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1
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0030742636
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Ishiyama, H.; Ishibashi, M.; Ogawa, A.; Yoshida, S.; Kobayashi, J. J. Org. Chem. 1997, 62, 3831-3836.
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Ishiyama, H.1
Ishibashi, M.2
Ogawa, A.3
Yoshida, S.4
Kobayashi, J.5
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2
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0030860279
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Tokunaga, M.; Larrow, J. F.; Kakiuchi, F.; Jacobsen, E. N. Science 1997, 277, 936-938.
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Tokunaga, M.1
Larrow, J.F.2
Kakiuchi, F.3
Jacobsen, E.N.4
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3
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0029757771
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(a) Larrow, J. F.; Schaus, S. E.; Jacobsen, E. N. J. Am. Chem. Soc. 1996, 118, 7420-7421.
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Larrow, J.F.1
Schaus, S.E.2
Jacobsen, E.N.3
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5
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0345664754
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(c) Martinez, L. E.; Leighton, J. L.; Carsten, D. H.; Jacobsen, E. N. J. Am. Chem. Soc. 1995, 117, 5897-5898.
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Martinez, L.E.1
Leighton, J.L.2
Carsten, D.H.3
Jacobsen, E.N.4
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6
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20644454724
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-
note
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Racemic epoxide 5 was prepared in two steps and 85% yield from commercially available 3-methyl-3-buten-1-ol (see the Supporting Information).
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-
-
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7
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-
0032576854
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For selected examples of kinetic resolution of 2,2-disubstituted epoxides, see: (a) Orru, R. V. A.; Mayer, S. F.; Kroutil, W.; Faber, K. Tetrahedron 1998, 54, 859-874. (b) Osprian, I.; Kroutil, W.; Mischitz, M.; Faber, K. Tetrahedron: Asymmetry 1997, 8, 65-71. (c) Lakner, F. J.; Hager, L. P. J. Org. Chem. 1996, 61, 3923-3925.
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(1998)
Tetrahedron
, vol.54
, pp. 859-874
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Orru, R.V.A.1
Mayer, S.F.2
Kroutil, W.3
Faber, K.4
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8
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-
0031016293
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-
For selected examples of kinetic resolution of 2,2-disubstituted epoxides, see: (a) Orru, R. V. A.; Mayer, S. F.; Kroutil, W.; Faber, K. Tetrahedron 1998, 54, 859-874. (b) Osprian, I.; Kroutil, W.; Mischitz, M.; Faber, K. Tetrahedron: Asymmetry 1997, 8, 65-71. (c) Lakner, F. J.; Hager, L. P. J. Org. Chem. 1996, 61, 3923-3925.
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(1997)
Tetrahedron: Asymmetry
, vol.8
, pp. 65-71
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Osprian, I.1
Kroutil, W.2
Mischitz, M.3
Faber, K.4
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9
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-
0029941844
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-
For selected examples of kinetic resolution of 2,2-disubstituted epoxides, see: (a) Orru, R. V. A.; Mayer, S. F.; Kroutil, W.; Faber, K. Tetrahedron 1998, 54, 859-874. (b) Osprian, I.; Kroutil, W.; Mischitz, M.; Faber, K. Tetrahedron: Asymmetry 1997, 8, 65-71. (c) Lakner, F. J.; Hager, L. P. J. Org. Chem. 1996, 61, 3923-3925.
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(1996)
J. Org. Chem.
, vol.61
, pp. 3923-3925
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Lakner, F.J.1
Hager, L.P.2
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10
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-
0001384657
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-
The stereochemical assignment was made by comparison with literature data: Gill, M.; Smrdel, A. F. Tetrahedron: Asymmetry 1990, 1, 453-464.
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(1990)
Tetrahedron: Asymmetry
, vol.1
, pp. 453-464
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Gill, M.1
Smrdel, A.F.2
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12
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0025766920
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(a) Kitamura, M.; Tokunaga, M.; Ohkuma, T.; Noyori, R. Tetrahedron Lett. 1991, 32, 4163-4166.
