A simple and efficient protocol for large-scale preparation of three flavonoids from the flower of Daphne genkwa by combination of macroporous resin and counter-current chromatography

Journal of Separation Science

Volumn 33, Issue 14, 2010, Pages 2168-2175

  Li, Ying Nan ^a   Yin, Lian Hong ^a   Xu, Li Na ^a   Peng, Jin Yong ^a  

^a DALIAN MEDICAL UNIVERSITY   (China)

Author keywords

Counter current chromatography; Daphne genkwa; Macroporous resin; Preparative chromatography

Indexed keywords

ADSORPTION; DESORPTION; ESTERS; ETHANOL; HEXANE; METHANOL; ORGANIC SOLVENTS; RESINS;

AQUEOUS ETHANOL; CHEMICAL STRUCTURE; CHINESE MEDICINAL HERBS; COUNTERCURRENT CHROMATOGRAPHY; CRUDE EXTRACT; DESORPTION TESTS; ETHYL ACETATES; FLAVONOIDS; LARGE SCALE PREPARATION; MACROPOROUS RESIN; METHANOL-WATER; N-HEXANE; PREPARATIVE CHROMATOGRAPHY; PREPARATIVE SEPARATION; SOLVENT SYSTEM; UV- AND;

COLUMN CHROMATOGRAPHY;

3 HYDROXY GENKWANIN; APIGENMIN; FLAVONOID; GENKWANIN; PLANT MEDICINAL PRODUCT; RESIN; UNCLASSIFIED DRUG; SOLVENT;

ADSORPTION; ARTICLE; CHEMICAL STRUCTURE; CHINESE MEDICINE; COLUMN CHROMATOGRAPHY; COUNTER CURRENT CHROMATOGRAPHY; DAPHNE; DAPHNE GENKWA; DESORPTION; FLOWER; HERB; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MACROPOROUS RESIN COLUMN CHROMATOGRAPHY; MASS SPECTROMETRY; MEDICINAL PLANT; PRIORITY JOURNAL; PURIFICATION; CHEMISTRY; CHROMATOGRAPHY; DEVICES; EVALUATION STUDY; ISOLATION AND PURIFICATION; PROCEDURES;

CHROMATOGRAPHY; COUNTERCURRENT DISTRIBUTION; DAPHNE; FLAVONOIDS; MEDICINE, CHINESE TRADITIONAL; MOLECULAR STRUCTURE; PLANTS, MEDICINAL; SOLVENTS;

EID: 77954972915     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201000054     Document Type: Article

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