth in precipitation of an aromatic amine derivative and l-glutamic acid, Journal of Crystal Growth, doi:10.1016/j.jcrysgro.2008.11.029.
6. Roelands C.P.M., ter Horst J.H., Kramer H.J.M., and Jansens P.J. Precipitation mechanism of stable and metastable polymorphs of l-glutamic acid. AICHhE Journal 53 (2007) 354-362
7. Roelands C.P.M., ter Horst J.H., Kramer H.J.M., and Jansens P.J. The unexpected formation of the stable beta phase of l-glutamic acid during pH-shift precipitation. Journal of Crystal Growth 275 (2005) e1389-e1395
8. Schöll J., Bonalumi D., Vicum L., and Mazzotti M. In situ monitoring and modeling of the solvent-mediated polymorphic transformation of l-glutamic acid. Crystal Growth & Design 6 (2006) 881-891
9. Kitamura M. Polymorphism in the crystallization of l-glutamic acid. Journal of Crystal Growth 96 (1989) 541-545
10. Andreassen J.-P., Flaten E.M., Beck R., and Lewis A.E. Investigations of Spherulitic Growth in Industrial Crystallization. ISIC 17, Maastricht, The Netherlands, 14th-17th September (2008)
11. Magill J.H. Review spherulites: a personal perspective. Journal of Materials Science 36 (2001) 3143-3164
12. Braatz R.D. Advanced control of crystallization processes. Annual Reviews in Control 26 (2002) 87-99
13. Müller M., Meier U., Wieckhusen D., Beck R., Pfeffer-Hennig S., and Schneeberger R. Process development strategy to ascertain reproducible API polymorph manufacture. Crystal Growth & Design 6 (2006) 946-954
14. Liotta V., and Sabesan V. Monitoring and feedback control of supersaturation using ATR-FTIR to produce an active pharmaceutical ingredient of a desired crystal size. Organic Process Research and Development 8 (2004) 488-494
15. Flaten E., and Andreassen J.-P. The effect of mono ethylene glycol on the precipitation of calcium carbonate. 18th International Oil Field Chemistry Symposium. Geilo, Norway, 25th-28th March (2008)
16. Chen D., Tang K., Li F., and Zheng H. A simple aqueous mineralization process to synthesize tetragonal molybdate microcrystallites. Crystal Growth & Design 6 (2006) 247-252
17. Spanos N., and Koutsoukos P.G. The transformation of vaterite to calcite: effect of the conditions of the solutions in contact with the mineral phase. Journal of Crystal Growth 191 (1998) 783-790
18. R. Holdich, Fundamentals of Particle Technology, Midland Information Technology and Publishing, Shepshed, Leicestershire, UK, 2002.
19. Zogg M. Einführung in die Mechanische Verfahrenstechnik. 3rd edition (1993), Teubner
20. Wakeman R. The influence of particle properties on filtration. Separation and Purification Technology 58 (2007) 234-241
21. Benesch T., and Meier U. Modelling filtration with superimposed sedimentation. Separation and Purification Technology 35 (2004) 37-46
22. Wakeman R., and Tarleton S. Solid Liquid Separation, Principles of Industrial Filtration. 1st edition (2005), Elsevier, Oxford, GB, UK
23. Svarovsky L. Solid-Liquid Separation. 4th edition (2000), Butterworth-Heinemann, Oxford, GB, UK
24. Neubauer S., and Peuker U.A. Filtration Properties in Solvent-Water Mixtures. WFC10, Leipzig, Germany, 14th-18th April (2008)
25. Ruf A., Worlitschek J., and Mazzotti M. Modeling and experimental analysis of PSD measurements through FBRM. Particle & Particle Systems Characterization 17 (2000) 167-179
26. Togkalidou T., Braatz R., Johnson B.K., Davison O., and Andrews A. Experimental design and inferential modeling in pharmaceutical crystallization. AIChE Journal 47 (2001) 160-168
27. M. Stieß, Mechanische Verfahrenstechnik 2, Springer-Verlag, Berlin, Heidelberg, Germany, 1997.
28. Hukkanen E., and Braatz R. Measurement of particle size distribution in suspension polymerization using in situ laser backscattering. Sensors and Actuators B 96 (2003) 451-459
29. Li W., and Tiller F.M. Characterizing the super-compactibility of wastewater filter cakes. Fluid/Particle Separation Journal 16 (2004) 27-35