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Volumn 12, Issue 12, 2010, Pages 2818-2821

Synthesis of taurospongin A

Author keywords

[No Author keywords available]

Indexed keywords

ALKENE; ALKYNE; TAUROSPONGIN A;

EID: 77953566270     PISSN: 15237060     EISSN: 15237052     Source Type: Journal    
DOI: 10.1021/ol100906k     Document Type: Article
Times cited : (10)

References (32)
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    • Total syntheses
    • Total syntheses
  • 6
    • 77953571245 scopus 로고    scopus 로고
    • Formal syntheses
    • Formal syntheses
  • 16
    • 9644292316 scopus 로고
    • For example: borohydride reduction of the cyclic sulfite/sulfate
    • For example: borohydride reduction of the cyclic sulfite/sulfate: Gao, Y.; Sharpless, K. B. J. Am. Chem. Soc. 1988, 110, 7538-7539
    • (1988) J. Am. Chem. Soc. , vol.110 , pp. 7538-7539
    • Gao, Y.1    Sharpless, K.B.2
  • 19
    • 0000676113 scopus 로고
    • Reduction of the α-mesylate: [Na(Hg)]
    • Reduction of the α-mesylate: [Na(Hg)]: Stork, G.; Rychnovsky, S. D. J. Am. Chem. Soc. 1987, 109, 1564-1565
    • (1987) J. Am. Chem. Soc. , vol.109 , pp. 1564-1565
    • Stork, G.1    Rychnovsky, S.D.2
  • 23
    • 77953547553 scopus 로고    scopus 로고
    • 2O; (c) TsCl, pyridine; (d) LiBr, acetone (38% overall); step (d) has to be performed with care to avoid alkene isomerization and loss of the volatile product during isolation
    • 2O; (c) TsCl, pyridine; (d) LiBr, acetone (38% overall); step (d) has to be performed with care to avoid alkene isomerization and loss of the volatile product during isolation.
  • 28
    • 77953547854 scopus 로고    scopus 로고
    • We are very grateful to Professor Tietze and his group for their invaluable advice in relation to this procedure
    • We are very grateful to Professor Tietze and his group for their invaluable advice in relation to this procedure.
  • 29
    • 77953595191 scopus 로고    scopus 로고
    • 13C NMR spectrum for 17 were doubled, including that at 34.6 ppm, which was sensitive to stereochemical change (34.4 ppm in the adduct generated using the (S)-configured auxiliary)
    • 13C NMR spectrum for 17 were doubled, including that at 34.6 ppm, which was sensitive to stereochemical change (34.4 ppm in the adduct generated using the (S)-configured auxiliary).
  • 30
    • 77953551498 scopus 로고    scopus 로고
    • We will report further details in a full description of this work
    • We will report further details in a full description of this work.
  • 32
    • 77953579874 scopus 로고    scopus 로고
    • Chemistry Part II Thesis, Oxford
    • Reynolds, L. Chemistry Part II Thesis, Oxford, 2008.
    • (2008)
    • Reynolds, L.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.