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77954215600
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note
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- 1): 3446(s), 1617(s), 1575(s), 1528(m), 1487(m), 1452(s), 1380(s), 1244(w), 1124(w), 967(w), 917(w), 808(w), 788(w), 774(w), 736(w), 472(w).
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24
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77954217339
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note
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3, Z = 2, F(000) = 1192, GOF = 1.078, R1 = 0.0506, wR2 = 0.1232 [I > 2r(I)]. Structural data for 1 was collected on a Bruker Smart Apex CCD with graphite monochromated Mo Kα radiation (λ = 0.71073 Å) at 273 K. The structure was solved by direct methods and refined with the fullmatrix least-squares technique using the SHELXS-97 and SHELXL-97 programs.
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