Development and optimization of a method for the separation of platycosides in Platycodi Radix by comprehensive two-dimensional liquid chromatography with mass spectrometric detection

Journal of Chromatography A

Volumn 1217, Issue 26, 2010, Pages 4375-4382

  Jeong, Eun Kyung ^a,b   Cha, Hyun Jeong ^a   Ha, Young Wan ^c   Kim, Yeong Shik ^d   Ha, In Jin ^d   Na, Yun Cheol ^a  

^a Korea Basic Science Institute (KBSI)   (South Korea)

^b Kyung Hee University   (South Korea)

^c Korea Institute of Science and Technology   (South Korea)

^d Seoul National University   (South Korea)

Author keywords

Comprehensive 2D LC; Orthogonality; Peak capacity; Platycoside

Indexed keywords

COMPREHENSIVE TWO-DIMENSIONAL CHROMATOGRAPHY; COMPREHENSIVE TWO-DIMENSIONAL LIQUID CHROMATOGRAPHY; CORRELATION COEFFICIENT; ELECTROSPRAYS; MASS SPECTROMETRIC DETECTION; MINOR COMPONENTS; ORTHOGONALITY; PEAK CAPACITY; RETENTION TIME; ROOT EXTRACTS; SEPARATION PERFORMANCE; TWO DIMENSIONAL SPACES;

ISOMERS; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

TWO DIMENSIONAL;

2 O ACETYL PLATYCODIN D; 2 O ACETYL POLYGALACIN D; 2 O ACETYL POLYGALACIN D3; 3 O ACETYL PLATYCODIN D; 3 O ACETYL POLYGALACIN D3; AMMONIA; DEAPI 2 O ACETYL POLYGALACIN D; DEAPI 2 O ACETYL POLYGALACIN D2; DEAPI 2 O ACETYL POLYGALACIN D3; DEAPI 3 O ACETYL PLATYCODIN D; DEAPI 3 O ACETYL POLYGALACIN D2; DEAPI 3 O ACETYL POLYGALACIN D3; DEAPI PLATYCODIN D; DEAPI PLATYCODIN D3; DEAPI PLATYCOSIDE E; DEAPI POLYGALACIN D3; DEAPI POLYGALACIN E; DEXYL 2 O ACETYL POLYGALACIN D3; DEXYL 3 O ACETYL POLYGALACIN D3; PLANT EXTRACT; PLATYCODIN; PLATYCODIN A; PLATYCODIN D3; PLATYCOSIDE DERIVATIVE; PLATYCOSIDE E; POLYGALACIN D; POLYGALACIN D2; UNCLASSIFIED DRUG;

ARTICLE; COMPREHENSIVE TWO DIMENSIONAL LIQUID CHROMATOGRAPHY; CONTROLLED STUDY; CORRELATION COEFFICIENT; DRUG DETERMINATION; ELECTROSPRAY MASS SPECTROMETRY; INTERMETHOD COMPARISON; LIQUID CHROMATOGRAPHY; NONHUMAN; PLANT ROOT; PLATYCODON; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; SEPARATION TECHNIQUE;

CAMPANULACEAE; CHROMATOGRAPHY, LIQUID; GLYCOSIDES; PLANT EXTRACTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

EID: 77953535023     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.04.053     Document Type: Article

References (58)

