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Volumn 13, Issue 5, 2010, Pages 683-685

Capturing copper(II) ions using {Cu(tpy)(bpy)} domains

Author keywords

Copper; Crystal structure; Helicate; Heterocycle; Oligopyridine

Indexed keywords

EID: 77952101629 PISSN: 13877003 EISSN: None Source Type: Journal
DOI: 10.1016/j.inoche.2010.03.019 Document Type: Article

Times cited : (9)

References (23)

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20
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- Ligand 2 (34.2 mg, 0.101 mmol, tpy (46.9 mg, 0.201 mmol, Cu(NO3)2.3H2O (48.5 mg, 0.201 mmol) and NH4PF6 (163 mg, 1.00 mmol) were dissolved in MeCN (10 cm3) and H2O (10 cm3) while the solvent mixture was being heated. The reaction mixture was heated at reflux for 5 min, and was then left open to the air at room temperature overnight. The viscous blue oil that formed was dissolved in MeCN/CH2Cl2 (10 cm3, washed with water (2 × 10 cm3, and dried over MgSO4.Removal of solvent yielded a blue powder which was dissolved in MeCN. Crystals of [Cu2(tpy)2(2, PF6]4 and [Cu(tpy)2, PF6]2 were grown by diffusion of Et2O into the MeCN solution
- 2O into the MeCN solution.

21
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- Cu2(tpy)2(2, PF6]4·2H2O: C52H33Cu2F24N10O2P4, M, 1547.96, blue block, tetragonal, space group P43212, a, b, 16.636(2, c, 25.956(5) Å, U, 7183.5(18) Å3, Z, 4, Dc, 1.428 Mg m-3, μ(Mo-Kα)=0.786 mm-1, T, 223(2) K. Total 203376 reflections, 8231 unique, Rint, 0.0661. Refinement of 7816 reflections (574 parameters) with I > 2σ (I) converged at final R1, 0.0564 (R1 all data, 0.0588, wR2, 0.1572 wR2 all data, 0.1597, gof, 1.171
- int = 0.0661. Refinement of 7816 reflections (574 parameters) with I > 2σ (I) converged at final R1 = 0.0564 (R1 all data = 0.0588), wR2 = 0.1572 (wR2 all data = 0.1597), gof = 1.171.

22
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- Cu(tpy)(2, PF6]2·MeCN: C39H32CuF12N8P2, M, 966.22, blue block, monoclinic, space group P21/n, a, 12.301(3, b, 25.999(5, c, 12.690(3) Å, β, 97.25(3)°, U, 4026.0(16) Å3, Z, 4, Dc, 1.594 Mg m-3, μ(Mo-Kα)=0.720 mm-1, T, 223(2) K. Total 82564 reflections, 10173 unique, Rint, 0.0827. Refinement of 9189 reflections (636 parameters) with I > 2σ (I) converged at final R1, 0.0461 (R1 all data, 0.0509, wR2, 0.1228 wR2 all data, 0.1269, gof, 1.059
- int = 0.0827. Refinement of 9189 reflections (636 parameters) with I > 2σ (I) converged at final R1 = 0.0461 (R1 all data = 0.0509), wR2 = 0.1228 (wR2 all data = 0.1269), gof = 1.059.

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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.