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Inorganic Chemistry Communications

Volumn 13, Issue 8, 2010, Pages 932-934

A new 2D 5-connected coordination polymer based on 3,4-bis(pyridin-4-ylmethoxy)benzoic acid ligand

(6) Xu, Guang Juan a Zhao, Ya Hui a Shao, Kui Zhan a Lan, Ya Qian a Li, Peng a Su, Zhong Min a

a NORTHEAST NORMAL UNIVERSITY (China)

Author keywords

3,4 bis(pyridin 4 ylmethoxy)benzoic acid; Coordination polymer; Crystal structure; Photoluminescent property

Indexed keywords

EID: 77953869708 PISSN: 13877003 EISSN: None Source Type: Journal
DOI: 10.1016/j.inoche.2010.04.029 Document Type: Article

Times cited : (5)

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- Syntheses: The ligand of HL2 was synthesized readily by the procedure reported in the literature [35,36, All chemicals were commercially available and used as received without further purification. The compound was synthesized by the following method: Zn(NO3)2·6H2O (0.089 g, 0.30 mmol, HL2 (0.033 g, 0.10 mmol, 1,4-H2bdc (0.050 g, 0.30 mmol) and NaOH (0.24 g, 0.60 mmol) in H2O (14 mL) was sealed in a 25 mL Teflon-lined stainless steel container, which was heated at 150 °C for 3 days and then cooled down to room temperature at a rate of 10 °C h-1. Colorless crystals of 1 were collected and washed with distilled water and dried in air to give the product; yield, 45.4, based on ZnII salts, Elemental analyses calcd, ) for C43H28N2O16Zn3 1024.78, C, 50.39; H, 2.76; N, 2.73. Found C, 50.41; H, 2.73; N, 2.75
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- 2 = 0.1621 (all data) and S = 1.038. Data were collected on a Bruker ApexII CCD diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å). The structure was solved with direct methods and refined with full-matrix least-squares (SHELX-97). Selected bond lengths (Å) and angles (°) for compound 1 are listed in Table S1, Supporting information.

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