1. Takagi K., Lee E.B. Yakugaku Zasshi 1972, 92:951.
2. Lee E.B. Yakugaku Zasshi 1973, 93:1188.
3. Kim K.S., Ezaki O., Ikemoto S., Itakura H. J. Nutr. Sci. Vitaminol. 1995, 41:485.
4. Han L.K., Xu B.J., Kimura Y., Zheng Y., Okuda H. J. Nutr. 2000, 130:2760.
5. Kim K.S., Seo E.K., Lee Y.C., Lee T.K., Cho Y.W., Ezaki O., Kim C.H. J. Nutr. Biochem. 2000, 11:420.
6. Choi C.Y., Kim J.Y., Kim Y.S., Chung Y.C., Hahm K.S., Jeong H.G. Cancer Lett. 2001, 166:17.
7. Choi C.Y., Kim J.Y., Kim Y.S., Chung Y.C., Seo J.K., Jeong H.G. Int. Immunopharmacol. 2001, 1:1141.
8. Lee K.J., Jeong H.G. Food Chem. Toxicol. 2002, 40:517.
9. Park D.I., Lee J.H., Moon S.K., Kim C.H., Lee Y.T., Cheong J., Choi B.T., Choi Y.H. Pharmacol. Res. 2005, 51:437.
10. Higashi A., Arimoto K., Iwata Y., Ujita K., Kawai T., Kobayashi Y., Sakurai K., Shimada Y., Takagi A., Taniyama T., Nakajima K., Hisata Y., Hosoda K., Yamamoto K., Yamamoto Y., Noguchi M. Nat. Med. 1997, 51:56.
11. Piao H.S., Kang C.H., Kim H.C., Ahn D.K. J. Orient. Med. 1998, 3:125.
12. Saeki T., Koike K., Nikaido T. Planta Med. 1999, 65:428.
13. Xu B.J., Xu C.L., Cui M., Liu M.X., Zheng Y.N. J. Jilin Agric. Univ. 1999, 21:35.
14. Xu C.L., Zheng Y.N., Tang L.H., Liu M.X., Xu B.J. J. Jilin Agric. Univ. 2001, 23:58.
15. Chung J.H., Shin P.G., Ryu J.C., Jang D.S., Cho S.H. Agric. Chem. Biotechnol. 1997, 40:152.
16. Kim G.S., Kim H.T., Seong J.D., Park H.S., Kim S.D. Korean J. Med. Crop Sci. 2002, 10:200.
17. Ha Y.W., Na Y.C., Seo J.J., Kim S.N., Linhardt R.J., Kim Y.S. J. Chromatogr. A 2006, 1135:27.
18. Na Y.C., Ha Y.W., Kim W.S., Kim K.J. J. Chromatogr. A 2008, 1189:467.
19. Giddings J.C. Anal. Chem. 1967, 39:1027.
20. Giddings J.C. J. Chromatogr. A 1995, 703:3.
21. Pasch H., Brinkmann C., Much H., Just U. J. Chromatogr. 1992, 623:315.
22. Van Doremaele G.H.J., Geerts F.H.J.M., Aan de Meulen L.J., German A.L. Polymer 1992, 33:1512.
23. Brinkman U.A.Th. J. Chromatogr. A 1994, 665:217.
24. Bushey M.M., Jorgenson J.W. Anal. Chem. 1990, 62:161.
25. Moore A.W., Jorgenson J.W. Anal. Chem. 1995, 67:3456.
26. Holland H.A., Jorgenson J.W. Anal. Chem. 1995, 67:3275.
27. Stronik T., Ortiz M.C., Bult A., Lingeman H., de Jong G.J., Underburg W.J.M. J. Chromatogr. B 2005, 817:49.
28. Wagner K., Miliotis T., Marko-Varge G., Bischoff R., Unger K.K. Anal. Chem. 2002, 74:809.
29. van der Horst A., Schoenmakers P.J. J. Chromatogr. A 2003, 1000:693.
30. Murphy R.E., Schure M.R., Foley J.P. Anal. Chem. 1998, 70:1585.
31. Ma S., Chen L.X., Luo G.A., Ren K.N., Wu J.F., Wang Y.M. J. Chromatogr. A 2006, 1127:207.
32. Jandera P., Fischer J., Lahovska H., Novotna K., Cesla P., Kolarova L. J. Chromatogr. A 2006, 1119:3.
33. Dugo P., Kumm T., Crupi M.L., Cotroneo A., Mondello L. J. Chromatogr. A 2006, 1112:269.
34. Francois I., Sandra K., Sandra P. Anal. Chim. Acta 2009, 641:14.
35. Dugo P., Cacciola F., Kumm T., Dugo G., Mondello L. J. Chromatogr. A 2008, 1184:353.
36. Stoll D.R., Li X., Wang X., Carr P.W., Porter S.E.G., Rutan S.C. J. Chromatogr. A 2007, 1168:3.
37. Jandera P. J. Sep. Sci. 2006, 29:1763.
38. Mayfield K.J., Shaliker R.A., Catchpoole H.J., Sweeney A.P., Wong V., Guiochon G. J. Chromatogr. A 2005, 1080:124.
39. Xu B.J., Zheng Y.N., Sung C.K. Nat. Prod. Sci. 2004, 10:141.
40. Xu B.J., Zheng Y.N., Cui M., Song F.R. Chin. J. Med. Chem. 2000, 10:193.
41. Seeley J.V. J. Chromatogr. A 2002, 962:21.
42. Horie K., Kimura H., Ikegami T., Iwatsuka A., Saad N., Fiehn O., Tanaka N. Anal. Chem. 2007, 79:3764.
43. Davis J.M., Stoll D.R., Carr P.W. Anal. Chem. 2008, 80:461.
44. Davis J.M., Stoll D.R., Carr P.W. Anal. Chem. 2008, 80:8122.
45. Li X., Stoll D.R., Carr P.W. Anal. Chem. 2009, 81:845.
46. Davis J.M. J. Sep. Sci. 2005, 28:347.
47. Dugo P., Favoino O., Luppino R., Dugo G., Mondello L. Anal. Chem. 2004, 76:2525.
48. Dugo P., Fernandez M.D., Cotroneo A., Dugo G., Mondello L. J. Chromatogr. Sci. 2006, 44:561.
49. Dugo P., Skerikova V., Kumm T., Trozzi A., Jandera P., Mondello L. Anal. Chem. 2006, 78:7743.
50. Liu Z., Patterson D.G., Lee M.L. Anal. Chem. 1995, 67:3840.
51. Slonecker P.J., Li X., Ridgway T.H., Dorsey J.G. Anal. Chem. 1996, 68:682.
52. Jandera P. LC-GC Eur. 2007, 20:510.
53. Gray M.J., Sweeney A.P., Dennis G.R., Slonecker P.J., Shalliker R.A. Analyst 2003, 128:598.
54. Gray M.J., Dennis G.R., Slonecker P.J., Shalliker R.A. J. Chromatogr. A 2003, 1015:89.
55. Gray M.J., Dennis G.R., Slonecker P.J., Shalliker R.A. J. Chromatogr. A 2004, 1041:101.
56. Gilar M., Olivova P., Daly A.E., Gebler J.C. Anal. Chem. 2005, 77:6426.
57. Watson N.E., Davis J.M., Synovec R.E. Anal. Chem. 2007, 79:7924.
58. Zhao H.L., Sim J.S., Shim S.J., Ha Y.W., Kang S.S., Kim Y.S. Int. J. Obes. (Lond.) 2005, 29:983.