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Volumn 13, Issue 5, 2010, Pages 580-583

18-Crown-6 as a linker for (imino ester)2Pt centers providing their assembly into 1D arrays via hydrogen bonding

Author keywords

18 Crown 6; 1D arrays; Imino ester ligand; Platinum; Supramolecular chemistry

Indexed keywords


EID: 77952103243     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.02.008     Document Type: Article
Times cited : (9)

References (53)
  • 34
    • 77952108491 scopus 로고    scopus 로고
    • note
    • 2]/18-crown-6 associate (1): the yellow crystals of 1 were obtained by a slow crystallization of the equimolar mixture of the complex [10] and 18-crown-6 from an acetone:chloroform (1:1, v/v) solution at 20-25 °C.
  • 35
    • 77952107186 scopus 로고    scopus 로고
    • note
    • 2] [11] was co-crystallized with 18-crown-6 in a ratio 1:1 from an acetone:p-xylene (4:1, v/v) solution at 20-25 °C.
  • 36
    • 77952104426 scopus 로고    scopus 로고
    • note
    • 3, 300 MHz): δ (ppm) = 1.35 (t, 7.5 Hz, 3H), 3.13 (quart, 7.5 Hz, 2H), 3.78 (s, 3H), 7.73 (s, br, 1H) [13].
  • 37
    • 77952103581 scopus 로고    scopus 로고
    • note
    • 3, 300 MHz): δ (ppm) = 1.23 (t, 7.5 Hz, 3H), 3.13 (quart, 7.5 Hz, 2H), 3.96 (s, 3H), 6.86 (s, br, 1H) [13].
  • 41
    • 77952104160 scopus 로고    scopus 로고
    • note
    • 1H NMR spectra were measured on a Bruker AMX 300 spectrometer at ambient temperature using chloroform as the reference standard (7.25 ppm).
  • 42
    • 77952106065 scopus 로고    scopus 로고
    • note
    • eq(parent atom). Deposited Data: CCDC 757137.
  • 43
    • 77952103287 scopus 로고    scopus 로고
    • note
    • The X-ray diffraction data were collected on a Nonius KappaCCD diffractometer using Mo Kα radiation (λ = 0.71073 Å). The Denzo-Scalepack [16] or EvalCCD [17] program packages were used for cell refinements and data reductions. The structure was solved by direct methods using the SIR2004 [18] or SHELXS-97 [19] with the WinGX [20] graphical user interface. An empirical absorption correction (SORTAV [21] or SADABS [22]) was applied to the data. Structural refinements were carried out using SHELXL-97 [19].
  • 44
    • 0031059866 scopus 로고    scopus 로고
    • Processing of X-ray diffraction data collected in oscillation mode
    • Sweet R.M. (Ed). Carter Jr. C.W. (Ed), Academic Press, New York
    • Otwinowski Z., and Minor W. Processing of X-ray diffraction data collected in oscillation mode. In: Sweet R.M. (Ed). In: Carter Jr. C.W. (Ed). Methods in Enzymology, Macromolecular Crystallography, Part A 276 (1997), Academic Press, New York 307
    • (1997) Methods in Enzymology, Macromolecular Crystallography, Part A , vol.276 , pp. 307
    • Otwinowski, Z.1    Minor, W.2
  • 51
    • 77952102065 scopus 로고    scopus 로고
    • note
    • eq(parent atom). Deposited Data: CCDC 757138.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.