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, pp. 4163-4166
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Kitamura, M.1
Tokunaga, M.2
Ohkuma, T.3
Noyori, R.4
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13
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0002166035
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(b) Kitamura, M.; Tokunaga, M.; Ohkuma, T.; Noyori, R. Org. Synth. 1992, 71, 1-13.
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Org. Synth.
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Kitamura, M.1
Tokunaga, M.2
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Noyori, R.4
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14
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0029084414
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Williams, J. M.; Jobson, R. B.; Yasuda, N.; Marchesini, G.; Dolling, U. H.; Grabowski, E. J. J. Tetrahedron Lett. 1995, 36, 5461-5464.
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Williams, J.M.1
Jobson, R.B.2
Yasuda, N.3
Marchesini, G.4
Dolling, U.H.5
Grabowski, E.J.J.6
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15
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20644440685
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note
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The starting terminal alkyne 9 was also recovered in 24% yield.
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-
-
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16
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0001164834
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For selected examples of diastereoselective reduction of β-alkoxy ketones to give syn-1,3-monoprotected diols, see: (a) Mori, Y.; Kuhara, M.; Takeuchi, A.; Suzuki, M. Tetrahedron Lett. 1988, 29, 5419-5422. (b) Yamazaki, N.; Kibayashi, C. J. Am. Chem. Soc. 1989, 111, 1396-1408. (c) Yoshimatsu, M.; Naito, M.; Shimizu, H.; Muraoka, O.; Tanabe, G.; Kataoka, T. J. Org. Chem. 1996, 61, 8200-8206.
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Mori, Y.1
Kuhara, M.2
Takeuchi, A.3
Suzuki, M.4
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17
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0000346930
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For selected examples of diastereoselective reduction of β-alkoxy ketones to give syn-1,3-monoprotected diols, see: (a) Mori, Y.; Kuhara, M.; Takeuchi, A.; Suzuki, M. Tetrahedron Lett. 1988, 29, 5419-5422. (b) Yamazaki, N.; Kibayashi, C. J. Am. Chem. Soc. 1989, 111, 1396-1408. (c) Yoshimatsu, M.; Naito, M.; Shimizu, H.; Muraoka, O.; Tanabe, G.; Kataoka, T. J. Org. Chem. 1996, 61, 8200-8206.
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J. Am. Chem. Soc.
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Yamazaki, N.1
Kibayashi, C.2
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18
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0029824648
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For selected examples of diastereoselective reduction of β-alkoxy ketones to give syn-1,3-monoprotected diols, see: (a) Mori, Y.; Kuhara, M.; Takeuchi, A.; Suzuki, M. Tetrahedron Lett. 1988, 29, 5419-5422. (b) Yamazaki, N.; Kibayashi, C. J. Am. Chem. Soc. 1989, 111, 1396-1408. (c) Yoshimatsu, M.; Naito, M.; Shimizu, H.; Muraoka, O.; Tanabe, G.; Kataoka, T. J. Org. Chem. 1996, 61, 8200-8206.
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Yoshimatsu, M.1
Naito, M.2
Shimizu, H.3
Muraoka, O.4
Tanabe, G.5
Kataoka, T.6
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19
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0030883527
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Matsumura, K.; Hashiguchi, S.; Ikariya, T.; Noyori, R. J. Am. Chem. Soc. 1997, 119, 8738-8739.
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Matsumura, K.1
Hashiguchi, S.2
Ikariya, T.3
Noyori, R.4
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20
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20644459560
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note
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1H NMR spectrum. Both diastereoisomers were separable by flash chromatography.
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21
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33845282179
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Anelli, P. L.; Biffi, C.; Montanari, F.; Quici, S. J. Org. Chem. 1987, 52, 2559-2562.
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Anelli, P.L.1
Biffi, C.2
Montanari, F.3
Quici, S.4
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