Closed-loop control of reactive crystallization. Part I: Supersaturation-controlled crystallization of L-glutamic acid

Chemical Engineering and Technology

Volumn 33, Issue 5, 2010, Pages 743-750

  Alatalo, Hannu M ^a   Hatakka, Henry ^a   Louhi Kultanen, Marjatta ^a   Kohonen, Jarno ^a   Reinikainen, Satu Pia ^a  

^a LAPPEENRANTA UNIVERSITY OF TECHNOLOGY   (Finland)

Author keywords

Closed loop control; Crystallization; L glutamic acid; Supersaturation

Indexed keywords

ATR FTIR; ATTENUATED TOTAL REFLECTIONS; CLOSED-LOOP CONTROL; CONCENTRATION OF; CONTROLLED CRYSTALLIZATION; CRYSTAL PROPERTIES; CRYSTAL SIZE; DYNAMIC CHANGES; FEEDBACK PROCESS; FOURIER TRANSFORM INFRARED; L-GLUTAMIC ACID; L-GLUTAMIC ACIDS; MULTIVARIATE MODELS; PRODUCT CRYSTALS; REACTIVE CRYSTALLIZATION; SEMI-BATCH;

CLOSED LOOP CONTROL SYSTEMS; CRYSTALLIZATION; INFRARED SPECTROSCOPY; POLYMORPHISM; PRECIPITATION (CHEMICAL); SUPERSATURATION;

PROCESS CONTROL;

EID: 77951671041     PISSN: 09307516     EISSN: 15214125     Source Type: Journal    
DOI: 10.1002/ceat.200900550     Document Type: Article

References (37)

1. O. Söhnel, J. Garside, Precipitation: Basic Principles and Industrial Applications, Butterworth-Heinemann, Oxford 1992.
2. H. G. Brittain, Polymorphism in Pharmaceutical Solids, Marcel Dekker, New York 1999.
3. M. Fujiwara, Z. K. Nagy, J. W. Chew, R. D. Braatz, J. Process Control 2005, 15, 493.
4. G. Févotte, Chem. Eng. Res. Des. 2007, 85, 906.
5. Z. Q. Yu et al., Chem. Eng. Res. Des. 2007, 85, 893.
6. F. M. Mirabella Jr., Internal Reflection Spectroscopy. Theory and Applications, Practical Spectroscopy Series, Vol. 15, Marcel Dekker, New York 1993.
7. D. D. Dunuwila, L. B. Carroll II, K. A. Berglund, J. Cryst. Growth 1994, 137, 561.
8. D. D. Dunuwila, K. A. Berglund, J. Cryst. Growth 1997, 179, 185.
9. M. Fujiwara, P. S. Chow, D. L. Ma, R. D. Braatz, Cryst. Growth Des. 2002, 2 (5), 363.
10. V. Liotta, V. Sabesan, Org. Process Res. Dev. 2004, 8, 488.
11. Z. K. Nagy, J. W Chew, M. Fujiwara, R. D. Braatz, J. Process Control 2008, 18, 399.
12. Z. Q. Yu, P. S. Chow, R. B. H. Tan, Org. Process Res. Dev. 2006, 10, 717.
13. G. X. Zhou et al., Cryst. Growth Des. 2006, 6 (4), 892.
14. N. C. S. Kee, R. B. H. Tan, R. D. Braatz, Cryst. Growth Des. 2009, 9 (7), 3044.
15. H. Grön, A. Borissova, K. J. Roberts, Ind. Eng. Chem. Res. 2003, 42, 198.
16. M. W. Hermanto, M.-S. Chiu, X.-Y. Woo, R. D. Braatz, Process Syst. Eng. 2007, 53 (10), 2643.
17. X. Y. Woo, Z. K. Nagy, R. B. H. Tan, R. D. Braatz, Cryst. Growth Des. 2009, 9 (1), 182.
18. E. S. Ferrari, R. J. Davey, Cryst. Growth Des. 2004, 4 (5), 1061.
19. J. Schöll, D. Bonalumi, L. Vicum, M. Mazzotti, Cryst. Growth Des. 2006, 6 (4), 881.
20. J. Schöll, L. Vicum, M. Müller, M. Mazzotti, Chem. Eng. Technol. 2006, 29 (2), 257.
21. C. P.M. Roelands, J. H. ter Horst, H. J. M. Kramer, P. J. Jansens, AIChE J. 2007, 53 (2), 354.
22. H. Alatalo et al., AIChE J., in press. DOI: 10.1002/aic.12137
23. J. I. Partanen, P. M. Juusola, P. O. Minkkinen, Acta Chem. Scand. 1998, 52, 198.
24. A. Borissova et al., Cryst. Growth Des. 2005, 5 (3), 845.
25. H. Alatalo et al., J. Chemom. 2008, 22 (11-12), 644.
26. A. S. Myerson, Handbook of Industrial Crystallization, Butterworth-Heinemann, Oxford 2002.
27. T. Togkalidou et al., Org. Proc. Res. Dev. 2002, 6 (3), 317.
28. H. Qu et al., J. Cryst. Growth 2005, 275, e1857.
29. H. Qu et al., J. Cryst. Growth 2009, 311 (13), 3466.
30. Y. Dai, Master Thesis, Lappeenranta University of Technology 2007.
31. H. Ohtaki, Crystallization Processes, Wiley Series in Solution Chemistry, Vol. 3, John Wiley & Sons, Chichester 1998.
32. T. Ono, J. H. ter Horst, P. J. Jansens, Cryst. Growth Des. 2004, 4 (3), 465.
33. P. Dhamelincourt, F. J. Ramirez, J. Raman Spectrosc. 1991, 22, 582.
34. H. Hatakka et al., Chem. Eng. Technol. 2010, 33 (5). DOI: 10.1002/ceat.200900577
35. N. Hirayama, K. Shirahata, Y. Ohashi, Y. Sasada, Bull. Chem. Soc. Jpn 1980, 53 (1), 30.
36. R. J. Davey, N. Blagden, G. D. Potts, R. Docherty, J. Am. Chem. Soc. 1997, 119, 1767.
37. M. Kitamura, T. Ishizu, J. Cryst. Growth 2000, 209, 138.