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1
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84986346889
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For selected examples, see D. Seebach, A.K. Beck, J. Golinski, J.N. Hay, and T. Laube Helv. Chim. Acta 1985 162 172
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Helv. Chim. Acta
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Seebach, D.1
Beck, A.K.2
Golinski, J.3
Hay, J.N.4
Laube, T.5
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2
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0035912345
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Li, X.; Yang, J.; Kozlowski, M.C. Org. Lett. 2001, 3, 1137-1140.
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Org. Lett.
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Li, X.1
Yang, J.2
Kozlowski, M.C.3
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4
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77955473809
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note
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There is one reference to 2,2′-biindoline in the literature which accomplishes its synthesis in a non-stereoselective fashion by radical dimerization of indoline - see: Naarmann, H.; Zdenek, J.; Viehe, H.G.; Beaujean, M.; Merenyi, R. German Patent DE 2,934,131, 1981. This report does not provide spectral data.
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-
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7
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1942500258
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A small quantity (5%) of the symmetrical byproduct N,N-diBoc-1,3-bis(2- allylphenyl)urea was also produced but was easily removed by crystallisation from the reaction mixture. A white byproduct from this reaction has been previously reported, however its structure was not identified - see: P.D. Knight, I. Munslow, P.N. O'Shaughnessy, and P. Scott Chem. Commun. 2004 894 895 Presumably, this is the same urea
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Knight, P.D.1
Munslow, I.2
O'Shaughnessy, P.N.3
Scott, P.4
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8
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77955467731
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note
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The ee discrepancy is in agreement with the literature in that trans olefins are dihydroxylated with higher stereochemical purity by ADmix β, see Ref. 7.
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12
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77955470544
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note
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This mixture was obtained from the inseparable cis and trans isomers formed from metathesis using Grubbs' I catalyst.
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13
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77955470621
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note
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The yields quoted were based on the quantity of each diastereomer present in the starting mixture.
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15
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20444504766
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S.T.A. Shah, K.M. Khan, H. Hussain, M.U. Anwar, M. Fecker, and W. Voelter Tetrahedron 61 2005 6652 6656
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I. Sapountzis, H. Dube, R. Lewis, N. Gommermann, and P. Knochel J. Org. Chem. 70 2005 2445 2454
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L. Boymond, M. Rottlander, G. Cahiez, and P. Knochel Angew. Chem., Int. Ed. 37 1998 1701 1703
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0001514892
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S.K. Taylor, D.L. Clark, K.J. Heinz, S.B. Schramm, C.D. Westermann, and K.K. Barnell J. Org. Chem. 48 1983 592 596
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