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34
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77952108491
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-
note
-
2]/18-crown-6 associate (1): the yellow crystals of 1 were obtained by a slow crystallization of the equimolar mixture of the complex [10] and 18-crown-6 from an acetone:chloroform (1:1, v/v) solution at 20-25 °C.
-
-
-
-
35
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77952107186
-
-
note
-
2] [11] was co-crystallized with 18-crown-6 in a ratio 1:1 from an acetone:p-xylene (4:1, v/v) solution at 20-25 °C.
-
-
-
-
36
-
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77952104426
-
-
note
-
3, 300 MHz): δ (ppm) = 1.35 (t, 7.5 Hz, 3H), 3.13 (quart, 7.5 Hz, 2H), 3.78 (s, 3H), 7.73 (s, br, 1H) [13].
-
-
-
-
37
-
-
77952103581
-
-
note
-
3, 300 MHz): δ (ppm) = 1.23 (t, 7.5 Hz, 3H), 3.13 (quart, 7.5 Hz, 2H), 3.96 (s, 3H), 6.86 (s, br, 1H) [13].
-
-
-
-
39
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0037156167
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Bokach N.A., Kuznetsov M.L., Garnovskii D.A., Natile G., Kukushkin V.Yu., and Pombeiro A.J.L. Inorg. Chem. 41 (2002) 2041
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Inorg. Chem.
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Bokach, N.A.1
Kuznetsov, M.L.2
Garnovskii, D.A.3
Natile, G.4
Kukushkin, V.Yu.5
Pombeiro, A.J.L.6
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40
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0037764732
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Bokach N.A., Kukushkin V.Yu., Haukka M., Fraústo da Silva J.J.R., and Pombeiro A.J.L. Inorg. Chem. 42 (2003) 3602
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Bokach, N.A.1
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Pombeiro, A.J.L.5
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41
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77952104160
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note
-
1H NMR spectra were measured on a Bruker AMX 300 spectrometer at ambient temperature using chloroform as the reference standard (7.25 ppm).
-
-
-
-
42
-
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77952106065
-
-
note
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eq(parent atom). Deposited Data: CCDC 757137.
-
-
-
-
43
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77952103287
-
-
note
-
The X-ray diffraction data were collected on a Nonius KappaCCD diffractometer using Mo Kα radiation (λ = 0.71073 Å). The Denzo-Scalepack [16] or EvalCCD [17] program packages were used for cell refinements and data reductions. The structure was solved by direct methods using the SIR2004 [18] or SHELXS-97 [19] with the WinGX [20] graphical user interface. An empirical absorption correction (SORTAV [21] or SADABS [22]) was applied to the data. Structural refinements were carried out using SHELXL-97 [19].
-
-
-
-
44
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0031059866
-
Processing of X-ray diffraction data collected in oscillation mode
-
Sweet R.M. (Ed). Carter Jr. C.W. (Ed), Academic Press, New York
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Otwinowski Z., and Minor W. Processing of X-ray diffraction data collected in oscillation mode. In: Sweet R.M. (Ed). In: Carter Jr. C.W. (Ed). Methods in Enzymology, Macromolecular Crystallography, Part A 276 (1997), Academic Press, New York 307
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Otwinowski, Z.1
Minor, W.2
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46
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16844363448
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Burla M.C., Camalli M., Carrozzini B., Cascarano G.L., Giacovazzo C., Polidori G., and Spagna R. J. Appl. Crystallogr. 38 (2005) 381
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Giacovazzo, C.5
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Spagna, R.7
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50
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0242590609
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Bruker AXS, Inc., Madison, WI
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Sheldrick G.M. SADABS-Bruker Nonius Scaling and Absorption Correction, version 2.10 (2003), Bruker AXS, Inc., Madison, WI
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(2003)
SADABS-Bruker Nonius Scaling and Absorption Correction, version 2.10
-
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Sheldrick, G.M.1
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51
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77952102065
-
-
note
-
eq(parent atom). Deposited Data: CCDC 757138.
-
-
-
-
52
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22544474986
-
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Bokach N.A., Kuznetsova T.V., Simanova S.A., Haukka M., Pombeiro A.J.L., and Kukushkin V.Yu. Inorg. Chem. 44 (2005) 5152
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Bokach, N.A.1
Kuznetsova, T.V.2
Simanova, S.A.3
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Pombeiro, A.J.L.5
Kukushkin, V.Yu.6
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