Batch cooling crystallization study based on in-line measurement of supersaturation and crystal size distribution

Journal of Crystal Growth

Volumn 275, Issue 1-2, 2005, Pages

  Qu, Haiyan ^a   Pöllänen, Kati ^a   Louhi Kultanen, Marjatta ^a   Kilpiö, Teuvo ^b   Oinas, Pekka ^c   Kallas, Juha ^a  

^a LAPPEENRANTA UNIVERSITY OF TECHNOLOGY   (Finland)

^b KEMIRA OYJ   (Finland)

^c Chem Fine Oy   (Finland)

Author keywords

A2. Growth from solution; A2. Seed crystals; B1. Organic compounds; B3. ATR FTIR

Indexed keywords

ATTENUATION; BENZENE; COOLING; FOURIER TRANSFORM INFRARED SPECTROSCOPY; ORGANIC COMPOUNDS; SENSORS; SPECTROPHOTOMETERS;

ATR FTIR; BATCH COOLING CRYSTALLIZATION; CRYSTAL SIZE DISTRIBUTION; GROWTH FROM SOLUTION; SEED CRYSTALS;

SUPERSATURATION;

EID: 15844369377     PISSN: 00220248     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jcrysgro.2004.11.278     Document Type: Conference Paper

References (8)

1. D.D. Dunuwila, and K.A. Berglund ATR FTIR spectroscopy for in situ measurement of supersaturation J. Crystal Growth 179 1997 185
2. F. Lewiner, J.P. Klein, F. Puel, and G. Fevotte On-line ATR FTIR measurement of supersaturation during solution crystallization processes. Calibration and applications on three solute/solvent systems Chem. Eng. Sci. 56 2001 2069
3. F. Lewiner, G. Fevotte, J.P. Klein, and F. Puel Improving batch cooling seeded crystallization of an organic weed-killer using on-line ATR FTIR measurement of supersaturation J. Crystal Growth 226 2001 348
4. P. Barrett, and B. Clennon In-line FBRM monitoring of particle size in dilute agitated suspensions Part. Part. Syst. Charact. 16 1999 207
5. A. Ruf, J. Worlitschek, and M. Mazzotti Modeling and experimental analysis of PSD measurements through FBRM Part. Part. Syst. Charact. 17 2000 167
6. J.W. Mullin, and J. Nyvlt Programmed cooling of batch crystallizers Chem. Eng. Sci. 26 1971 369
7. A. Höskuldsson Prediction methods in science and technology, Basic Theory vol. 1 1996 Colourscan Warsaw, Poland
8. T. Tähti, M. Louhi-Kultanen, S. Palosaari, On-line measurement of crystal size distribution during batch crystallization, Proceedings of the 14th International Symposium on Industrial Crystallization, Cambridge, UK, 1999.